KR20070089129A - 코어-쉘 입자 - Google Patents
코어-쉘 입자 Download PDFInfo
- Publication number
- KR20070089129A KR20070089129A KR1020077011011A KR20077011011A KR20070089129A KR 20070089129 A KR20070089129 A KR 20070089129A KR 1020077011011 A KR1020077011011 A KR 1020077011011A KR 20077011011 A KR20077011011 A KR 20077011011A KR 20070089129 A KR20070089129 A KR 20070089129A
- Authority
- KR
- South Korea
- Prior art keywords
- core
- shell
- weight
- methacrylate
- shell particles
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
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- 239000002245 particle Substances 0.000 title claims description 40
- 239000011258 core-shell material Substances 0.000 title claims description 3
- 239000011162 core material Substances 0.000 claims abstract description 86
- 239000010420 shell particle Substances 0.000 claims abstract description 69
- 239000007771 core particle Substances 0.000 claims abstract description 66
- 239000011257 shell material Substances 0.000 claims abstract description 54
- 239000000178 monomer Substances 0.000 claims abstract description 34
- 229920001577 copolymer Polymers 0.000 claims abstract description 22
- 239000000463 material Substances 0.000 claims abstract description 18
- 238000009826 distribution Methods 0.000 claims abstract description 8
- 230000009969 flowable effect Effects 0.000 claims abstract description 6
- 239000007787 solid Substances 0.000 claims abstract description 6
- 239000000203 mixture Substances 0.000 claims description 36
- 239000006185 dispersion Substances 0.000 claims description 34
- 238000000034 method Methods 0.000 claims description 31
- 229920000642 polymer Polymers 0.000 claims description 29
- 239000008187 granular material Substances 0.000 claims description 26
- 238000002360 preparation method Methods 0.000 claims description 24
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims description 20
- SOGAXMICEFXMKE-UHFFFAOYSA-N Butylmethacrylate Chemical group CCCCOC(=O)C(C)=C SOGAXMICEFXMKE-UHFFFAOYSA-N 0.000 claims description 18
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical group COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 claims description 16
- 229910052751 metal Inorganic materials 0.000 claims description 16
- 239000002184 metal Substances 0.000 claims description 16
- 238000006116 polymerization reaction Methods 0.000 claims description 16
- 238000004519 manufacturing process Methods 0.000 claims description 15
- 150000001875 compounds Chemical class 0.000 claims description 14
- 230000008569 process Effects 0.000 claims description 14
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- CQEYYJKEWSMYFG-UHFFFAOYSA-N butyl acrylate Chemical group CCCCOC(=O)C=C CQEYYJKEWSMYFG-UHFFFAOYSA-N 0.000 claims description 11
- 239000003995 emulsifying agent Substances 0.000 claims description 11
- 239000010410 layer Substances 0.000 claims description 11
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 10
- 229920006037 cross link polymer Polymers 0.000 claims description 10
- -1 alkyl aryl methacrylates Chemical class 0.000 claims description 9
- 239000002671 adjuvant Substances 0.000 claims description 8
- 239000000839 emulsion Substances 0.000 claims description 8
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- 239000011229 interlayer Substances 0.000 claims description 8
- 239000002612 dispersion medium Substances 0.000 claims description 7
- 230000000694 effects Effects 0.000 claims description 7
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims description 6
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 6
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 6
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- 229910010272 inorganic material Inorganic materials 0.000 claims description 4
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- 238000002844 melting Methods 0.000 claims description 4
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- 239000002904 solvent Substances 0.000 claims description 4
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 claims description 3
- 239000004793 Polystyrene Substances 0.000 claims description 3
- 150000001412 amines Chemical class 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 3
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- 239000003607 modifier Substances 0.000 claims description 3
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- 229920000620 organic polymer Polymers 0.000 claims description 3
- 229920002223 polystyrene Polymers 0.000 claims description 3
- LMAUULKNZLEMGN-UHFFFAOYSA-N 1-ethyl-3,5-dimethylbenzene Chemical compound CCC1=CC(C)=CC(C)=C1 LMAUULKNZLEMGN-UHFFFAOYSA-N 0.000 claims description 2
- RUMACXVDVNRZJZ-UHFFFAOYSA-N 2-methylpropyl 2-methylprop-2-enoate Chemical compound CC(C)COC(=O)C(C)=C RUMACXVDVNRZJZ-UHFFFAOYSA-N 0.000 claims description 2
- CFVWNXQPGQOHRJ-UHFFFAOYSA-N 2-methylpropyl prop-2-enoate Chemical compound CC(C)COC(=O)C=C CFVWNXQPGQOHRJ-UHFFFAOYSA-N 0.000 claims description 2
- NJCDRURWJZAMBM-UHFFFAOYSA-N 6-phenyl-1h-1,3,5-triazin-2-one Chemical class OC1=NC=NC(C=2C=CC=CC=2)=N1 NJCDRURWJZAMBM-UHFFFAOYSA-N 0.000 claims description 2
- 108010010803 Gelatin Proteins 0.000 claims description 2
- 229920000881 Modified starch Polymers 0.000 claims description 2
- WHNWPMSKXPGLAX-UHFFFAOYSA-N N-Vinyl-2-pyrrolidone Chemical compound C=CN1CCCC1=O WHNWPMSKXPGLAX-UHFFFAOYSA-N 0.000 claims description 2
- QVHMSMOUDQXMRS-UHFFFAOYSA-N PPG n4 Chemical compound CC(O)COC(C)COC(C)COC(C)CO QVHMSMOUDQXMRS-UHFFFAOYSA-N 0.000 claims description 2
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 2
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 2
- GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical group CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 claims description 2
- UWHCKJMYHZGTIT-UHFFFAOYSA-N Tetraethylene glycol, Natural products OCCOCCOCCOCCO UWHCKJMYHZGTIT-UHFFFAOYSA-N 0.000 claims description 2
- 239000012963 UV stabilizer Substances 0.000 claims description 2
- 239000000853 adhesive Substances 0.000 claims description 2
- 230000001070 adhesive effect Effects 0.000 claims description 2
- 125000002947 alkylene group Chemical group 0.000 claims description 2
- 239000003963 antioxidant agent Substances 0.000 claims description 2
- AOJOEFVRHOZDFN-UHFFFAOYSA-N benzyl 2-methylprop-2-enoate Chemical compound CC(=C)C(=O)OCC1=CC=CC=C1 AOJOEFVRHOZDFN-UHFFFAOYSA-N 0.000 claims description 2
- 239000003139 biocide Substances 0.000 claims description 2
- 239000004305 biphenyl Substances 0.000 claims description 2
- WXNRYSGJLQFHBR-UHFFFAOYSA-N bis(2,4-dihydroxyphenyl)methanone Chemical class OC1=CC(O)=CC=C1C(=O)C1=CC=C(O)C=C1O WXNRYSGJLQFHBR-UHFFFAOYSA-N 0.000 claims description 2
- 229920001400 block copolymer Polymers 0.000 claims description 2
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 claims description 2
- 229920003086 cellulose ether Polymers 0.000 claims description 2
- OIWOHHBRDFKZNC-UHFFFAOYSA-N cyclohexyl 2-methylprop-2-enoate Chemical compound CC(=C)C(=O)OC1CCCCC1 OIWOHHBRDFKZNC-UHFFFAOYSA-N 0.000 claims description 2
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 claims description 2
- UIWXSTHGICQLQT-UHFFFAOYSA-N ethenyl propanoate Chemical compound CCC(=O)OC=C UIWXSTHGICQLQT-UHFFFAOYSA-N 0.000 claims description 2
- 238000007046 ethoxylation reaction Methods 0.000 claims description 2
- FKIRSCKRJJUCNI-UHFFFAOYSA-N ethyl 7-bromo-1h-indole-2-carboxylate Chemical compound C1=CC(Br)=C2NC(C(=O)OCC)=CC2=C1 FKIRSCKRJJUCNI-UHFFFAOYSA-N 0.000 claims description 2
- 229920000159 gelatin Polymers 0.000 claims description 2
- 239000008273 gelatin Substances 0.000 claims description 2
- 235000019322 gelatine Nutrition 0.000 claims description 2
- 235000011852 gelatine desserts Nutrition 0.000 claims description 2
- LNCPIMCVTKXXOY-UHFFFAOYSA-N hexyl 2-methylprop-2-enoate Chemical compound CCCCCCOC(=O)C(C)=C LNCPIMCVTKXXOY-UHFFFAOYSA-N 0.000 claims description 2
- LNMQRPPRQDGUDR-UHFFFAOYSA-N hexyl prop-2-enoate Chemical compound CCCCCCOC(=O)C=C LNMQRPPRQDGUDR-UHFFFAOYSA-N 0.000 claims description 2
- 235000019426 modified starch Nutrition 0.000 claims description 2
- NZIDBRBFGPQCRY-UHFFFAOYSA-N octyl 2-methylprop-2-enoate Chemical compound CCCCCCCCOC(=O)C(C)=C NZIDBRBFGPQCRY-UHFFFAOYSA-N 0.000 claims description 2
- ANISOHQJBAQUQP-UHFFFAOYSA-N octyl prop-2-enoate Chemical compound CCCCCCCCOC(=O)C=C ANISOHQJBAQUQP-UHFFFAOYSA-N 0.000 claims description 2
- 150000002894 organic compounds Chemical class 0.000 claims description 2
- GYDSPAVLTMAXHT-UHFFFAOYSA-N pentyl 2-methylprop-2-enoate Chemical compound CCCCCOC(=O)C(C)=C GYDSPAVLTMAXHT-UHFFFAOYSA-N 0.000 claims description 2
- ULDDEWDFUNBUCM-UHFFFAOYSA-N pentyl prop-2-enoate Chemical compound CCCCCOC(=O)C=C ULDDEWDFUNBUCM-UHFFFAOYSA-N 0.000 claims description 2
- 239000004014 plasticizer Substances 0.000 claims description 2
- 229920001451 polypropylene glycol Polymers 0.000 claims description 2
- 229920000036 polyvinylpyrrolidone Polymers 0.000 claims description 2
- 239000001267 polyvinylpyrrolidone Substances 0.000 claims description 2
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 claims description 2
- NHARPDSAXCBDDR-UHFFFAOYSA-N propyl 2-methylprop-2-enoate Chemical compound CCCOC(=O)C(C)=C NHARPDSAXCBDDR-UHFFFAOYSA-N 0.000 claims description 2
- PNXMTCDJUBJHQJ-UHFFFAOYSA-N propyl prop-2-enoate Chemical compound CCCOC(=O)C=C PNXMTCDJUBJHQJ-UHFFFAOYSA-N 0.000 claims description 2
- 229920005604 random copolymer Polymers 0.000 claims description 2
- 239000003381 stabilizer Substances 0.000 claims description 2
- 125000000472 sulfonyl group Chemical group *S(*)(=O)=O 0.000 claims description 2
- 239000002562 thickening agent Substances 0.000 claims description 2
- ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 claims description 2
- 238000009281 ultraviolet germicidal irradiation Methods 0.000 claims description 2
- 230000000996 additive effect Effects 0.000 claims 4
- YHCGGLXPGFJNCO-UHFFFAOYSA-N 2-(2H-benzotriazol-4-yl)phenol Chemical class OC1=CC=CC=C1C1=CC=CC2=C1N=NN2 YHCGGLXPGFJNCO-UHFFFAOYSA-N 0.000 claims 1
- LCZVSXRMYJUNFX-UHFFFAOYSA-N 2-[2-(2-hydroxypropoxy)propoxy]propan-1-ol Chemical compound CC(O)COC(C)COC(C)CO LCZVSXRMYJUNFX-UHFFFAOYSA-N 0.000 claims 1
- 239000004368 Modified starch Substances 0.000 claims 1
- 150000001252 acrylic acid derivatives Chemical class 0.000 claims 1
- 230000006866 deterioration Effects 0.000 claims 1
- 238000002156 mixing Methods 0.000 claims 1
- YTSACTNRGUJEGO-UHFFFAOYSA-N oxirane prop-1-ene Chemical group CC=C.C1CO1 YTSACTNRGUJEGO-UHFFFAOYSA-N 0.000 claims 1
- 125000002572 propoxy group Chemical group [*]OC([H])([H])C(C([H])([H])[H])([H])[H] 0.000 claims 1
- YGSDEFSMJLZEOE-UHFFFAOYSA-M salicylate Chemical compound OC1=CC=CC=C1C([O-])=O YGSDEFSMJLZEOE-UHFFFAOYSA-M 0.000 claims 1
- 229960001860 salicylate Drugs 0.000 claims 1
- 238000007127 saponification reaction Methods 0.000 claims 1
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims 1
- 229920002554 vinyl polymer Polymers 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 27
- 238000000465 moulding Methods 0.000 description 25
- 239000000049 pigment Substances 0.000 description 21
- 239000000243 solution Substances 0.000 description 17
- 230000009471 action Effects 0.000 description 15
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 description 14
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 12
- 230000003287 optical effect Effects 0.000 description 12
- 230000000875 corresponding effect Effects 0.000 description 11
- 238000006243 chemical reaction Methods 0.000 description 10
- 238000001816 cooling Methods 0.000 description 10
- 235000019333 sodium laurylsulphate Nutrition 0.000 description 10
- 238000003756 stirring Methods 0.000 description 10
- 239000008367 deionised water Substances 0.000 description 9
- 229910021641 deionized water Inorganic materials 0.000 description 9
- GPRLSGONYQIRFK-MNYXATJNSA-N triton Chemical compound [3H+] GPRLSGONYQIRFK-MNYXATJNSA-N 0.000 description 9
- 229910044991 metal oxide Inorganic materials 0.000 description 8
- 150000004706 metal oxides Chemical class 0.000 description 8
- FBCQUCJYYPMKRO-UHFFFAOYSA-N prop-2-enyl 2-methylprop-2-enoate Chemical compound CC(=C)C(=O)OCC=C FBCQUCJYYPMKRO-UHFFFAOYSA-N 0.000 description 8
- 239000000976 ink Substances 0.000 description 7
- 239000002105 nanoparticle Substances 0.000 description 7
- JHWGFJBTMHEZME-UHFFFAOYSA-N 4-prop-2-enoyloxybutyl prop-2-enoate Chemical compound C=CC(=O)OCCCCOC(=O)C=C JHWGFJBTMHEZME-UHFFFAOYSA-N 0.000 description 6
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- 125000003118 aryl group Chemical group 0.000 description 6
- 238000007639 printing Methods 0.000 description 6
- 229910004298 SiO 2 Inorganic materials 0.000 description 5
- 238000000576 coating method Methods 0.000 description 5
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- 238000006068 polycondensation reaction Methods 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- JVBXVOWTABLYPX-UHFFFAOYSA-L sodium dithionite Chemical compound [Na+].[Na+].[O-]S(=O)S([O-])=O JVBXVOWTABLYPX-UHFFFAOYSA-L 0.000 description 5
- 239000007858 starting material Substances 0.000 description 5
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 4
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- JIGUQPWFLRLWPJ-UHFFFAOYSA-N Ethyl acrylate Chemical compound CCOC(=O)C=C JIGUQPWFLRLWPJ-UHFFFAOYSA-N 0.000 description 4
- 239000004952 Polyamide Substances 0.000 description 4
- 125000001931 aliphatic group Chemical group 0.000 description 4
- 239000002537 cosmetic Substances 0.000 description 4
- 238000007306 functionalization reaction Methods 0.000 description 4
- 230000009477 glass transition Effects 0.000 description 4
- 239000003999 initiator Substances 0.000 description 4
- 238000001746 injection moulding Methods 0.000 description 4
- 239000011159 matrix material Substances 0.000 description 4
- 150000002739 metals Chemical class 0.000 description 4
- 150000002924 oxiranes Chemical group 0.000 description 4
- PNJWIWWMYCMZRO-UHFFFAOYSA-N pent‐4‐en‐2‐one Natural products CC(=O)CC=C PNJWIWWMYCMZRO-UHFFFAOYSA-N 0.000 description 4
- 229920002647 polyamide Polymers 0.000 description 4
- 229920000728 polyester Polymers 0.000 description 4
- 238000012545 processing Methods 0.000 description 4
- CHQMHPLRPQMAMX-UHFFFAOYSA-L sodium persulfate Chemical compound [Na+].[Na+].[O-]S(=O)(=O)OOS([O-])(=O)=O CHQMHPLRPQMAMX-UHFFFAOYSA-L 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- 229910010413 TiO 2 Inorganic materials 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- ROOXNKNUYICQNP-UHFFFAOYSA-N ammonium persulfate Chemical compound [NH4+].[NH4+].[O-]S(=O)(=O)OOS([O-])(=O)=O ROOXNKNUYICQNP-UHFFFAOYSA-N 0.000 description 3
- 239000012935 ammoniumperoxodisulfate Substances 0.000 description 3
- 238000010560 atom transfer radical polymerization reaction Methods 0.000 description 3
- 238000009472 formulation Methods 0.000 description 3
- 229920001519 homopolymer Polymers 0.000 description 3
- 229930195733 hydrocarbon Natural products 0.000 description 3
- 150000002430 hydrocarbons Chemical class 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 239000003973 paint Substances 0.000 description 3
- 229920001568 phenolic resin Polymers 0.000 description 3
- 229920000647 polyepoxide Polymers 0.000 description 3
- 239000003505 polymerization initiator Substances 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 239000002243 precursor Substances 0.000 description 3
- 229910018072 Al 2 O 3 Inorganic materials 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 229910002601 GaN Inorganic materials 0.000 description 2
- JMASRVWKEDWRBT-UHFFFAOYSA-N Gallium nitride Chemical compound [Ga]#N JMASRVWKEDWRBT-UHFFFAOYSA-N 0.000 description 2
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 2
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 2
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- 229920002396 Polyurea Polymers 0.000 description 2
- 229910006404 SnO 2 Inorganic materials 0.000 description 2
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 2
- 150000001298 alcohols Chemical class 0.000 description 2
- 229910052786 argon Inorganic materials 0.000 description 2
- 239000011230 binding agent Substances 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 2
- 238000003490 calendering Methods 0.000 description 2
- 230000002759 chromosomal effect Effects 0.000 description 2
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- 238000002474 experimental method Methods 0.000 description 2
- 238000001125 extrusion Methods 0.000 description 2
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- SLGWESQGEUXWJQ-UHFFFAOYSA-N formaldehyde;phenol Chemical compound O=C.OC1=CC=CC=C1 SLGWESQGEUXWJQ-UHFFFAOYSA-N 0.000 description 2
- 125000000524 functional group Chemical group 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 238000012994 industrial processing Methods 0.000 description 2
- 230000003993 interaction Effects 0.000 description 2
- 239000012948 isocyanate Chemical group 0.000 description 2
- 150000002513 isocyanates Chemical group 0.000 description 2
- 210000003734 kidney Anatomy 0.000 description 2
- 239000012528 membrane Substances 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 229920002113 octoxynol Polymers 0.000 description 2
- 238000007645 offset printing Methods 0.000 description 2
- 239000008188 pellet Substances 0.000 description 2
- 230000000737 periodic effect Effects 0.000 description 2
- 150000002978 peroxides Chemical class 0.000 description 2
- JRKICGRDRMAZLK-UHFFFAOYSA-N peroxydisulfuric acid Chemical class OS(=O)(=O)OOS(O)(=O)=O JRKICGRDRMAZLK-UHFFFAOYSA-N 0.000 description 2
- 229910052698 phosphorus Inorganic materials 0.000 description 2
- 239000011574 phosphorus Substances 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- 229920002635 polyurethane Polymers 0.000 description 2
- 239000004814 polyurethane Substances 0.000 description 2
- 108090000623 proteins and genes Proteins 0.000 description 2
- 102000004169 proteins and genes Human genes 0.000 description 2
- 239000002096 quantum dot Substances 0.000 description 2
- 238000010526 radical polymerization reaction Methods 0.000 description 2
- 239000012429 reaction media Substances 0.000 description 2
- 238000010992 reflux Methods 0.000 description 2
- GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 239000004065 semiconductor Substances 0.000 description 2
- 150000004756 silanes Chemical group 0.000 description 2
- HRZFUMHJMZEROT-UHFFFAOYSA-L sodium disulfite Chemical compound [Na+].[Na+].[O-]S(=O)S([O-])(=O)=O HRZFUMHJMZEROT-UHFFFAOYSA-L 0.000 description 2
- 229940083575 sodium dodecyl sulfate Drugs 0.000 description 2
- HYHCSLBZRBJJCH-UHFFFAOYSA-M sodium hydrosulfide Chemical compound [Na+].[SH-] HYHCSLBZRBJJCH-UHFFFAOYSA-M 0.000 description 2
- 235000010262 sodium metabisulphite Nutrition 0.000 description 2
- 238000006557 surface reaction Methods 0.000 description 2
- ZXDDPOHVAMWLBH-UHFFFAOYSA-N 2,4-Dihydroxybenzophenone Chemical class OC1=CC(O)=CC=C1C(=O)C1=CC=CC=C1 ZXDDPOHVAMWLBH-UHFFFAOYSA-N 0.000 description 1
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- YMOONIIMQBGTDU-UHFFFAOYSA-N 2-bromoethenylbenzene Chemical class BrC=CC1=CC=CC=C1 YMOONIIMQBGTDU-UHFFFAOYSA-N 0.000 description 1
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Classifications
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K9/00—Use of pretreated ingredients
- C08K9/08—Ingredients agglomerated by treatment with a binding agent
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F257/00—Macromolecular compounds obtained by polymerising monomers on to polymers of aromatic monomers as defined in group C08F12/00
- C08F257/02—Macromolecular compounds obtained by polymerising monomers on to polymers of aromatic monomers as defined in group C08F12/00 on to polymers of styrene or alkyl-substituted styrenes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F292/00—Macromolecular compounds obtained by polymerising monomers on to inorganic materials
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J7/00—Chemical treatment or coating of shaped articles made of macromolecular substances
- C08J7/04—Coating
Landscapes
- Chemical & Material Sciences (AREA)
- Medicinal Chemistry (AREA)
- Organic Chemistry (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Graft Or Block Polymers (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Soft Magnetic Materials (AREA)
- Manufacturing Of Micro-Capsules (AREA)
- Glanulating (AREA)
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| DE102004055303A DE102004055303A1 (de) | 2004-11-16 | 2004-11-16 | Kern-Mantel-Partikel |
| DE102004055303.3 | 2004-11-16 |
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| KR20070089129A true KR20070089129A (ko) | 2007-08-30 |
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| JP (1) | JP2008520775A (enExample) |
| KR (1) | KR20070089129A (enExample) |
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| AT (1) | ATE416206T1 (enExample) |
| BR (1) | BRPI0518335A2 (enExample) |
| CA (1) | CA2587477A1 (enExample) |
| DE (2) | DE102004055303A1 (enExample) |
| MX (1) | MX2007005911A (enExample) |
| RU (1) | RU2007122279A (enExample) |
| TW (1) | TW200631967A (enExample) |
| WO (1) | WO2006053640A1 (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| KR20180004375A (ko) * | 2016-07-01 | 2018-01-11 | 삼성디스플레이 주식회사 | 유기 발광 디스플레이 장치 및 이의 제조 방법 |
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| JP5468741B2 (ja) * | 2008-02-18 | 2014-04-09 | 株式会社日本触媒 | 水性樹脂組成物及びそれを含む建築外装トップコート用塗料 |
| DE102008028638A1 (de) | 2008-06-18 | 2009-12-24 | Henkel Ag & Co. Kgaa | Kleb- und Dichtstoff oder Strukturschaum auf Epoxidbasis enthaltend anorganische Nanopartikel mit Acrylsäureester-haltiger Hülle |
| WO2010001894A1 (ja) * | 2008-07-04 | 2010-01-07 | 住友化学株式会社 | 水スラリーおよびその製造方法 |
| DE102008031555A1 (de) | 2008-07-07 | 2010-01-14 | Henkel Ag & Co. Kgaa | Polymerisierbare Zusammensetzung enthaltend anorganische Partikel mit organischer Hülle |
| DE102008053520A1 (de) | 2008-10-28 | 2010-05-06 | Henkel Ag & Co. Kgaa | Strukturschaum auf Epoxidbasis mit thermoplastischen Polyurethanen |
| DE102008053518A1 (de) | 2008-10-28 | 2010-06-02 | Henkel Ag & Co. Kgaa | Epoxid-basierter Strukturschaum mit verbesserter Zähigkeit |
| DE102009000813A1 (de) | 2009-02-12 | 2010-08-19 | Evonik Degussa Gmbh | Fluoreszenzkonversionssolarzelle I Herstellung im Plattengußverfahren |
| DE102009002386A1 (de) | 2009-04-15 | 2010-10-21 | Evonik Degussa Gmbh | Fluoreszenzkonversionssolarzelle - Herstellung im Spritzgussverfahren |
| DE102009026548A1 (de) | 2009-05-28 | 2011-03-24 | Henkel Ag & Co. Kgaa | Klebefolie oder Klebeband auf Basis von Epoxiden |
| DE102009027431A1 (de) | 2009-07-02 | 2011-01-05 | Evonik Degussa Gmbh | Fluoreszenzkonversionssolarzelle - Herstellung im Extrusionsverfahren oder im Coextrusionsverfahren |
| DE102009028180A1 (de) | 2009-08-03 | 2011-02-10 | Henkel Ag & Co. Kgaa | Verfahren zum Befestigen eines Magneten auf oder in einem Rotor oder Stator |
| DE102009046157A1 (de) | 2009-10-29 | 2011-05-05 | Henkel Ag & Co. Kgaa | Vormischung und Verfahren zur Herstellung einer thermisch expandierbaren und härtbaren Epoxid-basierten Masse |
| DE102010028186A1 (de) | 2010-04-26 | 2011-10-27 | Evonik Röhm Gmbh | Fluoreszenzkonversionssolarzelle Lacke |
| DE102010028180A1 (de) | 2010-04-26 | 2011-10-27 | Evonik Röhm Gmbh | Fluoreszenzkonversionssolarzelle - Herstellung im Extrusionslaminationsverfahren oder im Kleberlaminationsverfahren |
| DE102010038685A1 (de) | 2010-07-30 | 2012-02-02 | Evonik Röhm Gmbh | Fluoreszenzkonversionssolarzelle Herstellung im Plattengußverfahren |
| EP2431424A3 (en) * | 2010-09-21 | 2014-03-05 | Rohm and Haas Company | UV - reflecting compositions |
| DE102010044116A1 (de) | 2010-10-05 | 2011-04-07 | Henkel Ag & Co. Kgaa | Verfahren zur Herstellung von Bauteilen |
| DE102010044115A1 (de) | 2010-11-18 | 2012-05-24 | Henkel Ag & Co. Kgaa | Verfahren zur Herstellung von Rollstühlen |
| DE102011007896A1 (de) | 2011-04-12 | 2012-10-18 | Henkel Ag & Co. Kgaa | Hybridmatrix für Faserverbundwerkstoffe |
| DE102012205057A1 (de) | 2012-03-29 | 2013-10-02 | Henkel Ag & Co. Kgaa | Thermisch expandierbare Zubereitungen |
| CN105524222B (zh) * | 2016-01-29 | 2018-01-16 | 江苏大学 | 用于纸质文物抗紫外聚合物材料的制备方法及其应用 |
| CN105713155B (zh) * | 2016-01-29 | 2017-12-05 | 江苏大学 | 用于纸质文物保护的聚合物材料的制备方法及其应用 |
| KR102246054B1 (ko) | 2016-03-18 | 2021-04-28 | 피피지 인더스트리즈 오하이오 인코포레이티드 | 다층 코팅 및 이의 제조 방법 |
| CN108779351A (zh) | 2016-03-18 | 2018-11-09 | Ppg工业俄亥俄公司 | 涂料组合物，由其形成的弹性阻隔涂层和该涂料的施涂方法 |
| PL3301138T5 (pl) † | 2016-09-30 | 2022-07-04 | Daw Se | Wodne masy do obróbki ścian, sufitów i podłóg budynków |
| JP6766260B2 (ja) * | 2016-11-04 | 2020-10-07 | キャボット コーポレイションＣａｂｏｔ Ｃｏｒｐｏｒａｔｉｏｎ | 結晶性ポリエステル及び有機シリカを含有するナノコンポジット |
| CN108287378B (zh) * | 2018-01-04 | 2019-10-15 | 复旦大学 | 透明复合光子晶体材料及其制备方法和应用 |
| CN108563836B (zh) * | 2018-03-21 | 2020-07-14 | 河海大学 | 一种凸形核-壳结构体排斥体积计算方法 |
| DK3894212T3 (da) * | 2020-02-18 | 2026-07-27 | Polyvantis Gmbh | Flerlags-acrylfolie med forbedrede mekaniske egenskaber og høj vejrbestandighed |
| EP4692145A1 (en) * | 2023-03-30 | 2026-02-11 | Kaneka Corporation | Polymer microparticles, resin modifier, and resin composition |
| KR102812508B1 (ko) * | 2024-10-04 | 2025-05-23 | 이혜경 | 미용 접착제 조성물 및 이의 제조방법 |
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| CA1188022A (en) * | 1981-02-25 | 1985-05-28 | Kazuo Kishida | Multi-layer structure polymer composition having an inner two-layer elastic polymer structure |
| DE3843371A1 (de) * | 1988-12-23 | 1990-07-05 | Basf Ag | Pfropfpolymerisate |
| JP3474223B2 (ja) * | 1993-06-14 | 2003-12-08 | 株式会社クラレ | アクリル系熱可塑性樹脂 |
| JP3339116B2 (ja) * | 1993-06-24 | 2002-10-28 | 株式会社クラレ | 熱可塑性アクリル系樹脂及びその製造方法 |
| JP3818689B2 (ja) * | 1996-01-16 | 2006-09-06 | 富士写真フイルム株式会社 | コロイド状シリカをコアとし、有機ポリマーをシェルとするコア／シェル状複合粒子の水性分散物及びその製造方法 |
| US7241502B2 (en) * | 2001-09-14 | 2007-07-10 | Merck Patentgesellschaft | Moulded bodies consisting of core-shell particles |
| DE10204338A1 (de) * | 2002-02-01 | 2003-08-14 | Merck Patent Gmbh | Formkörper aus Kern-Mantel-Partikeln |
| US7179531B2 (en) * | 2002-09-12 | 2007-02-20 | Rohm And Haas Company | Polymer particles having select pendant groups and composition prepared therefrom |
-
2004
- 2004-11-16 DE DE102004055303A patent/DE102004055303A1/de not_active Withdrawn
-
2005
- 2005-11-03 RU RU2007122279/04A patent/RU2007122279A/ru unknown
- 2005-11-03 JP JP2007541731A patent/JP2008520775A/ja active Pending
- 2005-11-03 CN CNA2005800391964A patent/CN101090920A/zh active Pending
- 2005-11-03 EP EP05807885A patent/EP1812484B1/de not_active Expired - Lifetime
- 2005-11-03 DE DE502005006171T patent/DE502005006171D1/de not_active Expired - Lifetime
- 2005-11-03 MX MX2007005911A patent/MX2007005911A/es unknown
- 2005-11-03 CA CA002587477A patent/CA2587477A1/en not_active Abandoned
- 2005-11-03 AT AT05807885T patent/ATE416206T1/de not_active IP Right Cessation
- 2005-11-03 KR KR1020077011011A patent/KR20070089129A/ko not_active Ceased
- 2005-11-03 WO PCT/EP2005/011740 patent/WO2006053640A1/de not_active Ceased
- 2005-11-03 BR BRPI0518335-9A patent/BRPI0518335A2/pt not_active IP Right Cessation
- 2005-11-14 TW TW094139920A patent/TW200631967A/zh unknown
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20180004375A (ko) * | 2016-07-01 | 2018-01-11 | 삼성디스플레이 주식회사 | 유기 발광 디스플레이 장치 및 이의 제조 방법 |
Also Published As
| Publication number | Publication date |
|---|---|
| DE502005006171D1 (de) | 2009-01-15 |
| DE102004055303A1 (de) | 2006-05-18 |
| ATE416206T1 (de) | 2008-12-15 |
| EP1812484B1 (de) | 2008-12-03 |
| WO2006053640A1 (de) | 2006-05-26 |
| CA2587477A1 (en) | 2006-05-26 |
| RU2007122279A (ru) | 2008-12-27 |
| BRPI0518335A2 (pt) | 2008-11-11 |
| EP1812484A1 (de) | 2007-08-01 |
| TW200631967A (en) | 2006-09-16 |
| CN101090920A (zh) | 2007-12-19 |
| JP2008520775A (ja) | 2008-06-19 |
| MX2007005911A (es) | 2007-06-20 |
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