KR860000929B1 - 에폭시화 반응 생성물의 가수분해성 클로라이드의 감량방법 - Google Patents
에폭시화 반응 생성물의 가수분해성 클로라이드의 감량방법 Download PDFInfo
- Publication number
- KR860000929B1 KR860000929B1 KR1019840002181A KR840002181A KR860000929B1 KR 860000929 B1 KR860000929 B1 KR 860000929B1 KR 1019840002181 A KR1019840002181 A KR 1019840002181A KR 840002181 A KR840002181 A KR 840002181A KR 860000929 B1 KR860000929 B1 KR 860000929B1
- Authority
- KR
- South Korea
- Prior art keywords
- product
- toluene
- reaction
- mixture
- mek
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/27—Condensation of epihalohydrins or halohydrins with compounds containing active hydrogen atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
- C07D303/02—Compounds containing oxirane rings
- C07D303/12—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms
- C07D303/18—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms by etherified hydroxyl radicals
- C07D303/20—Ethers with hydroxy compounds containing no oxirane rings
- C07D303/24—Ethers with hydroxy compounds containing no oxirane rings with polyhydroxy compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/32—Separation; Purification
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Epoxy Resins (AREA)
- Epoxy Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Phenolic Resins Or Amino Resins (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US482,760 | 1983-04-07 | ||
| US06/482,760 US4447598A (en) | 1983-04-07 | 1983-04-07 | Method of preparing epoxy resins having low hydrolyzable chloride contents |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR850007441A KR850007441A (ko) | 1985-12-04 |
| KR860000929B1 true KR860000929B1 (ko) | 1986-07-19 |
Family
ID=23917350
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1019840002181A Expired KR860000929B1 (ko) | 1983-04-07 | 1984-04-24 | 에폭시화 반응 생성물의 가수분해성 클로라이드의 감량방법 |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US4447598A (https=) |
| EP (1) | EP0125454B1 (https=) |
| JP (1) | JPS59206430A (https=) |
| KR (1) | KR860000929B1 (https=) |
| AU (1) | AU562838B2 (https=) |
| BR (1) | BR8401625A (https=) |
| CA (1) | CA1203942A (https=) |
| DE (1) | DE3469298D1 (https=) |
| ES (1) | ES8607267A1 (https=) |
| GB (1) | GB2137629A (https=) |
| MY (1) | MY101974A (https=) |
Families Citing this family (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4485221A (en) * | 1983-11-03 | 1984-11-27 | Ciba-Geigy Corporation | Process for making epoxy novolac resins with low hydrolyzable chlorine and low ionic chloride content |
| US4585838A (en) * | 1985-08-06 | 1986-04-29 | The Dow Chemical Company | Process for preparing epoxy resins containing low levels of total halide |
| CN1004356B (zh) * | 1984-11-19 | 1989-05-31 | 陶氏化学公司 | 一种降低环氧树脂中卤化物总含量的工艺方法 |
| US4535150A (en) * | 1984-12-04 | 1985-08-13 | Celanese Corporation | Process for preparing epoxy resins having low hydrolyzable chlorine contents |
| JPS61195111A (ja) * | 1985-02-25 | 1986-08-29 | Toto Kasei Kk | エポキシ樹脂の製造方法 |
| US4684700A (en) * | 1986-02-14 | 1987-08-04 | The Dow Chemical Company | Advanced epoxy resins prepared from triglycidyl ethers and dihydri phenols |
| US4684701A (en) * | 1986-02-14 | 1987-08-04 | The Dow Chemical Company | Method for preparing advanced epoxy or phenoxy resins with low aliphatic halide content |
| US4672103A (en) * | 1986-02-14 | 1987-06-09 | The Dow Chemical Company | Non-sintering epoxy resins prepared from triglycidyl ethers and epihalohydrins |
| JPH0621150B2 (ja) * | 1986-03-13 | 1994-03-23 | 旭チバ株式会社 | エポキシ樹脂の製造方法 |
| US4810776A (en) * | 1986-07-14 | 1989-03-07 | Ciba-Geigy Corporation | Process for producing epoxy resin having a low-EHC-content from chlorine-substituted crude epoxy resin of high EHC-content and apparatus for automatically controlling such process |
| US4696982A (en) * | 1986-09-17 | 1987-09-29 | The Dow Chemical Company | Process for removing residual salts from epoxy novolacs |
| DE3636560A1 (de) * | 1986-10-28 | 1988-05-05 | Ruetgerswerke Ag | Verfahren zur entsalzung von steinkohlenteeren und -pechen |
| US4785061A (en) * | 1987-08-13 | 1988-11-15 | The Dow Chemical Company | Method for reducing the aliphatic halide content of epoxy resins using a solvent mixture including a polar aprotic solvent |
| US4778863A (en) * | 1987-08-13 | 1988-10-18 | The Dow Chemical Company | Preparation of epoxy resins having low undesirable halogen content |
| US4877857A (en) * | 1988-05-05 | 1989-10-31 | The Dow Chemical Company | Preparation of epoxy resins |
| JP2702515B2 (ja) * | 1988-08-10 | 1998-01-21 | 旭チバ株式会社 | エポキシ樹脂の精製法 |
| PL172981B1 (pl) * | 1994-01-26 | 1998-01-30 | Inst Ciezkiej Syntezy Orga | Sposób wytwarzania płynnych żywic epoksydowych |
| TW593401B (en) * | 1998-05-29 | 2004-06-21 | Sumitomo Chemical Co | Highly purified epoxy resin having glycidylamino group and the process thereof |
| JP4907821B2 (ja) | 1999-12-07 | 2012-04-04 | スリーエム イノベイティブ プロパティズ カンパニー | 加水分解性ハロゲン化物および他の高分子量材料を含有する材料をエピハロヒドリン誘導エポキシ樹脂から除去する方法 |
| US6211389B1 (en) | 2000-05-23 | 2001-04-03 | Dexter Corporation | Methods of reducing the chloride content of epoxy compounds |
| CN115010856A (zh) * | 2022-07-20 | 2022-09-06 | 杜彪 | 一种除氯剂的制备方法、除氯剂及其应用 |
Family Cites Families (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB746824A (en) * | 1952-08-01 | 1956-03-21 | Ici Ltd | Resins derived from phenol-formaldehyde condensates and epichlorohydrin |
| NL186312B (nl) * | 1953-04-06 | Henkel Kgaa | Werkwijze ter bereiding van guerbet-alcoholen onder toepassing van een loodzout als katalysator. | |
| US2943095A (en) * | 1955-06-28 | 1960-06-28 | Union Carbide Corp | Process for preparing glycidyl polyethers of polyhydric phenols |
| GB801728A (en) * | 1956-04-19 | 1958-09-17 | Basf Ag | Improvements in the production of glycidyl ethers |
| GB868861A (en) * | 1957-07-18 | 1961-05-25 | Union Carbide Corp | Preparation of glycidyl polyethers of polyhydric phenols |
| NL234777A (https=) * | 1959-01-02 | |||
| NL270270A (https=) * | 1960-10-17 | |||
| GB1173191A (en) * | 1965-12-31 | 1969-12-03 | Muanyagipari Ki | Process for Preparing Liquid Epoxy Oligomers |
| GB1169045A (en) * | 1967-07-21 | 1969-10-29 | Midland Silicones Ltd | Novel Epoxylated Phenolic Resins |
| CH505084A (de) * | 1968-12-06 | 1971-03-31 | Ciba Geigy Ag | Verfahren zur Herstellung von Polyglycidyläthern |
| NL161752C (nl) * | 1969-06-10 | 1980-08-15 | Shell Int Research | Werkwijze voor het bereiden van laagmoleculaire polyglycidijlethers. |
| CH544801A (de) * | 1970-03-16 | 1973-11-30 | Reichhold Albert Chemie Ag | Verfahren zum Herstellen von Glycidyläthern |
| CH541596A (de) * | 1970-05-14 | 1973-09-15 | Texaco Ag | Verfahren zur Herstellung von basischen, stickstoff- und hydroxylgruppenhaltigen Epoxidharzen |
| US4394496A (en) * | 1971-08-19 | 1983-07-19 | The Dow Chemical Company | Epoxidation products of 1,1,1-tri-(hydroxyphenyl) alkanes |
| IT1012923B (it) * | 1974-05-30 | 1977-03-10 | Sir Soc Italiana Resine Spa | Procedimento per la preparazione continua di eteri poliglicidilici di fenoli poliossidrilici |
| DE2533505C3 (de) * | 1974-08-02 | 1981-10-08 | Hoechst Ag, 6000 Frankfurt | Verfahren zum Herstellen von niedrigviskosen, niedermolekularen Glycidyläthern ein- oder mehrwertiger Phenole |
| IT1051400B (it) * | 1975-12-19 | 1981-04-21 | S I R S P A | Procedimento perfezionato per la preparazione di resine epossidiche liquide |
| DE2745150A1 (de) * | 1976-12-04 | 1978-06-08 | Leuna Werke Veb | Kontinuierliche herstellung und reinigung von epoxidharzen |
| GB2001991B (en) * | 1977-06-30 | 1982-01-06 | Shell Int Research | Preparation of polyglycidyl ethers of polyhydric phenols |
| CA1144933A (en) * | 1979-04-19 | 1983-04-19 | Johan Van Gogh | Process for the preparation of polyglycidyl ethers of polyhydric phenols |
| DD158479A3 (de) * | 1981-03-31 | 1983-01-19 | Wolfgang Boehm | Verfahren zur kontinuierlichen herstellung von epoxidharzen |
-
1983
- 1983-04-07 US US06/482,760 patent/US4447598A/en not_active Expired - Lifetime
-
1984
- 1984-04-03 AU AU26376/84A patent/AU562838B2/en not_active Ceased
- 1984-04-04 DE DE8484103685T patent/DE3469298D1/de not_active Expired
- 1984-04-04 EP EP84103685A patent/EP0125454B1/en not_active Expired
- 1984-04-06 GB GB08409035A patent/GB2137629A/en not_active Withdrawn
- 1984-04-06 ES ES531352A patent/ES8607267A1/es not_active Expired
- 1984-04-06 CA CA000451472A patent/CA1203942A/en not_active Expired
- 1984-04-06 BR BR8401625A patent/BR8401625A/pt not_active IP Right Cessation
- 1984-04-07 JP JP59069890A patent/JPS59206430A/ja active Granted
- 1984-04-24 KR KR1019840002181A patent/KR860000929B1/ko not_active Expired
-
1987
- 1987-08-10 MY MYPI87001260A patent/MY101974A/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| ES531352A0 (es) | 1985-12-16 |
| KR850007441A (ko) | 1985-12-04 |
| ES8607267A1 (es) | 1985-12-16 |
| AU2637684A (en) | 1984-10-11 |
| DE3469298D1 (en) | 1988-03-17 |
| JPS59206430A (ja) | 1984-11-22 |
| JPH0377208B2 (https=) | 1991-12-09 |
| MY101974A (en) | 1992-02-29 |
| BR8401625A (pt) | 1984-11-13 |
| EP0125454B1 (en) | 1988-02-10 |
| GB2137629A (en) | 1984-10-10 |
| GB8409035D0 (en) | 1984-05-16 |
| EP0125454A1 (en) | 1984-11-21 |
| AU562838B2 (en) | 1987-06-18 |
| CA1203942A (en) | 1986-04-29 |
| US4447598A (en) | 1984-05-08 |
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| A201 | Request for examination | ||
| PA0109 | Patent application |
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