KR900004625A - 기체성 수소화물의 정제방법 - Google Patents

기체성 수소화물의 정제방법 Download PDF

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Publication number
KR900004625A
KR900004625A KR1019890013748A KR890013748A KR900004625A KR 900004625 A KR900004625 A KR 900004625A KR 1019890013748 A KR1019890013748 A KR 1019890013748A KR 890013748 A KR890013748 A KR 890013748A KR 900004625 A KR900004625 A KR 900004625A
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KR
South Korea
Prior art keywords
nickel
gaseous hydride
selenide
hydride
pipe
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KR1019890013748A
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English (en)
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KR960010082B1 (ko
Inventor
고이찌 기따하라
다까시 시마다
게이이찌 이와따
노보루 아끼따
Original Assignee
야마자기 리요이찌
니혼 파이오닉스 가부시끼가이샤
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Priority claimed from JP63238920A external-priority patent/JP2732262B2/ja
Priority claimed from JP27326788A external-priority patent/JP2592312B2/ja
Priority claimed from JP27617788A external-priority patent/JP2640517B2/ja
Priority claimed from JP28236288A external-priority patent/JP2700396B2/ja
Priority claimed from JP28776588A external-priority patent/JP2627324B2/ja
Priority claimed from JP1004748A external-priority patent/JP2700398B2/ja
Priority claimed from JP1004749A external-priority patent/JP2700399B2/ja
Priority claimed from JP1004750A external-priority patent/JP2700400B2/ja
Priority claimed from JP1022684A external-priority patent/JP2700401B2/ja
Priority claimed from JP1022685A external-priority patent/JP2732277B2/ja
Application filed by 야마자기 리요이찌, 니혼 파이오닉스 가부시끼가이샤 filed Critical 야마자기 리요이찌
Publication of KR900004625A publication Critical patent/KR900004625A/ko
Publication of KR960010082B1 publication Critical patent/KR960010082B1/ko
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B35/00—Boron; Compounds thereof
    • C01B35/02—Boron; Borides
    • C01B35/04—Metal borides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B19/00—Selenium; Tellurium; Compounds thereof
    • C01B19/007—Tellurides or selenides of metals
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B19/00—Selenium; Tellurium; Compounds thereof
    • C01B19/04—Binary compounds including binary selenium-tellurium compounds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/06—Hydrogen phosphides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/08—Other phosphides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/04—Hydrides of silicon
    • C01B33/046—Purification
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/06—Metal silicides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B6/00—Hydrides of metals including fully or partially hydrided metals, alloys or intermetallic compounds ; Compounds containing at least one metal-hydrogen bond, e.g. (GeH3)2S, SiH GeH; Monoborane or diborane; Addition complexes thereof
    • C01B6/34—Purification; Stabilisation

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Silicon Compounds (AREA)
  • Catalysts (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)

Abstract

내용 없음

Description

기체성 수소화물의 정제방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (7)

  1. 조 기체성 수소하물을 니켈 비소화물, 니켈 인화물, 니켈 규화물, 니켈 셀렌화물, 및 니켈 붕소화물중 에서 선택된 적어도 하나의 원(member)과 접촉시켜 조기체성 수소화물중에 함유된 산소를 제거함을 특징으로 하는, 기체성 수소화물의 정제방법.
  2. 제1항에 있어서, 조 기체성 수소화물이 아르신, 포스핀, 실란, 셀렌화 수소 및 디보란중에서 선택된 적어도 하나인 방법.
  3. 제2항에 있어서, 조 기체성 수소화물을 수소 기체 또는 불활성 기체로 희석하는 방법.
  4. 제1항에 있어서, 니켈 비소화물, 니켈 인화물, 니켈 규화물, 니켈 셀렌화물 및 니켈 붕소화물을, 니켈을 아르신, 포스핀, 실란, 셀렌화 수소 및 디보란과 각각 접촉시킴으로써 수득하는 방법.
  5. 제1항에 있어서, 조 기체성 수소화물중에서 함유된 산소를 제거하기 위한, 상기 조 기체성 수소화물과 니켈 비소화물, 니켈 인화물, 니켈 규화물, 니켈 셀렌화물 또는 니켈 붕소화물과의 접촉을, 니켈을 정제용 파이프내에 패킹하고, 기체성 수소화물을 상기 파이프내로 통과시켜 니켈 비소화물, 니켈 인화물, 니켈 규화물, 니켈 셀렌화물 또는 니켈 붕소화물을 형성시킨 다음, 조 기체성 수소화물을 정제용 파이프내로 통과시킴으로써 수행하는 방법.
  6. 제5항에 있어서, 정제용 파이프내에 패킹된 니켈이 촉매 담체에 의해 지지되고, 전체 촉매의 특정 면적이 10 내지 300㎡/g의 범위내이며, 니켈의 함량이 금속 니켈로 산정하여 5 내지 95중량%의 범위내인 방법.
  7. 제5항에 있어서, 정제용 파이프내로 통과하는 조 기체성 수소화물의 유속이 100㎝/초 이하의 선속도(LV)이고 정제용 파이프의 입구에서의 기체 온도가 200℃이하인 방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019890013748A 1988-09-26 1989-09-25 기체성 수소화물의 정제방법 KR960010082B1 (ko)

Applications Claiming Priority (30)

Application Number Priority Date Filing Date Title
JP63238920A JP2732262B2 (ja) 1988-09-26 1988-09-26 アルシンの精製方法
JP88-238920 1988-09-26
JP?238920/88? 1988-09-26
JP?273267/88? 1988-10-31
JP27326788A JP2592312B2 (ja) 1988-10-31 1988-10-31 ホスフィンの精製方法
JP88-273267 1988-10-31
JP?276177/88? 1988-11-02
JP27617788A JP2640517B2 (ja) 1988-11-02 1988-11-02 セレン化水素の精製方法
JP88-276177 1988-11-02
JP88-282362 1988-11-10
JP?282362/88? 1988-11-10
JP28236288A JP2700396B2 (ja) 1988-11-10 1988-11-10 ジボランの精製方法
JP88-287765 1988-11-16
JP28776588A JP2627324B2 (ja) 1988-11-16 1988-11-16 シランの精製方法
JP?287765/88? 1988-11-16
JP1004748A JP2700398B2 (ja) 1989-01-13 1989-01-13 水素化物ガスの精製方法
JP?004749/89? 1989-01-13
JP?004748/89? 1989-01-13
JP?004750/89? 1989-01-13
JP89-004750 1989-01-13
JP1004749A JP2700399B2 (ja) 1989-01-13 1989-01-13 水素化物ガスの精製方法
JP89-004748 1989-01-13
JP1004750A JP2700400B2 (ja) 1989-01-13 1989-01-13 水素化物ガスの精製方法
JP89-004749 1989-01-13
JP1022684A JP2700401B2 (ja) 1989-02-02 1989-02-02 水素化物ガスの精製方法
JP1022685A JP2732277B2 (ja) 1989-02-02 1989-02-02 水素化物ガスの精製方法
JP?022685/89? 1989-02-02
JP89-022684 1989-02-02
JP?022684/89? 1989-02-02
JP89-022685 1989-02-02

Publications (2)

Publication Number Publication Date
KR900004625A true KR900004625A (ko) 1990-04-12
KR960010082B1 KR960010082B1 (ko) 1996-07-25

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Application Number Title Priority Date Filing Date
KR1019890013748A KR960010082B1 (ko) 1988-09-26 1989-09-25 기체성 수소화물의 정제방법

Country Status (4)

Country Link
US (1) US4976942A (ko)
EP (1) EP0361386B1 (ko)
KR (1) KR960010082B1 (ko)
DE (1) DE68911093T2 (ko)

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JP2732262B2 (ja) * 1988-09-26 1998-03-25 日本パイオニクス株式会社 アルシンの精製方法
JP3052317B2 (ja) * 1989-10-25 2000-06-12 三菱瓦斯化学株式会社 脱酸素剤
IT1246358B (it) * 1990-07-12 1994-11-17 Getters Spa Processo per eliminare impurita' da un gas idruro
JPH04318920A (ja) * 1991-04-17 1992-11-10 Mitsubishi Electric Corp 気相結晶成長装置
DE69202014T2 (de) * 1991-07-17 1995-08-31 Japan Pionics Verfahren zur Reinigung von gasförmigen organometallischen Verbindungen.
JP2002511376A (ja) 1998-04-09 2002-04-16 ユーエイチピー・マテリアルズ・インコーポレーテッド ジボランの調製および精製
WO2003037387A2 (en) * 2001-10-31 2003-05-08 Saes Pure Gas, Inc. Air purification system and method for maintaining nitrogen and oxygen ratios with regenerative purification units
US8268046B2 (en) 2008-05-16 2012-09-18 Matheson Tri-Gas Removal of impurities from hydrogen-containing materials
DE102012004417A1 (de) * 2012-03-08 2013-09-12 Technische Universität Bergakademie Freiberg Verfahren zur Herstellung von Aminboranen des Typs R3NBH3
CN105551810B (zh) * 2016-01-01 2018-03-27 三峡大学 一种原位电极的溶剂热制备方法
CN109759051B (zh) * 2019-01-15 2021-10-22 昆明理工大学 一种利用Zr-Nd-O改性白炭黑的催化剂制备方法

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Also Published As

Publication number Publication date
DE68911093D1 (de) 1994-01-13
KR960010082B1 (ko) 1996-07-25
US4976942A (en) 1990-12-11
DE68911093T2 (de) 1994-04-28
EP0361386A2 (en) 1990-04-04
EP0361386A3 (en) 1991-08-28
EP0361386B1 (en) 1993-12-01

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