KR20080069953A - A manure for preventing or treating clubroot using a by-product of tabacco and manufacturing method the same - Google Patents

A manure for preventing or treating clubroot using a by-product of tabacco and manufacturing method the same Download PDF

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KR20080069953A
KR20080069953A KR1020080066685A KR20080066685A KR20080069953A KR 20080069953 A KR20080069953 A KR 20080069953A KR 1020080066685 A KR1020080066685 A KR 1020080066685A KR 20080066685 A KR20080066685 A KR 20080066685A KR 20080069953 A KR20080069953 A KR 20080069953A
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weight
parts
fertilizer
mixture
root
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KR1020080066685A
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김진철
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김진철
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F11/00Other organic fertilisers
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G1/00Mixtures of fertilisers belonging individually to different subclasses of C05

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Fertilizers (AREA)

Abstract

An eco-friendly fertilizer which prevents or treats clubroot and a preparation method thereof are provided to create consumption of tobacco byproduct, to reduce the amount of agrichemicals in the control of clubroot and to facilitate eco-friendly farming by employing waste tobacco byproduct. An eco-friendly liquid fertilizer which prevents or treats clubroot is prepared by mixing 20-30 parts by weight of ethyl alcohol, 80-85 parts by weight of water and 40-45 parts by weight of complex fertilizer to 100 parts by weight of tobacco byproduct to form a mixture which is extracted and concentrated. The complex fertilizer comprises at least two selected from nitrogen, phosphate or potassium fertilizer ingredients and at least two selected from boron, manganese, iron, zinc, copper, molybdenum, magnesia and calcium. A preparation method of the liquid fertilizer comprises steps of: putting a mixture comprising 20-30 parts by weight of ethyl alcohol, 80-85 parts by weight of water and 40-45 parts by weight of complex fertilizer which are added to 100 parts by weight of tobacco byproduct in a heating tank; heating the tank at 95-100deg.C while stirring; and concentrating the mixture until the volume of the mixture reaches 27-35% with respect to the initial volume of the mixture. An eco-friendly granular fertilizer which prevents or treats clubroot is prepared by mixing 15-25 parts by weight of calcium hydroxide, 10-15 parts by weight of humic acid, 22-28 parts by weight of water and 4-10 parts by weight of microorganism in 100 parts by weight of tobacco byproduct, followed by forming granules with the mixture. A manufacturing method of the granular fertilizer comprises steps of: preparing a mixture comprising 15-25 parts by weight of calcium hydroxide, 10-15 parts by weight of humic acid, 22-28 parts by weight of water in 100 parts by weight of tobacco byproduct; forming granules having a size of 1-5mm by subjecting the mixture to a pelletizer; and mixing the mixture and microorganism in a ratio of 95-98:2-5, then drying the obtained mixture.

Description

담배부산물을 이용한 뿌리혹병 예방 또는 치료용 비료 및 그 제조방법{A Manure for preventing or treating Clubroot using A by-product of tabacco and manufacturing method the same}A manure for preventing or treating clubroot using a by-product of tabacco and manufacturing method the same}

본 발명은 담배부산물을 이용한 배추 뿌리혹병에 효과적인 비료 및 그 제조방법에 관한 것으로서 보다 상세하게는 배추 뿌리혹병 예방치료 효과가 우수함과 동시에 친환경적이므로 배추재배에 약해 염려 없이 뿌리혹병을 예방 및 치료할 수 있는 비료 및 그 제조방법에 관한 것이다.The present invention relates to an effective fertilizer for cabbage root gall disease using tobacco by-products and a method of manufacturing the same. More specifically, the cabbage root gall disease prevention effect is excellent and environmentally friendly, so it can prevent and treat root gall disease without concern about weak cabbage cultivation. It relates to a fertilizer and a method for producing the same.

무사마귀병으로 알려진 뿌리혹병은 원생동물계의 뿌리혹균문에 속하는 절대기생균의해 발뱅되는 토양전염병으로 무, 배추, 양배추, 순무 등 십자화과 채소의 뿌리에 주로 발생하여 처음 작은 혹이나 뿌리가 비대되어 나타나고, 진전되면 지하부 전체가 큰 혹으로 형성된다. 뿌리혹병이 걸린 채소는 잔뿌리가 없어 양분과 수분의 흡수가 부족하여 왜소해지고, 시드는 증상이 나타나며, 시드는 일을 반복하다 결국 채소를 말라 죽게한다.Root gall disease, also known as wart disease, is a soil infectious disease caused by the absolute parasites belonging to the protozoa's root nodule. It occurs mainly in the roots of cruciferous vegetables such as radish, cabbage, cabbage, and turnip. The entire basement is formed by large humps. Root gall diseased vegetables have no roots, lack of absorption of nutrients and water, dwarf, wither, symptomatic, and wilted.

이러한 뿌리혹병은 배추, 무, 양배추를 재배하는 농가에 막대한 피해를 끼치나 뿌리혹병의 병원균은 휴면포자, 유주자, 변형체 등의 형태로 토양 내에 존재하여 그 퇴치가 어려우며 토양중에 존재하는 병원균의 휴면포자는 기주식물 없이 수년간 생존할 수 있고, 빗물, 관개수, 흙바람, 농기구등에 의해서 멀리까지 전파될 수 있다. These root gall diseases cause enormous damage to farmers growing cabbage, radish, and cabbage, but the pathogens of root gall disease are dormant spores, fertilizers, and transformants, which exist in the soil, making it difficult to combat the dormant spores of pathogens present in the soil. Can survive for many years without host plants, and can be spread far away by rainwater, irrigation, earth breezes and farming equipment.

상기와 같은 농가에 막대한 피해를 끼치는 뿌리혹병을 방제하기 위해 종래에는 주로 농약을 사용하는 화학적 방제법인 유묘검정법이 이용되고 있으나, 방제율이 낮고 농약의 과도한 사용으로 인한 주변환경을 오염에 발생시키는 문제점이 있었다.Conventionally, the seedling assay, which is a chemical control method that mainly uses pesticides, is used to control root-knot diseases, which cause enormous damage to farms as described above. However, the control rate is low and problems causing pollution to the surrounding environment due to excessive use of pesticides. There was this.

최근에는 상기와 같은 문제점을 해결하기 위해 뿌리혹병에 저항력이 뛰어난 품종이 육성개발되고 있으나, 육성비용이 많이 들고, 육성에 많은 시간이 소요되며 뿌리혹병의 병원균의 변이로 그 실효성이 확실치 않아 뿌리혹병의 근본적인 해결책이 되지 못하는 실정이다.Recently, a variety of varieties that are resistant to root-knock disease have been developed and developed in order to solve the above problems, but it is expensive to grow, it takes a lot of time to grow, and its effect is not certain due to the variation of the pathogen of root-knock disease. This is not a fundamental solution of the situation.

본 발명은 상기와 같은 문제점을 해결하기 위해 발명된 것으로 폐기되는 담배부산물을 이용하여 뿌리혹병을 효과적으로 예방하고 치료할 수 있는 비료를 제공하는 것을 목적으로 한다.It is an object of the present invention to provide a fertilizer that can effectively prevent and treat root-knot disease using tobacco by-products discarded as invented to solve the above problems.

또한, 상기 뿌리혹병 예방 또는 치료용 비료의 제조방법 및 사용방법을 제공하는 것을 목적으로 한다.In addition, an object of the present invention is to provide a method of producing and using the fertilizer for the prevention or treatment of root root disease.

본 발명은 담배부산물을 이용한 뿌리혹병 예방 또는 치료용 액상 비료로 담배부산물 100중량부에 에틸알코올 20~30중량부, 물 80~85중량부, 복합비료 40~45중량부를 첨가하여 추출·농축하여 제조되는 것을 특징으로 한다.The present invention is a liquid fertilizer for the prevention or treatment of root gall disease using tobacco by-products 20 to 30 parts by weight of ethyl alcohol, 80 to 85 parts by weight of water, 40 to 45 parts by weight of complex fertilizer by extraction and concentration It is characterized by being manufactured.

또한, 담배부산물 100중량부에 에틸알코올 20~30중량부, 물 80~85중량부, 복합비료 40~45중량부를 혼합한 혼합물을 가열탱크에 투입하는 단계; 상기 가열탱크를 95~100℃로 가열·교반하는 단계; 상기 혼합물이 최초 혼합물의 부피의 27~35%가 될 때까지 농축하는 단계를 포함하여 제조되는 것을 특징으로 한다.In addition, the step of adding a mixture of 20 to 30 parts by weight of ethyl alcohol, 80 to 85 parts by weight of water, 40 to 45 parts by weight of complex fertilizers in a heating tank; Heating and stirring the heating tank at 95˜100 ° C .; The mixture is characterized in that it comprises the step of concentration until it is 27 to 35% of the volume of the original mixture.

또한, 본 발명은 담배부산물을 이용한 뿌리혹병 예방 또는 치료용 입상 비료로 담배부산물 100중량부에 수산화칼슘 15~25중량부, 부식산 10~15중량부, 물 22~28중량부, 미생물 4~10중량부를 첨가·혼합하고 입상형태로 제조되는 것을 특징으로 한다.In addition, the present invention is a granular fertilizer for the prevention or treatment of root gall disease using tobacco byproducts 15 to 25 parts by weight of calcium hydroxide, 10 to 15 parts by weight of humic acid, 22 to 28 parts by weight of water, microorganisms 4 to 10 parts by weight of tobacco byproducts It is characterized by the addition and mixing of the parts by weight to produce a granular form.

또한, 담배부산물 100중량부에 수산화칼슘 15~25중량부, 부식산 10~15중량부, 물 22~28중량부를 첨가하여 혼합한 혼합물을 제조하는 단계; 상기 혼합물을 펠렛기계를 이용하여 1~5㎜크기의 입상형태로 제조하는 단계; 상기 입상형태로 제조된 혼합물에 미생물을 중량비 95~98 대 2~5으로 혼합·건조하는 단계를 포함하여 제조되는 것을 특징으로 한다.In addition, preparing a mixture by adding 15 to 25 parts by weight of calcium hydroxide, 10 to 15 parts by weight of humic acid, 22 to 28 parts by weight of water to 100 parts by weight of tobacco byproducts; Preparing the mixture into granules having a size of 1 to 5 mm using a pellet machine; Mixing and drying the microorganisms in a weight ratio of 95 to 98 to 2 to 5 prepared in the granular form is characterized in that it is prepared.

또한 상기의 액상 비료 또는 입상 비료를 정식(定植)전 토양에 공급하는 사용방법을 특징으로 한다.It is also characterized by a method of supplying the above liquid fertilizer or granular fertilizer to the soil before planting.

본 발명은 담배부산물을 뿌리혹병의 예방과 치료에 친환경적으로 사용할 수 있도록 담배부산물을 이용한 액상 및 입상 비료를 제공함으로서, 연초제조창에서 발생하는 담배부산물을 효과적으로 처리할 수 있고 농민의 배추재배에 치명적인 뿌리혹병을 농약사용을 줄이고도 방제가 가능하므로 유기농 또는 친환경 농업을 할 수 있어 국민의 건강과 친환경 농업발전에 이바지 할 수 있는 유용한 발명인 것이다.The present invention provides liquid and granular fertilizers using tobacco by-products so that tobacco by-products can be used in the prevention and treatment of root-knot disease, and can effectively process tobacco by-products generated in tobacco production window and are deadly to farmers' cabbage cultivation. It is a useful invention that can contribute to the health of people and the development of eco-friendly agriculture because organic or eco-friendly farming is possible because the disease can be controlled even by reducing the use of pesticides.

본 발명은 담배 제조를 위한 담배 잎이 수거된 후 버려지는 담배의 주맥, 잎줄기, 각초 부스러기 등의 담배부산물을 이용하여 배추 뿌리혹병을 예방 및 치료할 수 있는 친환경적인 비료 및 그 제조방법에 관한 것이다. The present invention relates to an environmentally friendly fertilizer capable of preventing and treating Chinese cabbage root gall disease by using tobacco by-products, such as the stem of the tobacco, leaf stem, vinegar debris after the tobacco leaves are collected for tobacco production. .

이하, 본 발명의 뿌리혹병 예방 또는 치료용 비료에 대해 바람직한 실시예를 통해 상세히 설명한다.Hereinafter, the preferred embodiment of the fertilizer for preventing or treating root gall disease of the present invention will be described in detail.

담배에는 약 10종의 알칼로이드(alkaloid)가 함유되어 있는데, 니코틴(nicotine; C16H14N2)이 95%로서 대부분을 차지하고 있으며, 5% 이하의 노르니코틴(nornicontine; C9H14N2)과 극미량의 아나바신(anabasine; C10H14N2)이 함유되어 있다. Cigarettes contain about 10 alkaloids, with nicotine (C16H14N2) accounting for 95% of the total, with less than 5% nornicontine (C9H14N2) and trace amounts of anabasine (C10H14N2). ) Is contained.

니코틴은 강력한 살충효과를 가진 것으로 알려져 있어 황산니코틴, 연초분말 등의 제품이 살충제로 사용되고 있고, 현재 합성 니코틴 계 살충제가 개발되어 사용되고 있다. 본 발명은 담배에 가장 많이 함유된 니코틴의 강한 살충효과를 이용한 것이다. Nicotine is known to have a strong insecticidal effect, so products such as nicotine sulfate and tobacco powder are used as insecticides, and synthetic nicotine insecticides have been developed and used. The present invention utilizes the strong insecticidal effect of nicotine contained most in tobacco.

본 발명은 담배부산물을 이용하여 뿌리혹병을 예방 또는 치료할 수 있는 비료에 관한 것으로 본 발명에 따른 담배부산물을 이용한 뿌리혹병 예방 또는 치료용 비료는 액상(液狀) 또는 알갱이 형태의 입상(粒狀)으로 제조될 수 있다.The present invention relates to a fertilizer capable of preventing or treating root gall disease using tobacco by-products. The fertilizer for preventing or treating root gall disease using tobacco by-products according to the present invention is granular in the form of liquid or granules. It can be prepared as.

본 발명에 따른 뿌리혹병 예방 또는 치료용 액상 비료는 담배부산물 100중량부에 에틸알코올 20~30중량부, 물 80~85중량부, 복합비료 40~45중량부를 첨가하여 추출·농축하여 제조한다.The liquid fertilizer for preventing or treating root gall disease according to the present invention is prepared by extracting and concentrating by adding 20-30 parts by weight of ethyl alcohol, 80-85 parts by weight of water, and 40-45 parts by weight of complex fertilizer to 100 parts by weight of tobacco byproducts.

본 발명에 사용되는 담배부산물은 농가나 연초제조창에서 버려지는 담배의 주맥, 잎줄기, 각초 부스러기 등을 분쇄하여 분말형태로 제조하여 사용한다.Tobacco by-products used in the present invention are used in the form of powder by grinding the stem, leaf stem, vinegar shavings, etc. of tobacco discarded in farms or tobacco production windows.

상기 복합비료는 질소, 인산, 칼륨의 비료성분 중 선택되는 2종 이상을 함유하고 붕소, 망간, 철, 아연, 구리, 몰리브덴, 고토, 칼슘 중 선택되는 2종 이상 함유하는 것을 사용하는 것이 바람직할 것이다.The compound fertilizer contains at least two kinds selected from fertilizer components of nitrogen, phosphoric acid and potassium, and at least two kinds selected from boron, manganese, iron, zinc, copper, molybdenum, goto, and calcium may be used. will be.

본 발명에 따른 뿌리혹병 예방 또는 치료용 액상 비료는 담배부산물 100중량부에 에틸알코올 20~30중량부, 물 80~85중량부, 제4종 복합비료 40~45중량부를 혼합한 혼합물을 가열탱크에 투입하는 단계; 상기 가열탱크를 95~100℃로 가열·교반하는 단계; 상기 혼합물이 최초 혼합물의 부피의 27~35%가 될 때까지 농축하는 단계로 제조된다.Liquid fertilizer for preventing or treating root-knot disease according to the present invention is a heating tank of a mixture of 20 to 30 parts by weight of ethyl alcohol, 80 to 85 parts by weight of water, and 40 to 45 parts by weight of the fourth compound fertilizer in 100 parts by weight of tobacco byproducts. Putting in; Heating and stirring the heating tank at 95˜100 ° C .; The mixture is prepared by concentrating until it reaches 27-35% of the volume of the original mixture.

상기 혼합물은 물과 에틸알코올을 먼저 혼합하고 담배부산물을 조금씩 투입하여 혼합하는 것이 바람직하다.The mixture is preferably mixed with water and ethyl alcohol first and then by adding a little by-product tobacco.

본 발명에 따른 뿌리혹병 예방 또는 치료용 입상 비료는 담배부산물 100중량부에 수산화칼슘 15~25중량부, 부식산 10~15중량부, 물 22~28중량부, 미생물 4~10중량부를 첨가하고 혼합한 후, 펠렛기를 이용하여 입상형태로 제조된다.The granular fertilizer for preventing or treating root gall disease according to the present invention is added to 100 parts by weight of tobacco byproducts and added with 15 to 25 parts by weight of calcium hydroxide, 10 to 15 parts by weight of humic acid, 22 to 28 parts by weight of water, and 4 to 10 parts by weight of microorganisms. After that, it is produced in a granular form using a pellet machine.

상기 수산화칼슘은 석회질 비료로 식물에 칼슘을 공급한다.The calcium hydroxide is a calcium fertilizer to supply the calcium to the plant.

상기 부식산은 한랭한 늪지에 오랜동안 퇴적된 식물이 긴 세월에 걸쳐 분해,중합되어 만들어진 천연적으로 부식된 물질로 토양의 물리적,화학적 구조 및 식물성장환경 개선에 탁월한 효능이 있으며 토양속에 들어있는 식물 영양소를 추출하여 작물에 공급하는 작용을 하고, 가축의 생장에 도움이 되며,토양,수질의 개선과 폐기물처리에도 효능이 있다 The humic acid is a naturally corroded material produced by decomposition and polymerization of plants that have been deposited for a long time in a cold swamp, and have excellent effects on improving the physical and chemical structure of the soil and the growth environment of plants. Extracts and supplies nutrients to crops, helps to grow livestock, and improves soil, water quality and waste disposal

상기 미생물은 토양의 유효미생물로 식물에게 중요한 아미노산, 저분자핵산, 비타민, 호르몬 등을 분비하여 식물의 뿌리에 직, 간접적으로 흡수시켜 식물을 건전하게 생육되도록 하여 수확율을 높여주고 수확물의 맛, 색, 향기, 저장성 증대 등 품질향상과 양분함량 증대에도 크게 기여한다.The microorganisms are effective microorganisms in the soil, secreting amino acids, low molecular weight nucleic acids, vitamins, hormones, etc., which are important to plants, and absorbing them directly or indirectly into the roots of plants. It also contributes greatly to the improvement of quality and nutrient content such as increased flavor, fragrance and shelf life.

본 발명에 사용되는 미생물은 광합성세균, 바실러스, 유산균 및 효모균 중 선택되는 2종이상의 혼합균주를 사용하는 것이 바람직할 것이다.As the microorganism used in the present invention, it will be preferable to use two or more kinds of mixed strains selected from photosynthetic bacteria, Bacillus, lactic acid bacteria and yeast.

상기 본 발명의 담배부산물을 이용한 뿌리혹병 예방 또는 치료용 입상 비료는 담배부산물 100중량부에 수산화칼슘 15~25중량부, 부식산 10~15중량부, 물 22~28중량부를 첨가하여 혼합한 혼합물을 제조하는 단계; 상기 혼합물을 펠렛기계를 이용하여 1~5㎜크기의 입상형태로 제조하는 단계; 상기 입상형태로 제조된 혼합물에 미생물을 중량비 95~98 대 2~5으로 혼합·건조하는 단계로 제조된다.The granular fertilizer for preventing or treating root gall disease using the tobacco byproduct of the present invention is a mixture of 15 to 25 parts by weight of calcium hydroxide, 10 to 15 parts by weight of humic acid, and 22 to 28 parts by weight of water to 100 parts by weight of tobacco byproducts. Manufacturing; Preparing the mixture into granules having a size of 1 to 5 mm using a pellet machine; Mixing and drying the microorganisms in a weight ratio of 95 to 98 to 2 to 5 prepared in the granular form.

상기 혼합물은 담배부산물, 수산화칼슘, 부식산을 먼저 1차 혼합하고 물을 가하여 2차 혼합하는 것이 바람직할 것이다. The mixture may be preferably mixed firstly with tobacco by-products, calcium hydroxide and humic acid, followed by addition of water.

본 발명에 따른 담배부산물을 이용한 뿌리혹병 예방 또는 치료용 액상 및 입상 비료는 단독으로 사용할 수 있으나, 붕소, 구리, 철, 망간, 몰리브덴, 아연 등의 성분 중 2종 이상을 혼합하여 제조되는 미량요소 복합비료나 어박, 골분, 잠용유박, 대두박, 채종유박 등 기타식물성유박, 미강유박, 혼합유박, 계분가공비료, 혼합유기질비료, 증제피혁분, 맥주오니등의 유기질비료나, 그린퇴비, 퇴비, 부숙겨, 재, 분뇨잔사, 부엽토, 아미노산발효 부산비료, 부산동물질비료, 가축분뇨발효 비료, 건계분, 부숙왕겨 또는 부숙톱밥, 건조축산 페기물, 토양미생물제제 및 토양활성제제비료등의 부산물비료를 같은 친환경 비료를 같이 사용하여 농작물의 작황을 더욱더 좋게 할 수 있다.Liquid and granular fertilizer for preventing or treating root gall disease using tobacco by-products according to the present invention may be used alone, but trace elements prepared by mixing two or more kinds of components such as boron, copper, iron, manganese, molybdenum, and zinc Organic fertilizers such as compound fertilizers, fish meal, bone meal, sleepable oil meal, soybean meal, rapeseed oil and other vegetable oils, rice bran oil, mixed oil meal, manure processing fertilizer, mixed organic fertilizer, thickened leather powder, beer sludge, green compost, compost, By-product fertilizers, such as boiled bran, ash, manure residue, foliar soil, amino acid fermentation by-product fertilizer, Busan fertilizer, livestock manure fermentation fertilizer, dry powder, cooked rice husk or cooked sawdust, dry livestock waste, soil microbial agent and soil activator fertilizer The same environmentally friendly fertilizers can be used together to produce better crops.

또한, 본 발명에 따른 담배부산물을 이용한 뿌리혹병 예방 또는 치료용 비료는 농작물의 재배시에 토양에 공급하는 것보다 정식(定植)전에 토양에 공급하여 토양 내에 존재하는 뿌리혹병의 병원균을 사멸시키고 정식(定植)하여 재배하는 것이 뿌리혹병의 예방 및 치료에 더 이로울 것이다.In addition, the fertilizer for the prevention or treatment of root gall disease using tobacco by-products according to the present invention, rather than feeding to the soil during the cultivation of crops, is supplied to the soil before the formula (을) to kill the pathogens of root gall disease present in the soil and form Cultivation by cultivation will be more beneficial for the prevention and treatment of root gall disease.

이하 실시예를 들어 본 발명을 더욱 상세히 설명하나, 이들 실시예는 어디까지나 본 발명의 이해를 돕기 위해 제시되는 예시적 구체예에 불과할 뿐, 본 발명의 보호범위가 이들 실시예로 한정되는 것은 아니다.Hereinafter, the present invention will be described in more detail with reference to the following examples, but these examples are merely exemplary embodiments presented to aid the understanding of the present invention, but the protection scope of the present invention is not limited to these examples. .

1. 본 발명에 따른 담배부산물을 이용한 뿌리혹병 예방 또는 치료용 액상 비료 제조 및 효능실험1. Preparation and efficacy test of liquid fertilizer for the prevention or treatment of root gall disease using tobacco by-product according to the present invention

1) 액상 비료 제조 및 함량분석1) Liquid Fertilizer Preparation and Content Analysis

원재료명 Raw material name 혼합 비율 (kg)Mix ratio (kg) 담배 부산물Tobacco by-products 2.002.00 에틸알코올Ethyl alcohol 0.500.50 water 1.801.80 복합비료Compound fertilizer 0.900.90

상기 표 1에 따라 각 원료를 계량하고 혼합하여 혼합물을 제조하였다.According to Table 1, each raw material was weighed and mixed to prepare a mixture.

상기 혼합물을 2중 가열탱크에 투입하여 교반하면서 가열하여 100℃를 유지하며 12시간 추출한 후 계속 가열하여 혼합물의 최초 부피의 1/3정도 까지 농축하여 여과한 후 미량요소 또는 비료성분을 첨가하여 시료 1 액상 비료를 제조하였다.The mixture was added to a double heating tank, heated with stirring to maintain 100 ° C., and extracted for 12 hours. The mixture was then heated, concentrated to about 1/3 of the initial volume of the mixture, filtered, and added with trace elements or fertilizers. 1 liquid fertilizer was prepared.

또한 Also

추출 온도를 100℃에서 가열추출하지 않고 상온에서 추출하여 시료 2 액상 비료를 제조하였다.Extraction temperature was extracted at room temperature without heating extraction at 100 ℃ to prepare Sample 2 liquid fertilizer.

상기의 방법으로 제조된 시료 1, 시료 2 비료의 성분과 물성을 분석하여 그 결과를 하기 표 2에서 나타내었다. Analysis of the components and physical properties of Sample 1, Sample 2 fertilizer prepared by the above method is shown in Table 2 below.

구 분division 니코틴 성분량(중량%)Nicotine content (% by weight) PHPH 비중importance 시료 1Sample 1 0.850.85 6.26.2 1.231.23 시료 2Sample 2 0.230.23 6.46.4 1.081.08

상기 표 1에 나타난 바와 같이 주성분, PH, 비중의 비교분석 결과 시료 1과같이 가열추출농축 방법이 상온에서 추출한 것에 비하여 니코틴함량이 월등히 높음을 알 수 있었다.As shown in Table 1, as a result of the comparative analysis of the main components, PH, and specific gravity, it was found that the nicotine content was much higher than that of the heat extraction concentration method extracted at room temperature as in Sample 1.

2) 액상 비료의 효능실험2) Efficacy test of liquid fertilizer

상기 가열추출농축 방법으로 제조된 시료 1의 액상 비료를 뿌리혹병이 잘 발생하는 경기도 안성시 미양면소재 비닐하우스에서 시료 1, 대조약제와 무처리구 처리하여 재배시험을 하였다.The liquid fertilizer of Sample 1 prepared by the method of heat extraction concentration was cultivated by treating the sample 1, control agent and no treatment in a vinyl house located in Miyang-myeon, Anseong-si, Gyeonggi-do, where the root-knot disease occurs well.

상기 대조약제는 영일케미컬의 배추혹뿌리병농약인 제품명 영일혹안나를 사용하였으며, 시험방법은 표 3의 조건에 따라 시험하였다.The control agent was used as a product name Young-il Anna Anna, a cabbage hump root pesticide of Young-il Chemical, the test method was tested according to the conditions of Table 3.

1. 공시품종1. Disclosure varieties 배추 (노랑 봄배추)Chinese Cabbage (Yellow Spring Cabbage) 2. 공시비료2. Public Fertilizer 시료 1 제품Sample 1 product 3. 포장위치3. Packing location 경기도 안성시 미양면소재 포장Miyang Cotton Packaging, Anseong-si, Gyeonggi-do 4. 포장 토질4. Packing Soil 사질양토Sandy loam 5. 시험기간5. Test period 2008년 3월 24일 ~ 5월 24일 (60일)March 24-May 24, 2008 (60th) 6. 시험구 배치 및 반복6. Test Piece Placement and Repetition 1처리 3반복 1 treatment 3 repetitions 7. 처리내용7. Contents of Treatment 정식 전 토양 전면에 충분히 살포. 토양혼화. (300평당 공시료 2L 사용)Full spray over soil before planting. Soil admixture. (Use 2L of public charge per 300 pyeong)

정식(定植) 전 시험구에 따라 약제 처리를 하고 정식을 하였고 정식 후 30일이 경과한 다음 생육상태를 조사하였으며 20일이 경과한 후 수확하여 수량과 뿌리상태를 달관조사 하여 다음 표 4에 그 결과를 나타내었다.After treatment, the drug was treated and formulated according to the pre-establishment test, and after 30 days, the growth condition was examined. After 20 days, the harvest was harvested and the yield and root condition were examined. The results are shown.

조사항목Survey Item 시료 1처리구Sample 1 treatment zone 대조약제 처리구Control agent 무처리구No treatment 엽폭 (cm)Lobe width (cm) 24.8 (115)24.8 (115) 25.1 (116)25.1 (116) 21.6 (100)21.6 (100) 엽장 (cm)Leaf length (cm) 29.2 (120)29.2 (120) 27,8 (114)27,8 (114) 24.4 (100)24.4 (100) 초장 (cm)Extra long (cm) 29.0 (120)29.0 (120) 27.6(115)27.6 (115) 24.1 (100)24.1 (100) 생체중 (kg)Live weight (kg) 2.6 (217)2.6 (217) 2.3 (192)2.3 (192) 1.2 (100)1.2 (100) 뿌리혹병 발생율 (%)Root gall disease incidence (%) 13 (31)13 (31) 14 (33)14 (33) 42 (100)42 (100)

* ( ) = 무처리구에 대한 백분율 지수이다.* () = Percentage index for no treatment.

* 생체중 수치는 시험 구 전체의 무계를 포기수로 나누어 구한 한 포기의 중량이다.* The live weight value is the weight of abandonment obtained by dividing the entire test plot by the abandonment count.

* 뿌리혹병에 대한 달관조사는 배추를 반복 처리 구별로 모두 수확하여 뿌리를 잘라 뿌리혹의 발생을 구별하여 각각의 무게를 달아 백분율로 표시하였다.* In the case of root gall disease, all the cabbages were harvested by repetitive treatment, the roots were cut, and the occurrence of root gall was distinguished.

* 표 4의 시험결과는 1처리 3반복의 평균을 계산하여 표시한 것이다.* The test results in Table 4 are calculated and displayed as the average of 1 treatment and 3 repetitions.

생육조사에 의한 결과는 무처리구에 비해 대조약제 처리구와 시료 1처리구는 생육초기부터 뿌리혹병이 발생하지 않아 생육상태가 양호한 것으로 분석되며 대조약제처리구에 비해 시료 1처리구의 생육이 좋은 것은 담배와 비료성분에 의한 효과로 분석되었다.The results of the growth investigation showed that the control group and the sample 1 treatment group had better root growth than the non-treated group because root gall disease did not occur from the beginning of growth. The effect was analyzed by.

상기 표 4에서 나타난 바와 같이 본 발명에 따라 제조된 시료 1처리구와 대조약제 처리구와 무처리구와의 효과를 비교하면 시료 1과 대조약제 처리구는 무처리구에 비해 뿌리혹병에 대한 예방, 치료효과는 큰 차이로 효과가 확인되었다.As shown in Table 4, when comparing the effect of the sample 1 treatment group and the control agent treated group and the non-treated group prepared according to the present invention, the sample 1 and the control agent treated group had a significant difference in the prevention and treatment effect against root gall disease compared to the non-treated group. The effect was confirmed.

또한 대조약제 (혹안나 수화제) 와의 차이는 대등소이 하나 화학농약의 효과에 비해 약간의 좋은 생육 상태와 뿌리혹병 예방치료에 더욱 효과적인 것으로 확인 되었다.In addition, the difference with the reference drug (Hannah Hydration) was found to be more effective in the prevention of root growth and some good growth compared to the effect of chemically equivalent pesticides.

2. 본 발명에 따른 담배부산물을 이용한 뿌리혹병 예방 또는 치료용 입상 비료 제조 및 효능실험2. Preparation and efficacy test of granular fertilizer for preventing or treating root gall disease using tobacco byproducts according to the present invention

1) 입상 비료 제조 및 함량분석1) Granular Fertilizer Preparation and Content Analysis

원재료명Raw material name 혼합비율 (kg)Mixing ratio (kg) 담배부산물Tobacco by-products 2.002.00 수산화칼슘Calcium hydroxide 0.400.40 부식산Humic acid 0.200.20 water 0.400.40

하기 표 5에 따라 각 원료를 계량하고 혼합물을 제조한 후, 펠렛기를 이용하여 1~ 5mm의 규격으로 입상형태로 제조하고, 혼합물과 미생물을 중량비 97 대 3로 혼합하고 건조하여 입상 비료를 제조하였다.After weighing each raw material and preparing a mixture according to the following Table 5, it was prepared in the form of granules in the size of 1 ~ 5mm by using a pellet machine, and the mixture and microorganisms were mixed in a weight ratio of 97 to 3 and dried to prepare a granular fertilizer. .

상기의 방법으로 제조된 입상 비료의 성분과 물성을 분석하여 그 결과를 하기 표 6에서 나타내었다.Analysis of the components and physical properties of the granular fertilizer prepared by the above method is shown in Table 6 below.

구 분division 니코틴 성분량 (중량%)Nicotine content (% by weight) PHPH 수분 %moisture % 입상 비료Granular fertilizer 0.770.77 6.76.7 1515

상기 표 6에 나타낸바와 같이 주성분인 니코틴이 국내산 연초가 함유하고 있는 니코틴이 0.5 ~ 1%인 것에 비하면 완성 제품의 니코틴이 0.77%이면 아주 양호한 것임을 알 수 있었다.As shown in Table 6 above, it was found that nicotine of the finished product was very good when nicotine of the finished product was 0.77% as compared to 0.5-1% of nicotine contained in domestic tobacco.

2) 입상 비료의 효능실험2) Efficacy test of granular fertilizer

상기 방법으로 제조된 본 발명의 뿌리혹병 예방 또는 치료용 입상 비료를 뿌리혹병이 잘 발생하는 경기도 안성시 미양면소재 비닐하우스에서 무처리구와 대조약제를 비교 재배시험을 하였다.Root gall disease prevention or treatment of the root gall disease of the present invention prepared by the above method was compared to the non-treated group and control agent in a plastic house in Miyang-myeon, Anyang-si, Gyeonggi-do, where root gall disease occurs well.

시험 수행방법 : 다음 표 7의 조건에 따라 시험하였다.Test Execution Method

1. 공시품종1. Disclosure varieties 배추 (노랑 봄배추) Chinese Cabbage (Yellow Spring Cabbage) 2. 공시비료2. Public Fertilizer 입상 비료 Granular fertilizer 3. 포장위치3. Packing location 경기도 안성시 미양면소재 포장 Miyang Cotton Packaging, Anseong-si, Gyeonggi-do 4. 포장 토질4. Packing Soil 사질양토 Sandy loam 5. 시험기간5. Test period 2008년 4월 5일 ~ 6월 10일 April 5-June 10, 2008 6. 시험구 배치 및 반복6. Test Piece Placement and Repetition 1처리 3반복 1 treatment 3 repetitions 7. 처리내용7. Contents of Treatment 정식전 토양 전면에 충분히 살포 후 토양혼화 (300평당 공시료 5KG 사용) Soil admixture after spraying the entire soil before planting (use 5KG blank sample per 300 pyeong)

정식(定植) 전 시험구에 따라 약제 처리를 하고 정식을 하였고 정식 후 30일이 경과한 다음 생육상태를 조사하였으며 20일이 경과한 후 수확하여 수량과 뿌리상태를 달관조사 하여 다음 표 8에 그 결과를 나타내었다.After treatment, the drug was treated and formulated according to the pre-establishment test, and after 30 days, the growth condition was examined. After 20 days, the harvest was harvested and the yield and root condition were examined. The results are shown.

조사항목Survey Item 입상비료 처리구Granular Fertilizer 대조약제 처리구Control agent 무처리구No treatment 엽폭 (cm)Lobe width (cm) 24.9 (122)24.9 (122) 25.4 (125)25.4 (125) 20.3 (100)20.3 (100) 엽장 (cm)Leaf length (cm) 27.1 (120)27.1 (120) 26.8 (118)26.8 (118) 22.6 (100)22.6 (100) 초장 (cm)Extra long (cm) 26.7 (121)26.7 (121) 26.5 (120)26.5 (120) 22.1 (100)22.1 (100) 생체중 (kg)Live weight (kg) 3.1 (182)3.1 (182) 2.9 (170)2.9 (170) 1.7 (100)1.7 (100) 뿌리혹병 발생율 (%)Root gall disease incidence (%) 12.4 (26.1)12.4 (26.1) 12.6 (26. )12.6 (26.) 47.5 (100)47.5 (100)

* ( )안은 무처리구에 대한 백분율 지수이다.* () Is the percentage index for the untreated.

* 표 8의 시험결과는 1처리 3반복의 평균을 계산하여 표시한 것이다.* The test results in Table 8 are calculated and displayed as the average of 1 treatment and 3 repetitions.

* 뿌리혹병에 대한 달관조사는 배추를 반복 처리 구별로 모두 수확하여 뿌리를 잘라 뿌리혹의 발생을 구별로 각각의 중량을 달아 백분율로 표시하였다.* In the case of root gall disease, all cabbages were harvested by repetitive treatment, and the roots were cut and weighed to distinguish the occurrence of root gall.

* 생체 중 수치는 시험구 전체의 무계를 포기수로 나누어 구한 한 포기의중량이다.* The live weight value is the weight of abandonment calculated by dividing the entire test area by the abandonment number.

정식 후 30일이 경과한 후, 생육조사를 실시한 결과 무처리구는 부분적으로 뿌리혹병이 발생하여 생육저하가 나타나 보였으며 입상비료 처리구와 대조약제 처리구는 뿌리혹병이 초기에 나타나지 않아 생육상태가 표 8에서와 같이 무처리구에 비해 월등히 효과가 있었다.After 30 days after the establishment, the growth test showed that root untreated group showed partial growth and the growth was decreased. In the granulated fertilizer treatment and control drug treatment group, root nodule disease did not appear early. As compared to the untreated, the effect was much better.

상기 표 8에 나타난 바와 같이 본 발명에 따른 뿌리혹병 예방 또는 치료용 입상 비료는 앞에서의 뿌리혹병 예방 또는 치료용 액상 비료와 거의 동등한 효과가 있는 것을 확인할 수 있다.As shown in Table 8, it can be confirmed that the granular fertilizer for preventing or treating root gall disease according to the present invention has almost the same effect as the liquid fertilizer for preventing or treating root gall disease.

따라서 본 발명에 따른 뿌리혹병 예방 또는 치료용 액상 또는 입상 비료는 배추 뿌리혹병에 탁월한 효과가 인정되므로 화학 농약사용을 대체할 친환경 배추뿌리혹병 예방 및 치료용 비료로 사용될 수 있을 것이다.Therefore, liquid or granular fertilizer for preventing or treating root gall disease according to the present invention can be used as an environmentally friendly cabbage root gall disease prevention and treatment to replace the use of chemical pesticides because the excellent effect is recognized in Chinese cabbage root gall.

Claims (7)

담배부산물 100중량부에 에틸알코올 20~30중량부, 물 80~85중량부, 복합비료 40~45중량부를 첨가하여 추출·농축하여 제조되는 것을 특징으로 하는 뿌리혹병 예방 또는 치료용 액상 비료.20 to 30 parts by weight of ethyl alcohol, 80 to 85 parts by weight of water, and 40 to 45 parts by weight of compound fertilizer by extracting and concentrating liquid fertilizer for preventing or treating root gall disease. 제1항에 있어서,The method of claim 1, 상기 복합비료는 질소, 인산, 칼륨의 비료성분 중 선택되는 2종 이상을 함유하고 붕소, 망간, 철, 아연, 구리, 몰리브덴, 고토, 칼슘 중 선택되는 2종 이상 함유하는 비료를 특징으로 하는 뿌리혹병 예방 또는 치료용 액상 비료.The compound fertilizer contains two or more selected from the fertilizer components of nitrogen, phosphoric acid, potassium, and the root knot characterized by fertilizer containing two or more selected from boron, manganese, iron, zinc, copper, molybdenum, goto, calcium Liquid fertilizer for disease prevention or treatment. 담배부산물 100중량부에 에틸알코올 20~30중량부, 물 80~85중량부, 복합비료 40~45중량부를 혼합한 혼합물을 가열탱크에 투입하는 단계;Adding a mixture of 20 to 30 parts by weight of ethyl alcohol, 80 to 85 parts by weight of water, and 40 to 45 parts by weight of complex fertilizer to 100 parts by weight of tobacco by-products in a heating tank; 상기 가열탱크를 95~100℃로 가열·교반하는 단계;Heating and stirring the heating tank at 95˜100 ° C .; 상기 혼합물이 최초 혼합물의 부피의 27~35%가 될 때까지 농축하는 단계를 포함하는 것을 특징으로 하는 뿌리혹병 예방 또는 치료용 액상 비료 제조방법.Method for producing a liquid fertilizer for the prevention or treatment of root-knot disease comprising the step of concentrating until the mixture is 27 to 35% of the volume of the initial mixture. 담배부산물 100중량부에 수산화칼슘 15~25중량부, 부식산 10~15중량부, 물 22~28중량부, 미생물 4~10중량부를 첨가혼합하고 입상형태로 제조되는 것을 특징으로 하는 뿌리혹병 예방 또는 치료용 입상 비료.To prevent root root disease, characterized in that the mixture is prepared in a granular form by adding 15 to 25 parts by weight of calcium hydroxide, 10 to 15 parts by weight of humic acid, 22 to 28 parts by weight of water, and 4 to 10 parts by weight of microorganisms. Granular fertilizer for treatment. 제4항에 있어서,The method of claim 4, wherein 상기 미생물은 광합성세균, 바실러스, 유산균 및 효모균 중 선택되는 2종이상의 혼합균주인 것을 특징으로 하는 것을 뿌리혹병 예방 또는 치료용 입상 비료.The microorganism is a granular fertilizer for preventing or treating root gall disease, characterized in that the mixture of at least two species selected from photosynthetic bacteria, Bacillus, lactic acid bacteria and yeast. 담배부산물 100중량부에 수산화칼슘 15~25중량부, 부식산 10~15중량부, 물 22~28중량부를 첨가하여 혼합한 혼합물을 제조하는 단계;Preparing a mixture by adding 15 to 25 parts by weight of calcium hydroxide, 10 to 15 parts by weight of humic acid and 22 to 28 parts by weight of water to 100 parts by weight of tobacco byproducts; 상기 혼합물을 펠렛기계를 이용하여 1~5㎜크기의 입상형태로 제조하는 단계;Preparing the mixture into granules having a size of 1 to 5 mm using a pellet machine; 상기 입상형태로 제조된 혼합물에 미생물을 중량비 95~98 대 2~5으로 혼합·건조하는 단계를 포함하는 것을 특징으로 하는 뿌리혹병 예방 또는 치료용 입상 비료제조방법.Granules fertilizer manufacturing method for preventing or treating root gall disease, comprising the step of mixing and drying the microorganism in the mixture prepared in the granular form in a weight ratio of 95 ~ 98 to 2 ~ 5. 제1항 또는 제4항의 비료를 정식(定植)전 토양에 공급하는 것을 특징으로 하는 뿌리혹병 예방 또는 치료용 비료 사용방법.A method of using a fertilizer for preventing or treating root-knot disease, wherein the fertilizer of claim 1 or 4 is supplied to the soil before planting.
KR1020080066685A 2008-07-09 2008-07-09 A manure for preventing or treating clubroot using a by-product of tabacco and manufacturing method the same KR20080069953A (en)

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