KR20150030198A - 스크러빙 시스템을 이용한 우레아 과립화 방법 - Google Patents

스크러빙 시스템을 이용한 우레아 과립화 방법 Download PDF

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Publication number
KR20150030198A
KR20150030198A KR1020147034352A KR20147034352A KR20150030198A KR 20150030198 A KR20150030198 A KR 20150030198A KR 1020147034352 A KR1020147034352 A KR 1020147034352A KR 20147034352 A KR20147034352 A KR 20147034352A KR 20150030198 A KR20150030198 A KR 20150030198A
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KR
South Korea
Prior art keywords
stream
ammonia
dust
urea
stage
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KR1020147034352A
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English (en)
Korean (ko)
Inventor
마티아스 포트토프
헤럴드 프란쯔라헤
루크 알베르트 반메르케
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우데 퍼틸라이저 테크널러지 비.브이.
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Application filed by 우데 퍼틸라이저 테크널러지 비.브이. filed Critical 우데 퍼틸라이저 테크널러지 비.브이.
Publication of KR20150030198A publication Critical patent/KR20150030198A/ko
Ceased legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05CNITROGENOUS FERTILISERS
    • C05C9/00Fertilisers containing urea or urea compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34Chemical or biological purification of waste gases
    • B01D53/46Removing components of defined structure
    • B01D53/54Nitrogen compounds
    • B01D53/58Ammonia
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34Chemical or biological purification of waste gases
    • B01D53/73After-treatment of removed components
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05CNITROGENOUS FERTILISERS
    • C05C9/00Fertilisers containing urea or urea compounds
    • C05C9/005Post-treatment
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05CNITROGENOUS FERTILISERS
    • C05C9/00Fertilisers containing urea or urea compounds
    • C05C9/02Fertilisers containing urea or urea compounds containing urea-formaldehyde condensates
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C273/00Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C273/02Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C273/00Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C273/02Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
    • C07C273/14Separation; Purification; Stabilisation; Use of additives
    • C07C273/16Separation; Purification
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2258/00Sources of waste gases
    • B01D2258/02Other waste gases
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/20Air quality improvement or preservation, e.g. vehicle emission control or emission reduction by using catalytic converters

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Environmental & Geological Engineering (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Biomedical Technology (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Treating Waste Gases (AREA)
  • Gas Separation By Absorption (AREA)
  • Fertilizers (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
KR1020147034352A 2012-05-08 2013-05-02 스크러빙 시스템을 이용한 우레아 과립화 방법 Ceased KR20150030198A (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP12003585.2A EP2662349A1 (en) 2012-05-08 2012-05-08 Urea granulation process with scrubbing system
EP12003585.2 2012-05-08
PCT/EP2013/001292 WO2013167245A1 (en) 2012-05-08 2013-05-02 Urea granulation process with scrubbing system

Publications (1)

Publication Number Publication Date
KR20150030198A true KR20150030198A (ko) 2015-03-19

Family

ID=48470891

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020147034352A Ceased KR20150030198A (ko) 2012-05-08 2013-05-02 스크러빙 시스템을 이용한 우레아 과립화 방법

Country Status (12)

Country Link
US (2) US9493407B2 (https=)
EP (2) EP2662349A1 (https=)
JP (1) JP2015522503A (https=)
KR (1) KR20150030198A (https=)
CN (2) CN107459372A (https=)
AR (1) AR090974A1 (https=)
BR (1) BR112014027819A2 (https=)
CA (1) CA2872529A1 (https=)
IN (1) IN2014DN10096A (https=)
MY (1) MY171086A (https=)
RU (1) RU2615811C2 (https=)
WO (1) WO2013167245A1 (https=)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10330654B2 (en) 2014-07-20 2019-06-25 Sabic Global Technologies B.V. Methods for determining low sulfate concentrations in synthetic urea samples, produced in a manufacturing process and containing high levels of impurities
EP3020702A1 (en) * 2014-11-12 2016-05-18 Casale SA Urea finishing process with acid scrubbing
KR101577573B1 (ko) 2014-11-27 2015-12-15 휴켐스주식회사 질산암모늄 제조 공정용 스크러버 시스템
US10519103B2 (en) * 2015-04-01 2019-12-31 Toyo Engineering Corporation Urea production method
WO2018069870A1 (en) * 2016-10-13 2018-04-19 Koch Agronomic Services, Llc Recovery and reuse of components from urea finishing waste streams
ES3028584T3 (en) * 2016-12-28 2025-06-19 Sabic Agri Nutrients Company Solvent recovery from sweep gas streams obtained from a fertilzer coating process
EP3366670A1 (en) * 2017-02-27 2018-08-29 Casale Sa A process and system to capture ammonia from a purge gas of a urea plant
JP6851869B2 (ja) * 2017-03-17 2021-03-31 東洋エンジニアリング株式会社 尿素の造粒方法
CN107715676A (zh) * 2017-10-10 2018-02-23 鲁西化工集团股份有限公司煤化工分公司 一种降低尿素造粒塔尾气氨含量的生产工艺
CN111111407A (zh) * 2019-12-16 2020-05-08 安徽德利来环保科技有限公司 一种车用尿素溶液的生产工艺
US11420937B2 (en) * 2019-12-30 2022-08-23 Stamicarbon B.V. Urea plant with chilled condensation section
WO2021137700A1 (en) 2019-12-30 2021-07-08 Stamicarbon B.V. Ammonia removal from urea finishing
US11332437B2 (en) * 2019-12-30 2022-05-17 Stamicarbon B.V. Urea production with multiple evaporators
PL3848341T3 (pl) * 2020-01-08 2024-06-24 Thyssenkrupp Fertilizer Technology Gmbh Sposób i urządzenie do wytwarzania nawozu
CN111318042A (zh) * 2020-03-03 2020-06-23 中海石油华鹤煤化有限公司 一种生产改性尿素的装置系统及方法
US12103905B2 (en) * 2021-04-07 2024-10-01 Casale Sa Urea production process and plant
CN113101682B (zh) * 2021-05-28 2023-03-24 新疆心连心能源化工有限公司 减少蒸发掉缩合物稳定尿素生产的装置及处理方法
WO2023161232A1 (en) * 2022-02-22 2023-08-31 Tessenderlo Group Nv Methods for the production of nitrogen fertilizer and nitrogen-sulfur fertilizer
AU2023225099A1 (en) * 2022-02-22 2024-08-29 Tessenderlo Group Nv Methods for the production of a solid urea-thiosulfate fertilizer
WO2025244534A1 (en) * 2024-05-23 2025-11-27 Stamicarbon B.V. Technical grade urea granulate
WO2026037775A1 (en) 2024-08-14 2026-02-19 Casale Sa Urea granulation process and method of revamping

Family Cites Families (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA1041484A (en) * 1974-12-20 1978-10-31 Silvio Vargiu Process for the preparation of urea-formaldehyde condensates to be used as fertilizers
US4370198A (en) 1980-03-13 1983-01-25 Mta Muszaki Kemiai Kutato Intezet Method and apparatus for the recovery of the solid material content of solutions and/or suspensions as granules in a gas fluidized bed
NO150667C (no) * 1982-01-07 1984-11-28 Norsk Hydro As Fremgangsmaate for rensing av gassblandinger fra ureaproduksjonsanlegg
DE69412100T2 (de) * 1994-11-18 1999-04-01 Norsk Hydro A/S, Oslo Verfahren zur Herstellung von Harnstoff
NL1002862C2 (nl) 1996-04-15 1997-10-17 Dsm Nv Werkwijze voor het bereiden van granules.
JPH09313860A (ja) 1996-05-27 1997-12-09 Shigeru Saito 湿式同時除害、除塵ガス処理装置及び方法
JP2000001466A (ja) * 1998-06-12 2000-01-07 Toyo Eng Corp 排ガス中の尿素ダスト及びアンモニアの回収・利用方法
JP2000279736A (ja) 1999-03-29 2000-10-10 Toyo Eng Corp 尿素ダスト及びアンモニアを含有する流体の処理装置、それを用いた処理方法及びそれを付設した尿素製造装置
NL1020665C2 (nl) 2002-05-23 2003-11-25 Dsm Nv Werkwijze voor het verwijderen van ammoniak uit een ammoniak-bevattende gasstroom.
DE10346519A1 (de) * 2003-10-02 2005-05-04 Uhde Gmbh Verfahren zur Entfernung von Ammoniak und Staub aus einem Abgas, das bei der Herstellung von Düngemitteln anfällt
CA2598815C (en) * 2005-03-02 2012-06-05 Yara International Asa Pipe reactor and plant for manufacturing of especially urea ammonium sulphate
ITMI20072206A1 (it) * 2007-11-21 2009-05-22 Snam Progetti Metodo per il recupero di ammoniaca da una corrente gassosa in un processo di sintesi di urea
EP2119489A1 (en) * 2008-05-14 2009-11-18 Uhde Fertilizer Technology B.V. Method for reducing aerosol emissions in a urea granulation plant
EP2192099A1 (en) * 2008-11-28 2010-06-02 Uhde Fertilizer Technology B.V. Urea granulation process with an acidic scrubbing system and the subsequent integration of ammonium salt into urea granules
TW201032887A (en) 2009-01-13 2010-09-16 Saipem Spa Process for the recovery of ammonia from a gaseous stream
WO2010106053A2 (en) 2009-03-17 2010-09-23 Bioecon International Holding N.V. Process for converting polysaccharides in an inorganic molten salt hydrate

Also Published As

Publication number Publication date
JP2015522503A (ja) 2015-08-06
CN104321292A (zh) 2015-01-28
CN107459372A (zh) 2017-12-12
WO2013167245A1 (en) 2013-11-14
EP2847144B1 (en) 2018-04-04
BR112014027819A2 (pt) 2017-06-27
CN104321292B (zh) 2017-12-05
US20160376230A1 (en) 2016-12-29
AR090974A1 (es) 2014-12-17
HK1201515A1 (en) 2015-09-04
US9745256B2 (en) 2017-08-29
MY171086A (en) 2019-09-24
CA2872529A1 (en) 2013-11-14
RU2615811C2 (ru) 2017-04-11
US20150133689A1 (en) 2015-05-14
EP2662349A1 (en) 2013-11-13
US9493407B2 (en) 2016-11-15
EP2847144A1 (en) 2015-03-18
IN2014DN10096A (https=) 2015-08-21
RU2014146274A (ru) 2016-06-27

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