KR860000929B1 - 에폭시화 반응 생성물의 가수분해성 클로라이드의 감량방법 - Google Patents

에폭시화 반응 생성물의 가수분해성 클로라이드의 감량방법 Download PDF

Info

Publication number
KR860000929B1
KR860000929B1 KR1019840002181A KR840002181A KR860000929B1 KR 860000929 B1 KR860000929 B1 KR 860000929B1 KR 1019840002181 A KR1019840002181 A KR 1019840002181A KR 840002181 A KR840002181 A KR 840002181A KR 860000929 B1 KR860000929 B1 KR 860000929B1
Authority
KR
South Korea
Prior art keywords
product
toluene
reaction
mixture
mek
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
KR1019840002181A
Other languages
English (en)
Korean (ko)
Other versions
KR850007441A (ko
Inventor
엘. 카스키 테렌스
에치. 마틴 패트릭
엘. 파커 데오도르
Original Assignee
더 다우 케미칼 캄파니
리차드 고든 워터맨
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=23917350&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=KR860000929(B1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by 더 다우 케미칼 캄파니, 리차드 고든 워터맨 filed Critical 더 다우 케미칼 캄파니
Publication of KR850007441A publication Critical patent/KR850007441A/ko
Application granted granted Critical
Publication of KR860000929B1 publication Critical patent/KR860000929B1/ko
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D301/00Preparation of oxiranes
    • C07D301/27Condensation of epihalohydrins or halohydrins with compounds containing active hydrogen atoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D303/00Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
    • C07D303/02Compounds containing oxirane rings
    • C07D303/12Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms
    • C07D303/18Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms by etherified hydroxyl radicals
    • C07D303/20Ethers with hydroxy compounds containing no oxirane rings
    • C07D303/24Ethers with hydroxy compounds containing no oxirane rings with polyhydroxy compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D301/00Preparation of oxiranes
    • C07D301/32Separation; Purification
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Epoxy Resins (AREA)
  • Epoxy Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Phenolic Resins Or Amino Resins (AREA)
KR1019840002181A 1983-04-07 1984-04-24 에폭시화 반응 생성물의 가수분해성 클로라이드의 감량방법 Expired KR860000929B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US482,760 1983-04-07
US06/482,760 US4447598A (en) 1983-04-07 1983-04-07 Method of preparing epoxy resins having low hydrolyzable chloride contents

Publications (2)

Publication Number Publication Date
KR850007441A KR850007441A (ko) 1985-12-04
KR860000929B1 true KR860000929B1 (ko) 1986-07-19

Family

ID=23917350

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019840002181A Expired KR860000929B1 (ko) 1983-04-07 1984-04-24 에폭시화 반응 생성물의 가수분해성 클로라이드의 감량방법

Country Status (11)

Country Link
US (1) US4447598A (https=)
EP (1) EP0125454B1 (https=)
JP (1) JPS59206430A (https=)
KR (1) KR860000929B1 (https=)
AU (1) AU562838B2 (https=)
BR (1) BR8401625A (https=)
CA (1) CA1203942A (https=)
DE (1) DE3469298D1 (https=)
ES (1) ES8607267A1 (https=)
GB (1) GB2137629A (https=)
MY (1) MY101974A (https=)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4485221A (en) * 1983-11-03 1984-11-27 Ciba-Geigy Corporation Process for making epoxy novolac resins with low hydrolyzable chlorine and low ionic chloride content
US4585838A (en) * 1985-08-06 1986-04-29 The Dow Chemical Company Process for preparing epoxy resins containing low levels of total halide
CN1004356B (zh) * 1984-11-19 1989-05-31 陶氏化学公司 一种降低环氧树脂中卤化物总含量的工艺方法
US4535150A (en) * 1984-12-04 1985-08-13 Celanese Corporation Process for preparing epoxy resins having low hydrolyzable chlorine contents
JPS61195111A (ja) * 1985-02-25 1986-08-29 Toto Kasei Kk エポキシ樹脂の製造方法
US4684700A (en) * 1986-02-14 1987-08-04 The Dow Chemical Company Advanced epoxy resins prepared from triglycidyl ethers and dihydri phenols
US4684701A (en) * 1986-02-14 1987-08-04 The Dow Chemical Company Method for preparing advanced epoxy or phenoxy resins with low aliphatic halide content
US4672103A (en) * 1986-02-14 1987-06-09 The Dow Chemical Company Non-sintering epoxy resins prepared from triglycidyl ethers and epihalohydrins
JPH0621150B2 (ja) * 1986-03-13 1994-03-23 旭チバ株式会社 エポキシ樹脂の製造方法
US4810776A (en) * 1986-07-14 1989-03-07 Ciba-Geigy Corporation Process for producing epoxy resin having a low-EHC-content from chlorine-substituted crude epoxy resin of high EHC-content and apparatus for automatically controlling such process
US4696982A (en) * 1986-09-17 1987-09-29 The Dow Chemical Company Process for removing residual salts from epoxy novolacs
DE3636560A1 (de) * 1986-10-28 1988-05-05 Ruetgerswerke Ag Verfahren zur entsalzung von steinkohlenteeren und -pechen
US4785061A (en) * 1987-08-13 1988-11-15 The Dow Chemical Company Method for reducing the aliphatic halide content of epoxy resins using a solvent mixture including a polar aprotic solvent
US4778863A (en) * 1987-08-13 1988-10-18 The Dow Chemical Company Preparation of epoxy resins having low undesirable halogen content
US4877857A (en) * 1988-05-05 1989-10-31 The Dow Chemical Company Preparation of epoxy resins
JP2702515B2 (ja) * 1988-08-10 1998-01-21 旭チバ株式会社 エポキシ樹脂の精製法
PL172981B1 (pl) * 1994-01-26 1998-01-30 Inst Ciezkiej Syntezy Orga Sposób wytwarzania płynnych żywic epoksydowych
TW593401B (en) * 1998-05-29 2004-06-21 Sumitomo Chemical Co Highly purified epoxy resin having glycidylamino group and the process thereof
JP4907821B2 (ja) 1999-12-07 2012-04-04 スリーエム イノベイティブ プロパティズ カンパニー 加水分解性ハロゲン化物および他の高分子量材料を含有する材料をエピハロヒドリン誘導エポキシ樹脂から除去する方法
US6211389B1 (en) 2000-05-23 2001-04-03 Dexter Corporation Methods of reducing the chloride content of epoxy compounds
CN115010856A (zh) * 2022-07-20 2022-09-06 杜彪 一种除氯剂的制备方法、除氯剂及其应用

Family Cites Families (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB746824A (en) * 1952-08-01 1956-03-21 Ici Ltd Resins derived from phenol-formaldehyde condensates and epichlorohydrin
NL186312B (nl) * 1953-04-06 Henkel Kgaa Werkwijze ter bereiding van guerbet-alcoholen onder toepassing van een loodzout als katalysator.
US2943095A (en) * 1955-06-28 1960-06-28 Union Carbide Corp Process for preparing glycidyl polyethers of polyhydric phenols
GB801728A (en) * 1956-04-19 1958-09-17 Basf Ag Improvements in the production of glycidyl ethers
GB868861A (en) * 1957-07-18 1961-05-25 Union Carbide Corp Preparation of glycidyl polyethers of polyhydric phenols
NL234777A (https=) * 1959-01-02
NL270270A (https=) * 1960-10-17
GB1173191A (en) * 1965-12-31 1969-12-03 Muanyagipari Ki Process for Preparing Liquid Epoxy Oligomers
GB1169045A (en) * 1967-07-21 1969-10-29 Midland Silicones Ltd Novel Epoxylated Phenolic Resins
CH505084A (de) * 1968-12-06 1971-03-31 Ciba Geigy Ag Verfahren zur Herstellung von Polyglycidyläthern
NL161752C (nl) * 1969-06-10 1980-08-15 Shell Int Research Werkwijze voor het bereiden van laagmoleculaire polyglycidijlethers.
CH544801A (de) * 1970-03-16 1973-11-30 Reichhold Albert Chemie Ag Verfahren zum Herstellen von Glycidyläthern
CH541596A (de) * 1970-05-14 1973-09-15 Texaco Ag Verfahren zur Herstellung von basischen, stickstoff- und hydroxylgruppenhaltigen Epoxidharzen
US4394496A (en) * 1971-08-19 1983-07-19 The Dow Chemical Company Epoxidation products of 1,1,1-tri-(hydroxyphenyl) alkanes
IT1012923B (it) * 1974-05-30 1977-03-10 Sir Soc Italiana Resine Spa Procedimento per la preparazione continua di eteri poliglicidilici di fenoli poliossidrilici
DE2533505C3 (de) * 1974-08-02 1981-10-08 Hoechst Ag, 6000 Frankfurt Verfahren zum Herstellen von niedrigviskosen, niedermolekularen Glycidyläthern ein- oder mehrwertiger Phenole
IT1051400B (it) * 1975-12-19 1981-04-21 S I R S P A Procedimento perfezionato per la preparazione di resine epossidiche liquide
DE2745150A1 (de) * 1976-12-04 1978-06-08 Leuna Werke Veb Kontinuierliche herstellung und reinigung von epoxidharzen
GB2001991B (en) * 1977-06-30 1982-01-06 Shell Int Research Preparation of polyglycidyl ethers of polyhydric phenols
CA1144933A (en) * 1979-04-19 1983-04-19 Johan Van Gogh Process for the preparation of polyglycidyl ethers of polyhydric phenols
DD158479A3 (de) * 1981-03-31 1983-01-19 Wolfgang Boehm Verfahren zur kontinuierlichen herstellung von epoxidharzen

Also Published As

Publication number Publication date
ES531352A0 (es) 1985-12-16
KR850007441A (ko) 1985-12-04
ES8607267A1 (es) 1985-12-16
AU2637684A (en) 1984-10-11
DE3469298D1 (en) 1988-03-17
JPS59206430A (ja) 1984-11-22
JPH0377208B2 (https=) 1991-12-09
MY101974A (en) 1992-02-29
BR8401625A (pt) 1984-11-13
EP0125454B1 (en) 1988-02-10
GB2137629A (en) 1984-10-10
GB8409035D0 (en) 1984-05-16
EP0125454A1 (en) 1984-11-21
AU562838B2 (en) 1987-06-18
CA1203942A (en) 1986-04-29
US4447598A (en) 1984-05-08

Similar Documents

Publication Publication Date Title
KR860000929B1 (ko) 에폭시화 반응 생성물의 가수분해성 클로라이드의 감량방법
US4499255A (en) Preparation of epoxy resins
US3305565A (en) Polyepihalohydrin preparation using fluoboric acid catalyst
JPS58219173A (ja) 二官能エポキシドおよびエポキシ樹脂
US4535150A (en) Process for preparing epoxy resins having low hydrolyzable chlorine contents
EP0103282B1 (en) A process for preparing glycidyl derivatives of compounds having at least one aromatic hydroxyl group or aromatic amine group
US2864805A (en) Epoxide resins
US3514418A (en) Epoxy ethers,their preparation and cured products obtained therefrom
US3600362A (en) Epoxy resin cured with liquid resinous amine curing agents
US3842037A (en) Process for preparing higher molecular weight polyepoxide products by condensing lower molecular weight polyepoxide with polyhydric phenols
US4764580A (en) High functionality, low melt viscosity, flakable solid epoxy resin with good heat resistance
CA1085990A (en) Method for the preparation of novolak epoxy resins
JPS6252764B2 (https=)
EP0340716A2 (en) Preparation of epoxy resins
CA1293837C (en) Preparation of epoxy resins
US4337367A (en) Oligomer of m-isopropenylphenol
CN104136478A (zh) 环十二烷多酚的环氧树脂的制备和用途
US3351673A (en) Process for preparing composite epoxide resins
JPS6222988B2 (https=)
US3867346A (en) Process for the production of liquid epoxy-novolak resins and product thereof
US3383432A (en) Epoxide composition containing the polyglycidyl ethers of 2, 4-bis-(4-hydroxycumyl)-phenol, bis-(4-hydroxy cumyl)-bis-(4-hydroxy-phenyl) 2, 2-propane and 2, 2-bis-(4-hydroxy phenyl)-propane
JPS6317852B2 (https=)
US3325452A (en) Preparation of glycidyl polyethers
US3530096A (en) Reduction of hydroxyl group content of epoxide resins
US4783519A (en) High functionality, low melt viscosity, flakable solid epoxy resin with good heat resistance

Legal Events

Date Code Title Description
A201 Request for examination
PA0109 Patent application

St.27 status event code: A-0-1-A10-A12-nap-PA0109

PA0201 Request for examination

St.27 status event code: A-1-2-D10-D11-exm-PA0201

R17-X000 Change to representative recorded

St.27 status event code: A-3-3-R10-R17-oth-X000

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

PG1501 Laying open of application

St.27 status event code: A-1-1-Q10-Q12-nap-PG1501

G160 Decision to publish patent application
PG1605 Publication of application before grant of patent

St.27 status event code: A-2-2-Q10-Q13-nap-PG1605

E701 Decision to grant or registration of patent right
PE0701 Decision of registration

St.27 status event code: A-1-2-D10-D22-exm-PE0701

GRNT Written decision to grant
PR0701 Registration of establishment

St.27 status event code: A-2-4-F10-F11-exm-PR0701

PR1002 Payment of registration fee

St.27 status event code: A-2-2-U10-U11-oth-PR1002

Fee payment year number: 1

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 4

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 5

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 6

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 7

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 8

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 9

FPAY Annual fee payment

Payment date: 19950620

Year of fee payment: 10

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 10

LAPS Lapse due to unpaid annual fee
PC1903 Unpaid annual fee

St.27 status event code: A-4-4-U10-U13-oth-PC1903

Not in force date: 19960720

Payment event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

PC1903 Unpaid annual fee

St.27 status event code: N-4-6-H10-H13-oth-PC1903

Ip right cessation event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

Not in force date: 19960720

PN2301 Change of applicant

St.27 status event code: A-5-5-R10-R13-asn-PN2301

St.27 status event code: A-5-5-R10-R11-asn-PN2301

PN2301 Change of applicant

St.27 status event code: A-5-5-R10-R13-asn-PN2301

St.27 status event code: A-5-5-R10-R11-asn-PN2301

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000

PN2301 Change of applicant

St.27 status event code: A-5-5-R10-R13-asn-PN2301

St.27 status event code: A-5-5-R10-R11-asn-PN2301

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000