KR890005300A - 동 또는 동합금 표면의 화학적 연마방법과 배드 - Google Patents
동 또는 동합금 표면의 화학적 연마방법과 배드 Download PDFInfo
- Publication number
- KR890005300A KR890005300A KR1019880012138A KR880012138A KR890005300A KR 890005300 A KR890005300 A KR 890005300A KR 1019880012138 A KR1019880012138 A KR 1019880012138A KR 880012138 A KR880012138 A KR 880012138A KR 890005300 A KR890005300 A KR 890005300A
- Authority
- KR
- South Korea
- Prior art keywords
- bed
- aqueous solution
- copper
- ions
- phosphate ions
- Prior art date
Links
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 title claims description 6
- 229910052802 copper Inorganic materials 0.000 title claims description 6
- 239000010949 copper Substances 0.000 title claims description 6
- 238000000034 method Methods 0.000 title claims description 6
- 238000005498 polishing Methods 0.000 title claims description 6
- 229910000881 Cu alloy Inorganic materials 0.000 title claims 3
- 239000000126 substance Substances 0.000 title claims 3
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims 8
- 239000007864 aqueous solution Substances 0.000 claims 8
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims 6
- NBIIXXVUZAFLBC-UHFFFAOYSA-L Phosphate ion(2-) Chemical compound OP([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-L 0.000 claims 5
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims 4
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims 4
- 229910019142 PO4 Inorganic materials 0.000 claims 2
- 229910052751 metal Inorganic materials 0.000 claims 2
- 239000002184 metal Substances 0.000 claims 2
- 239000010452 phosphate Substances 0.000 claims 2
- 229910052783 alkali metal Inorganic materials 0.000 claims 1
- 229910001514 alkali metal chloride Inorganic materials 0.000 claims 1
- -1 alkali metal salt Chemical class 0.000 claims 1
- 239000000203 mixture Substances 0.000 claims 1
- 238000007517 polishing process Methods 0.000 claims 1
- 239000000243 solution Substances 0.000 claims 1
- 239000000463 material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23F—NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
- C23F3/00—Brightening metals by chemical means
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23F—NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
- C23F3/00—Brightening metals by chemical means
- C23F3/04—Heavy metals
- C23F3/06—Heavy metals with acidic solutions
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- ing And Chemical Polishing (AREA)
Abstract
내용 없음
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
제1도는 연마전의 동표면의 확대 단면도.
제2도는 본 발명의 방법에 따라 연마한 후의 동일한 동표면의 단면도.
제3도는 제료 SU-A-1,211,338에 서술된 연마 방법으로 처리한 후의 제1도와 유사한 동표면의 단면도.
Claims (10)
- 수용액에 대하여 1.25-3의 pH값을 나타내도록 조정된 각 양의 과산화 수소, 염화물 이온과 인산, 인산염 이온과 인산 수소이온의 혼합물 수용액으로 이루어짐을 특징으로 하는 동 또는 동합금 표면의 화학적 연마용 배드.
- 제1항에 있어서, 수용액에서 각 몰양의 인산, 인산염 이온과 인산 수소 이온의 합이 용액 리터당 10-4-1몰임을 특징으로 하는 배드.
- 제2항에 있어서, 수용액에서 각 몰양의 인산, 인산염 이온과 인산 수소 이온이 다음 조건에 적용됨을 특징으로 하는 배드.(여기서는 수용액에서 구성성분를 몰/1로 표시한 농도를 나타낸다)
- 제3항에 있어서, 수용액이 1-6몰/1의 과산화수소와 10-4-1몰/1의 염화물 이온으로 이루어짐을 특징으로하는 배드.
- 제4항에 있어서, 수용액이 1.65-2.35의 pH값을 갖고 다음 성분으로 이루어짐을 특징으로하는 배드 : -3~5몰/1의 과산화 수소; -5×10-3-5×10-2몰/1의 염화물 이온; -다음 관계식에 따른 각 몰양의 인산과 인산염과 인산수소 이온 :
- 제1항 내지 제5항중 어느 한 항에 있어서, 염화물 이온을 알카리 금속 염화물 형태의 수용액으로 도입하고 인산 수소 이온을 인산의 알카리 금속염 형태로 도입함을 특징으로하는 배드.
- 표면을 제1항 내지 제6항중 어느 한 항에 다른 화학적 연마 배드와 접촉시킴을 특징으로하는, 동 또는 동합금 표면의 연마방법.
- 제7항에 있어서, 표면을 배드와 접촉시켜서 최소한 10미크론의 깊이로 금속을 부식시킴을 특징으로 하는 방법.
- 제8항에 있어서, 표면을 배드와 접촉시켜서 20-50미크론의 깊이로 금속을 부식시킴을 특징으로하는연마 방법.
- 제8항 또는 제9항에 있어서, 배드의 온도를 30-60℃로 조정하고, 배드를 1-5시간 동안 표면과 접촉시킴을 특징으로하는 연마 방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR8713407A FR2621052A1 (fr) | 1987-09-25 | 1987-09-25 | Bains et procede pour le polissage chimique de surfaces en cuivre ou en alliage de cuivre |
FR87.13407 | 1987-09-25 |
Publications (1)
Publication Number | Publication Date |
---|---|
KR890005300A true KR890005300A (ko) | 1989-05-13 |
Family
ID=9355301
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019880012138A KR890005300A (ko) | 1987-09-25 | 1988-09-20 | 동 또는 동합금 표면의 화학적 연마방법과 배드 |
Country Status (9)
Country | Link |
---|---|
US (1) | US4981553A (ko) |
EP (1) | EP0309031A1 (ko) |
JP (1) | JPH01159385A (ko) |
KR (1) | KR890005300A (ko) |
BR (1) | BR8804929A (ko) |
DK (1) | DK529488A (ko) |
FI (1) | FI884332A (ko) |
FR (1) | FR2621052A1 (ko) |
NO (1) | NO884228L (ko) |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
BE1003761A3 (fr) * | 1989-10-24 | 1992-06-09 | Solvay | Bains et procede pour le polissage chimique de surfaces en cuivre ou en alliage de cuivre. |
DE4026015A1 (de) * | 1990-08-17 | 1992-02-20 | Hoechst Ag | Verfahren zur herstellung von formkoerpern aus vorstufen oxidischer hochtemperatursupraleiter |
BE1003944A3 (fr) * | 1990-10-02 | 1992-07-22 | Interox Sa | Polymeres organophosphoniques et leur utilisation comme stabilisants de solutions aqueuses de peroxyde d'hydrogene. |
US5454876A (en) * | 1994-08-02 | 1995-10-03 | 21St Century Companies, Inc. | Process for reducing lead leachate in brass plumbing components |
US5609972A (en) * | 1996-03-04 | 1997-03-11 | Polystor Corporation | Cell cap assembly having frangible tab disconnect mechanism |
US5916453A (en) | 1996-09-20 | 1999-06-29 | Fujitsu Limited | Methods of planarizing structures on wafers and substrates by polishing |
US6830627B1 (en) | 1999-03-23 | 2004-12-14 | International Business Machines Corporation | Copper cleaning compositions, processes and products derived therefrom |
Family Cites Families (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2834659A (en) * | 1957-03-25 | 1958-05-13 | Du Pont | Chemical polishing of metals |
US3345217A (en) * | 1964-06-01 | 1967-10-03 | Fremont Ind Inc | Method of cleaning and phosphatizing copper circuits |
US3779842A (en) * | 1972-04-21 | 1973-12-18 | Macdermid Inc | Method of and composition for dissolving metallic copper |
GB1449525A (en) * | 1974-08-21 | 1976-09-15 | Tokai Electro Chemical Co | Method of stabilizing acid aqueous solutions of hydrogen peroxide |
JPS5221223A (en) * | 1975-08-13 | 1977-02-17 | Mitsubishi Gas Chemical Co | Chemical polishing solution for copper and its alloy |
JPS5265725A (en) * | 1975-11-27 | 1977-05-31 | Mitsubishi Gas Chemical Co | Method of chemically polishing metals |
IT1083401B (it) * | 1977-05-27 | 1985-05-21 | Alfachimici Spa | Soluzione acida per l'attacco selettivo del rame |
US4144119A (en) * | 1977-09-30 | 1979-03-13 | Dutkewych Oleh B | Etchant and process |
CA1209886A (en) * | 1982-01-11 | 1986-08-19 | Thomas W. Bleeks | Peroxide selective stripping compositions and method |
FR2539140A1 (fr) * | 1983-01-07 | 1984-07-13 | Ugine Kuhlmann | Stabilisation de solutions aqueuses contenant du peroxyde d'hydrogene, de l'acide fluorhydrique et des ions metalliques |
US4788086A (en) * | 1984-07-14 | 1988-11-29 | Nippondenso Co., Ltd. | Copper-based metallic member having a chemical conversion film and method for producing same |
SU1211338A1 (ru) * | 1984-07-18 | 1986-02-15 | Ордена Трудового Красного Знамени Институт Органической И Физической Химии Им.А.Е.Арбузова | Раствор дл химического полировани меди и ее сплавов |
JPS61124585A (ja) * | 1984-11-21 | 1986-06-12 | Kosaku:Kk | プリント基板製造用銅エツチング液の濃度管理法 |
JPS62237447A (ja) * | 1986-04-08 | 1987-10-17 | Mitsubishi Paper Mills Ltd | 一液型エツチングブリ−チ液 |
DE3623504A1 (de) * | 1986-07-09 | 1988-01-21 | Schering Ag | Kupferaetzloesungen |
-
1987
- 1987-09-25 FR FR8713407A patent/FR2621052A1/fr not_active Withdrawn
-
1988
- 1988-09-13 EP EP88201981A patent/EP0309031A1/fr not_active Withdrawn
- 1988-09-16 US US07/245,340 patent/US4981553A/en not_active Expired - Fee Related
- 1988-09-20 KR KR1019880012138A patent/KR890005300A/ko not_active Application Discontinuation
- 1988-09-21 FI FI884332A patent/FI884332A/fi not_active IP Right Cessation
- 1988-09-23 NO NO88884228A patent/NO884228L/no unknown
- 1988-09-23 BR BR8804929A patent/BR8804929A/pt unknown
- 1988-09-23 DK DK529488A patent/DK529488A/da not_active Application Discontinuation
- 1988-09-26 JP JP63240636A patent/JPH01159385A/ja active Pending
Also Published As
Publication number | Publication date |
---|---|
NO884228L (no) | 1989-03-28 |
DK529488A (da) | 1989-03-26 |
BR8804929A (pt) | 1989-05-02 |
DK529488D0 (da) | 1988-09-23 |
US4981553A (en) | 1991-01-01 |
FR2621052A1 (fr) | 1989-03-31 |
JPH01159385A (ja) | 1989-06-22 |
NO884228D0 (no) | 1988-09-23 |
FI884332A0 (fi) | 1988-09-21 |
FI884332A (fi) | 1989-03-26 |
EP0309031A1 (fr) | 1989-03-29 |
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WITN | Application deemed withdrawn, e.g. because no request for examination was filed or no examination fee was paid |