CN104321292B - 具有洗涤系统的尿素造粒工艺 - Google Patents

具有洗涤系统的尿素造粒工艺 Download PDF

Info

Publication number
CN104321292B
CN104321292B CN201380024430.0A CN201380024430A CN104321292B CN 104321292 B CN104321292 B CN 104321292B CN 201380024430 A CN201380024430 A CN 201380024430A CN 104321292 B CN104321292 B CN 104321292B
Authority
CN
China
Prior art keywords
stream
urea
dust
ammonia
process according
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201380024430.0A
Other languages
English (en)
Chinese (zh)
Other versions
CN104321292A (zh
Inventor
M·波特霍夫
H·弗伦茨若哈
L·A·万马克
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Uhde Fertilizer Technology BV
Original Assignee
Uhde Fertilizer Technology BV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=48470891&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=CN104321292(B) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Uhde Fertilizer Technology BV filed Critical Uhde Fertilizer Technology BV
Priority to CN201710685089.3A priority Critical patent/CN107459372A/zh
Publication of CN104321292A publication Critical patent/CN104321292A/zh
Application granted granted Critical
Publication of CN104321292B publication Critical patent/CN104321292B/zh
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05C—NITROGENOUS FERTILISERS
    • C05C9/00—Fertilisers containing urea or urea compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/46—Removing components of defined structure
    • B01D53/54—Nitrogen compounds
    • B01D53/58—Ammonia
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/73—After-treatment of removed components
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05C—NITROGENOUS FERTILISERS
    • C05C9/00—Fertilisers containing urea or urea compounds
    • C05C9/005—Post-treatment
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05C—NITROGENOUS FERTILISERS
    • C05C9/00—Fertilisers containing urea or urea compounds
    • C05C9/02—Fertilisers containing urea or urea compounds containing urea-formaldehyde condensates
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C273/02—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C273/02—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
    • C07C273/14—Separation; Purification; Stabilisation; Use of additives
    • C07C273/16—Separation; Purification
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2258/00—Sources of waste gases
    • B01D2258/02—Other waste gases
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/20—Air quality improvement or preservation, e.g. vehicle emission control or emission reduction by using catalytic converters

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Environmental & Geological Engineering (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Health & Medical Sciences (AREA)
  • Biomedical Technology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Treating Waste Gases (AREA)
  • Gas Separation By Absorption (AREA)
  • Fertilizers (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
CN201380024430.0A 2012-05-08 2013-05-02 具有洗涤系统的尿素造粒工艺 Expired - Fee Related CN104321292B (zh)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710685089.3A CN107459372A (zh) 2012-05-08 2013-05-02 具有洗涤系统的尿素造粒工艺

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP12003585.2A EP2662349A1 (en) 2012-05-08 2012-05-08 Urea granulation process with scrubbing system
EP12003585.2 2012-05-08
PCT/EP2013/001292 WO2013167245A1 (en) 2012-05-08 2013-05-02 Urea granulation process with scrubbing system

Related Child Applications (1)

Application Number Title Priority Date Filing Date
CN201710685089.3A Division CN107459372A (zh) 2012-05-08 2013-05-02 具有洗涤系统的尿素造粒工艺

Publications (2)

Publication Number Publication Date
CN104321292A CN104321292A (zh) 2015-01-28
CN104321292B true CN104321292B (zh) 2017-12-05

Family

ID=48470891

Family Applications (2)

Application Number Title Priority Date Filing Date
CN201380024430.0A Expired - Fee Related CN104321292B (zh) 2012-05-08 2013-05-02 具有洗涤系统的尿素造粒工艺
CN201710685089.3A Pending CN107459372A (zh) 2012-05-08 2013-05-02 具有洗涤系统的尿素造粒工艺

Family Applications After (1)

Application Number Title Priority Date Filing Date
CN201710685089.3A Pending CN107459372A (zh) 2012-05-08 2013-05-02 具有洗涤系统的尿素造粒工艺

Country Status (12)

Country Link
US (2) US9493407B2 (https=)
EP (2) EP2662349A1 (https=)
JP (1) JP2015522503A (https=)
KR (1) KR20150030198A (https=)
CN (2) CN104321292B (https=)
AR (1) AR090974A1 (https=)
BR (1) BR112014027819A2 (https=)
CA (1) CA2872529A1 (https=)
IN (1) IN2014DN10096A (https=)
MY (1) MY171086A (https=)
RU (1) RU2615811C2 (https=)
WO (1) WO2013167245A1 (https=)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2016012925A1 (en) * 2014-07-20 2016-01-28 Sabic Global Technologies B.V. Methods for determining low sulfate concentrations in synthetic urea samples, produced in a manufacturing process and containing high levels of impurities
EP3020702A1 (en) * 2014-11-12 2016-05-18 Casale SA Urea finishing process with acid scrubbing
KR101577573B1 (ko) 2014-11-27 2015-12-15 휴켐스주식회사 질산암모늄 제조 공정용 스크러버 시스템
JPWO2016159336A1 (ja) * 2015-04-01 2018-02-01 東洋エンジニアリング株式会社 尿素製造方法
BR112019007135A2 (pt) * 2016-10-13 2019-07-02 Koch Agronomic Services Llc recuperação e reutilização de componentes dos fluxos de resíduos de acabamento de ureia
ES3028584T3 (en) 2016-12-28 2025-06-19 Sabic Agri Nutrients Company Solvent recovery from sweep gas streams obtained from a fertilzer coating process
EP3366670A1 (en) * 2017-02-27 2018-08-29 Casale Sa A process and system to capture ammonia from a purge gas of a urea plant
JP6851869B2 (ja) * 2017-03-17 2021-03-31 東洋エンジニアリング株式会社 尿素の造粒方法
CN107715676A (zh) * 2017-10-10 2018-02-23 鲁西化工集团股份有限公司煤化工分公司 一种降低尿素造粒塔尾气氨含量的生产工艺
CN111111407A (zh) * 2019-12-16 2020-05-08 安徽德利来环保科技有限公司 一种车用尿素溶液的生产工艺
US11420937B2 (en) * 2019-12-30 2022-08-23 Stamicarbon B.V. Urea plant with chilled condensation section
US11912649B2 (en) 2019-12-30 2024-02-27 Stamicarbon B.V. Ammonia removal from urea finishing
AU2020416567B2 (en) * 2019-12-30 2023-06-15 Stamicarbon B.V. Urea production with multiple evaporators
PL3848341T3 (pl) * 2020-01-08 2024-06-24 Thyssenkrupp Fertilizer Technology Gmbh Sposób i urządzenie do wytwarzania nawozu
CN111318042A (zh) * 2020-03-03 2020-06-23 中海石油华鹤煤化有限公司 一种生产改性尿素的装置系统及方法
EP4320095B1 (en) * 2021-04-07 2025-01-22 Casale Sa Urea production process and plant
CN113101682B (zh) * 2021-05-28 2023-03-24 新疆心连心能源化工有限公司 减少蒸发掉缩合物稳定尿素生产的装置及处理方法
CA3244835A1 (en) * 2022-02-22 2023-08-31 Tessenderlo Group Nv PROCESS FOR THE PRODUCTION OF NITROGEN AND NITROGEN-SULFUR FERTILIZERS
CA3244902A1 (en) * 2022-02-22 2023-08-31 Tessenderlo Group Nv PROCESSES FOR PRODUCING A SOLID UREA-THIOSULFATE BASED FERTILIZER
WO2025244534A1 (en) * 2024-05-23 2025-11-27 Stamicarbon B.V. Technical grade urea granulate
WO2026037775A1 (en) 2024-08-14 2026-02-19 Casale Sa Urea granulation process and method of revamping

Family Cites Families (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA1041484A (en) * 1974-12-20 1978-10-31 Silvio Vargiu Process for the preparation of urea-formaldehyde condensates to be used as fertilizers
US4370198A (en) 1980-03-13 1983-01-25 Mta Muszaki Kemiai Kutato Intezet Method and apparatus for the recovery of the solid material content of solutions and/or suspensions as granules in a gas fluidized bed
NO150667C (no) * 1982-01-07 1984-11-28 Norsk Hydro As Fremgangsmaate for rensing av gassblandinger fra ureaproduksjonsanlegg
ES2119071T3 (es) 1994-11-18 1998-10-01 Norsk Hydro As Procedimiento para preparar urea.
NL1002862C2 (nl) 1996-04-15 1997-10-17 Dsm Nv Werkwijze voor het bereiden van granules.
JPH09313860A (ja) 1996-05-27 1997-12-09 Shigeru Saito 湿式同時除害、除塵ガス処理装置及び方法
JP2000001466A (ja) * 1998-06-12 2000-01-07 Toyo Eng Corp 排ガス中の尿素ダスト及びアンモニアの回収・利用方法
JP2000279736A (ja) 1999-03-29 2000-10-10 Toyo Eng Corp 尿素ダスト及びアンモニアを含有する流体の処理装置、それを用いた処理方法及びそれを付設した尿素製造装置
NL1020665C2 (nl) 2002-05-23 2003-11-25 Dsm Nv Werkwijze voor het verwijderen van ammoniak uit een ammoniak-bevattende gasstroom.
DE10346519A1 (de) 2003-10-02 2005-05-04 Uhde Gmbh Verfahren zur Entfernung von Ammoniak und Staub aus einem Abgas, das bei der Herstellung von Düngemitteln anfällt
PL1861335T3 (pl) * 2005-03-02 2013-06-28 Yara Int Asa Reaktor rurowy i instalacja do wytwarzania zwłaszcza siarczanu mocznikowo-amonowego
ITMI20072206A1 (it) 2007-11-21 2009-05-22 Snam Progetti Metodo per il recupero di ammoniaca da una corrente gassosa in un processo di sintesi di urea
EP2119489A1 (en) * 2008-05-14 2009-11-18 Uhde Fertilizer Technology B.V. Method for reducing aerosol emissions in a urea granulation plant
EP2192099A1 (en) * 2008-11-28 2010-06-02 Uhde Fertilizer Technology B.V. Urea granulation process with an acidic scrubbing system and the subsequent integration of ammonium salt into urea granules
TW201032887A (en) 2009-01-13 2010-09-16 Saipem Spa Process for the recovery of ammonia from a gaseous stream
EP2408781B1 (en) 2009-03-17 2013-09-25 BIOeCON International Holding N.V. Process for converting polysaccharides in an inorganic molten salt hydrate

Also Published As

Publication number Publication date
HK1201515A1 (en) 2015-09-04
JP2015522503A (ja) 2015-08-06
EP2662349A1 (en) 2013-11-13
US9493407B2 (en) 2016-11-15
CN107459372A (zh) 2017-12-12
AR090974A1 (es) 2014-12-17
EP2847144A1 (en) 2015-03-18
BR112014027819A2 (pt) 2017-06-27
EP2847144B1 (en) 2018-04-04
WO2013167245A1 (en) 2013-11-14
IN2014DN10096A (https=) 2015-08-21
US9745256B2 (en) 2017-08-29
CA2872529A1 (en) 2013-11-14
US20150133689A1 (en) 2015-05-14
CN104321292A (zh) 2015-01-28
MY171086A (en) 2019-09-24
US20160376230A1 (en) 2016-12-29
RU2014146274A (ru) 2016-06-27
KR20150030198A (ko) 2015-03-19
RU2615811C2 (ru) 2017-04-11

Similar Documents

Publication Publication Date Title
CN104321292B (zh) 具有洗涤系统的尿素造粒工艺
CN102227392B (zh) 使用酸洗涤系统的尿素成粒过程和氨盐到尿素颗粒中的相应集成
CN107001248B (zh) 酸洗涤尿素精整加工方法
JP7277672B2 (ja) 尿素仕上げからのアンモニア除去
CN102596901A (zh) 从废气中去除尿素和氨的方法
EP2386346A1 (en) Process for the reduction of ammonia emissions in a urea manufacturing process
CN114870599A (zh) 一种氨法脱碳系统生产碳酸氢铵的方法及装置
CN101862584B (zh) 硝铵废水与烟道气综合治理工艺
HK1201515B (en) Urea granulation process with scrubbing system
SA515360667B1 (ar) طريقة لتقليل الاعتام بالغبار المرئي المنفصل في اتجاه الريح
OA17151A (en) Urea granulation process with scrubbing system
HK1159063B (en) Urea granulation process with an acidic scrubbing system and the subsequent integration of ammonium salt into urea granules
HK1159063A (en) Urea granulation process with an acidic scrubbing system and the subsequent integration of ammonium salt into urea granules
JP7538382B2 (ja) 尿素造粒物の製造方法及び製造プラント
KR20250013083A (ko) 암모니아 기반 탈탄소화 시스템에서 중탄산암모늄을 제조하기 위한 방법 및 장치
EA051782B1 (ru) Способы получения азотного удобрения и азотно-серного удобрения
EA043041B1 (ru) Удаление аммиака из доводочной секции карбамида
EA042818B1 (ru) Производство карбамида с применением множества испарителей

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
REG Reference to a national code

Ref country code: HK

Ref legal event code: DE

Ref document number: 1201515

Country of ref document: HK

GR01 Patent grant
GR01 Patent grant
REG Reference to a national code

Ref country code: HK

Ref legal event code: GR

Ref document number: 1201515

Country of ref document: HK

CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20171205

Termination date: 20200502