KR840007864A - 오르토-벤조일벤조산, 플루오르화수소 및 삼플루오르화붕소의 착물분해 방법 - Google Patents

오르토-벤조일벤조산, 플루오르화수소 및 삼플루오르화붕소의 착물분해 방법 Download PDF

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Publication number
KR840007864A
KR840007864A KR1019840001625A KR840001625A KR840007864A KR 840007864 A KR840007864 A KR 840007864A KR 1019840001625 A KR1019840001625 A KR 1019840001625A KR 840001625 A KR840001625 A KR 840001625A KR 840007864 A KR840007864 A KR 840007864A
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KR
South Korea
Prior art keywords
complex
ortho
weight
sulfuric acid
hydrogen fluoride
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KR1019840001625A
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English (en)
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KR900003141B1 (ko
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데빅 미쉘
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미쉘 로쉐
소시에떼 아토샹
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C50/00—Quinones
    • C07C50/16—Quinones the quinoid structure being part of a condensed ring system containing three rings
    • C07C50/18—Anthraquinones, i.e. C14H8O2
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C46/00—Preparation of quinones
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/584—Recycling of catalysts

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

내용 없음.

Description

오르토-벤조일벤조산, 플루오르화수소 및 삼플루오르화붕소의 착물분해 방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
제1도는 본 발명을 구체적으로 나타대는 도식적인 유통도.

Claims (7)

  1. HF와 BF3의 회수 및 오르토-벤조일벤조산의 고리화로 생성되는 안트라퀴논을 수득하기 위한 하기 일반식(Ⅰ)로 표시되는 착물을 최대한 대기압하에서, 100 내지 180℃의 온도로, 최소한 96중량% 농도의 황산 또는 발연황산과 작용시킴을 특징으로 하는 하기 일반식(Ⅰ)의 오르토-벤조일벤조산, 플루오르화수소 및 삼플루오르화붕소의 착물분해 방법.
    (식중에서, n 및 m은 1 내지 6이다.)
  2. 제1항에 있어서, 황산의 중량이 착물에 함유된 오르토-벤조일벤조산 중량의 1내지 3배임을 특징으로 하는 방법.
  3. 제1항에 있어서, 발연황산의 중량이 착물에 함유된 오르토-벤조일벤조산 중량의 0.5내지 2배임을 특징으로 하는 방법.
  4. 제1 내지 3항중 어느 한항에 있어서, 착물분해 기간이 15분 내지 2시간임을 특징으로 하는 방법.
  5. 제1 내지 4항중 어느 한항에 있어서, 착물분해가 착물에 함유된 플루오르화수소 전부 또는 일부를 삼플루오르화붕소로 전환하기에 충분한 양의 붕산 존재하에서 수행됨을 특징으로 하는 방법.
  6. 제1 내지 5항중 어느 한항에 있어서, 최종 반응 혼합물이 안트라퀴논을 침전시키기 위해 물로 희석됨을 특징으로 하는 방법.
  7. 제1 내지 5항중 어느한항에 있어서, 최종반응 매질이 안트라퀴논을 침전시키기 위해 황산수용액으로 희석됨을 특징으로 하는 방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019840001625A 1983-03-30 1984-03-29 오르토-벤조일벤조산, 플루오르화수소 및 삼플루오르화 붕소의 착물 분해 방법 KR900003141B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR8305207A FR2543544B1 (fr) 1983-03-30 1983-03-30 Procede de decomposition d'un complexe d'acide orthobenzoyl-benzoique, de fluorure d'hydrogene et de trifluorure de bore
FR05207 1983-03-30
FR8305207 1983-03-30

Publications (2)

Publication Number Publication Date
KR840007864A true KR840007864A (ko) 1984-12-11
KR900003141B1 KR900003141B1 (ko) 1990-05-09

Family

ID=9287370

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019840001625A KR900003141B1 (ko) 1983-03-30 1984-03-29 오르토-벤조일벤조산, 플루오르화수소 및 삼플루오르화 붕소의 착물 분해 방법

Country Status (12)

Country Link
US (1) US4591460A (ko)
EP (1) EP0121466B1 (ko)
JP (1) JPS59184145A (ko)
KR (1) KR900003141B1 (ko)
CA (1) CA1204110A (ko)
CS (1) CS241076B2 (ko)
DE (2) DE3465466D1 (ko)
ES (1) ES531088A0 (ko)
FI (1) FI78288C (ko)
FR (1) FR2543544B1 (ko)
IN (1) IN160308B (ko)
PL (1) PL246877A1 (ko)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2572396B1 (fr) * 1984-10-31 1986-12-19 Atochem Procede de preparation d'amyl-2-anthraquinone a partir d'amyl-benzene et d'anhydride phtalique
FR2575154B1 (fr) * 1984-12-21 1987-01-23 Atochem Procede de preparation d'anthraquinone
JPH0513664Y2 (ko) * 1988-03-19 1993-04-12
NL8802732A (nl) * 1988-11-08 1990-06-01 Philips Nv Magnetische resonantiewerkwijze en -inrichting.
US5041571A (en) * 1990-03-29 1991-08-20 Hoechst Celanese Corporation Process of producing anthraquinones in one step
FR2731705B1 (fr) * 1995-03-15 1997-04-30 Atochem Elf Sa Procede de synthese de 2-ethyl-anthraquinone
FR2748023B1 (fr) * 1996-04-30 1998-07-24 Rhone Poulenc Chimie Hydrogenofluorosulfonates de base organique, leur utilisation pour liberer les bases organiques de leur fluorhydrate, leur procede de preparation, compositions les comportant

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1895788A (en) * 1923-11-21 1933-01-31 Nat Aniline & Chem Co Inc Process of making anthraquinones
US2496894A (en) * 1947-02-26 1950-02-07 American Cyanamid Co Manufacture of anthraquinone
US3032560A (en) * 1959-05-29 1962-05-01 Lynn H Dawsey Process for preparing amylanthraquinone
US4035396A (en) * 1975-04-07 1977-07-12 E. I. Du Pont De Nemours And Company Process for preparing alkylanthraquinone
DE2527491C2 (de) * 1975-06-20 1983-06-09 Basf Ag, 6700 Ludwigshafen Verfahren zur Herstellung von Anthrachinonen
AT351019B (de) * 1976-05-10 1979-07-10 Yamamoto Kagaku Gosei Kk Verfahren zur herstellung von 2-(p-amylbenzoyl) -benzoesaeure
JPS5547639A (en) * 1978-09-29 1980-04-04 Mitsubishi Chem Ind Ltd Preparation of alkylanthraquinone
FR2496097A1 (fr) * 1980-12-16 1982-06-18 Ugine Kuhlmann Procede pour la preparation de l'anthraquinone et de ses derives substitues
FR2532303A1 (fr) * 1982-09-01 1984-03-02 Ugine Kuhlmann Procede de decomposition d'un complexe d'acide ortho-benzoyl-benzoique, de fluorure d'hydrogene et de trifluorure de bore

Also Published As

Publication number Publication date
CS218684A2 (en) 1985-06-13
CS241076B2 (en) 1986-03-13
FR2543544B1 (fr) 1986-01-17
JPS59184145A (ja) 1984-10-19
CA1204110A (fr) 1986-05-06
KR900003141B1 (ko) 1990-05-09
FR2543544A1 (fr) 1984-10-05
US4591460A (en) 1986-05-27
IN160308B (ko) 1987-07-04
ES8501730A1 (es) 1984-12-01
FI78288C (fi) 1989-07-10
DE121466T1 (de) 1985-04-11
ES531088A0 (es) 1984-12-01
EP0121466A1 (fr) 1984-10-10
DE3465466D1 (en) 1987-09-24
PL246877A1 (en) 1985-03-26
JPS6323179B2 (ko) 1988-05-16
EP0121466B1 (fr) 1987-08-19
FI841262A0 (fi) 1984-03-29
FI78288B (fi) 1989-03-31
FI841262A (fi) 1984-10-01

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