KR102450069B1 - 폴리머 폴리올의 제조 방법 - Google Patents

폴리머 폴리올의 제조 방법 Download PDF

Info

Publication number
KR102450069B1
KR102450069B1 KR1020167033275A KR20167033275A KR102450069B1 KR 102450069 B1 KR102450069 B1 KR 102450069B1 KR 1020167033275 A KR1020167033275 A KR 1020167033275A KR 20167033275 A KR20167033275 A KR 20167033275A KR 102450069 B1 KR102450069 B1 KR 102450069B1
Authority
KR
South Korea
Prior art keywords
polyol
extruder
stabilizer
process according
rotor
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
KR1020167033275A
Other languages
English (en)
Korean (ko)
Other versions
KR20170002494A (ko
Inventor
크리스티안 쾨닉
데얀 페트로빅
아힘 뢰플러
안드레아스 보더
다니엘 프라이단크
더크 오페르만
다 폰세카 아이사 알렉산드라 케이로스
캐롤라인 마기스-사우터
추안 롱 푸
슈쿠이 왕
Original Assignee
바스프 에스이
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 바스프 에스이 filed Critical 바스프 에스이
Publication of KR20170002494A publication Critical patent/KR20170002494A/ko
Application granted granted Critical
Publication of KR102450069B1 publication Critical patent/KR102450069B1/ko
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/63—Block or graft polymers obtained by polymerising compounds having carbon-to-carbon double bonds on to polymers
    • C08G18/633—Block or graft polymers obtained by polymerising compounds having carbon-to-carbon double bonds on to polymers onto polymers of compounds having carbon-to-carbon double bonds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F257/00—Macromolecular compounds obtained by polymerising monomers on to polymers of aromatic monomers as defined in group C08F12/00
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/0838—Manufacture of polymers in the presence of non-reactive compounds
    • C08G18/0842—Manufacture of polymers in the presence of non-reactive compounds in the presence of liquid diluents
    • C08G18/0861—Manufacture of polymers in the presence of non-reactive compounds in the presence of liquid diluents in the presence of a dispersing phase for the polymers or a phase dispersed in the polymers
    • C08G18/0871—Manufacture of polymers in the presence of non-reactive compounds in the presence of liquid diluents in the presence of a dispersing phase for the polymers or a phase dispersed in the polymers the dispersing or dispersed phase being organic
    • C08G18/0876—Manufacture of polymers in the presence of non-reactive compounds in the presence of liquid diluents in the presence of a dispersing phase for the polymers or a phase dispersed in the polymers the dispersing or dispersed phase being organic the dispersing or dispersed phase being a polyol
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/63—Block or graft polymers obtained by polymerising compounds having carbon-to-carbon double bonds on to polymers
    • C08G18/636—Block or graft polymers obtained by polymerising compounds having carbon-to-carbon double bonds on to polymers characterised by the presence of a dispersion-stabiliser
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72—Polyisocyanates or polyisothiocyanates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00—Processes of treating or compounding macromolecular substances
    • C08J3/005—Processes for mixing polymers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00—Processes of treating or compounding macromolecular substances
    • C08J3/02—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
    • C08J3/09—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in organic liquids
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L71/00—Compositions of polyethers obtained by reactions forming an ether link in the main chain; Compositions of derivatives of such polymers
    • C08L71/02—Polyalkylene oxides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L75/00—Compositions of polyureas or polyurethanes; Compositions of derivatives of such polymers
    • C08L75/04—Polyurethanes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2205/00—Foams characterised by their properties
    • C08J2205/06—Flexible foams
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2371/00—Characterised by the use of polyethers obtained by reactions forming an ether link in the main chain; Derivatives of such polymers
    • C08J2371/02—Polyalkylene oxides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2425/00—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring; Derivatives of such polymers
    • C08J2425/02—Homopolymers or copolymers of hydrocarbons
    • C08J2425/04—Homopolymers or copolymers of styrene
    • C08J2425/08—Copolymers of styrene
    • C08J2425/12—Copolymers of styrene with unsaturated nitriles

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Dispersion Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Polymerisation Methods In General (AREA)
KR1020167033275A 2014-04-30 2015-04-20 폴리머 폴리올의 제조 방법 Active KR102450069B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP14166515.8 2014-04-30
EP14166515 2014-04-30
PCT/EP2015/058467 WO2015165761A1 (en) 2014-04-30 2015-04-20 Process for making a polymer polyol

Publications (2)

Publication Number Publication Date
KR20170002494A KR20170002494A (ko) 2017-01-06
KR102450069B1 true KR102450069B1 (ko) 2022-09-30

Family

ID=50677961

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020167033275A Active KR102450069B1 (ko) 2014-04-30 2015-04-20 폴리머 폴리올의 제조 방법

Country Status (11)

Country Link
US (1) US10370479B2 (cg-RX-API-DMAC7.html)
EP (1) EP3137529B1 (cg-RX-API-DMAC7.html)
JP (1) JP6715185B2 (cg-RX-API-DMAC7.html)
KR (1) KR102450069B1 (cg-RX-API-DMAC7.html)
CN (1) CN106459346B (cg-RX-API-DMAC7.html)
ES (1) ES2818108T3 (cg-RX-API-DMAC7.html)
HU (1) HUE050534T2 (cg-RX-API-DMAC7.html)
MX (1) MX384711B (cg-RX-API-DMAC7.html)
RU (1) RU2713651C2 (cg-RX-API-DMAC7.html)
SA (1) SA516380147B1 (cg-RX-API-DMAC7.html)
WO (1) WO2015165761A1 (cg-RX-API-DMAC7.html)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10472458B2 (en) * 2014-04-30 2019-11-12 Basf Se Stabilizer for polymer polyol production processes
CN110283308B (zh) * 2019-06-21 2024-12-03 南京金栖化工集团有限公司 一种用于合成聚合物多元醇的稳定剂的制备方法
CN112708037B (zh) * 2019-10-25 2022-07-12 中国石油化工股份有限公司 一种宽粒径分布聚合多元醇及制备方法与应用
JP7762701B2 (ja) 2020-07-08 2025-10-30 ダウ グローバル テクノロジーズ エルエルシー ポリマーポリオールを作製するための溶融分散プロセス
KR102832049B1 (ko) * 2022-06-14 2025-07-10 금호석유화학 주식회사 폴리머 폴리올 및 그 제조방법
CN120225585A (zh) * 2022-12-01 2025-06-27 Sika技术股份公司 具有可调节适用期的用于喷涂施用的双组分聚氨酯组合物

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007077396A (ja) 2005-09-09 2007-03-29 Bayer Material Science Llc 高ヒドロキシル価を特徴とする低粘度ポリマーポリオール
JP2010150547A (ja) 2008-12-23 2010-07-08 Bayer Material Science Llc 天然油ベースポリオールを含むポリマーポリオール、該ポリマーポリオールを含むポリウレタンフォーム、およびその製造方法

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB8410480D0 (en) 1984-04-24 1984-05-31 Bp Chem Int Ltd Preparation of polymer polyols
US5196476A (en) 1990-06-12 1993-03-23 Arco Chemical Technology, L.P. Polymer/polyol and preformed stabilizer systems
US5494957A (en) 1991-04-22 1996-02-27 The Dow Chemical Company Stabilizers for preparing polymer polyols, and process for preparing polymer polyols
CA2078318C (en) 1991-09-20 1999-04-13 Terry Lee Petzold Carbody to crawler connection
ES2148397T3 (es) * 1995-10-10 2000-10-16 Bayer Ag Procedimiento continuo para la preparacion de polioles polimericos de baja viscosidad, finamente divididos, muy estables, de pequeño tamaño medio de particulas.
BR9510656A (pt) 1995-10-23 1999-01-05 Polyol Int Bv Composição de poliol polimérico processo para a fabricação de uma composição de poliol polimérico composição para a preparação de uma espuma de poliuretano e espuma de poliuretano
US5854386A (en) * 1997-08-25 1998-12-29 Arco Chemical Technology, L.P. Stabilizers for polymer polyols
US6013731A (en) * 1997-12-16 2000-01-11 Arco Chemical Technology L.P. Stabilizer based on high molecular weight polyols having low monol content for polymer polyol production
EP1326923B1 (en) * 2000-10-05 2008-09-03 Dow Global Technologies Inc. Dispersion of a preformed polymer in a polyol
US6475588B1 (en) 2001-08-07 2002-11-05 General Electric Company Colored digital versatile disks
US7148288B2 (en) 2003-06-27 2006-12-12 Basf Corporation Process for formation of preformed stabilizer polyols
US20050085613A1 (en) 2003-10-16 2005-04-21 Adkins Rick L. Novel unsaturated macromers for preformed stabilizers and polymer polyols
RU2265031C1 (ru) * 2004-04-28 2005-11-27 Еганов Владимир Федорович Способ получения полимер-полиола, полиольной дисперсной композиции
US7759423B2 (en) * 2004-08-02 2010-07-20 Bayer Materialscience Llc Polymer polyols with ultra-high solids contents
EP2297219B1 (en) * 2008-06-19 2012-04-04 Dow Global Technologies LLC Melt dispersion process for making polymer polyols
US8146458B2 (en) * 2009-07-27 2012-04-03 Eaton Corporation Locking differential having improved torque capacity
BR112013028982B1 (pt) * 2011-05-12 2020-10-27 Dow Global Technologies Llc. processo para fazer um poliol polimérico estabilizante e poliol polimérico estabilizante

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007077396A (ja) 2005-09-09 2007-03-29 Bayer Material Science Llc 高ヒドロキシル価を特徴とする低粘度ポリマーポリオール
JP2010150547A (ja) 2008-12-23 2010-07-08 Bayer Material Science Llc 天然油ベースポリオールを含むポリマーポリオール、該ポリマーポリオールを含むポリウレタンフォーム、およびその製造方法

Also Published As

Publication number Publication date
JP2017514959A (ja) 2017-06-08
RU2016146803A3 (cg-RX-API-DMAC7.html) 2018-10-19
KR20170002494A (ko) 2017-01-06
RU2016146803A (ru) 2018-05-30
MX384711B (es) 2025-03-14
CN106459346B (zh) 2020-02-21
HUE050534T2 (hu) 2020-12-28
JP6715185B2 (ja) 2020-07-01
CN106459346A (zh) 2017-02-22
EP3137529B1 (en) 2020-06-17
ES2818108T3 (es) 2021-04-09
SA516380147B1 (ar) 2020-03-22
WO2015165761A1 (en) 2015-11-05
MX2016014296A (es) 2017-02-06
EP3137529A1 (en) 2017-03-08
US20170044297A1 (en) 2017-02-16
RU2713651C2 (ru) 2020-02-06
US10370479B2 (en) 2019-08-06

Similar Documents

Publication Publication Date Title
KR102450069B1 (ko) 폴리머 폴리올의 제조 방법
JP5368523B2 (ja) 微粒子分散ポリオールの製造方法及びポリウレタン樹脂の製造方法
CN102137881B (zh) 制备聚合物多元醇的熔体分散法
JP4862028B2 (ja) ポリマーポリオール、その製造方法及びポリウレタン樹脂の製造方法
CN101578309B (zh) 聚合物多元醇、其制造方法以及聚氨酯的制造方法
CN111448232B (zh) 胺基聚合物多元醇稳定剂
KR20140039219A (ko) 안정화제 중합 방법 및 중합체 폴리올의 제조 방법
CN101218299B (zh) 微粒分散多元醇组合物、聚合物多元醇的制造方法及聚氨酯树脂的制造方法
KR102447659B1 (ko) 불포화 폴리올 중 폴리머 폴리올의 합성, 폴리머 폴리올 및 이의 용도
JP2009040946A (ja) 重合体ポリオールの製造方法
JP4921324B2 (ja) 微粒子分散ポリオールの製造方法
JP2018162355A (ja) 硬質ポリウレタンフォーム用組成物及び硬質ポリウレタンフォームの製造方法
JP2010132738A (ja) 重合体ポリオール、この製造方法及びポリウレタン樹脂の製造方法
JP5415121B2 (ja) ポリマーポリオール及びポリウレタン樹脂の製造方法
JP5415098B2 (ja) 重合体ポリオール、この製造方法及びポリウレタン樹脂の製造方法
CN105622861A (zh) 一种连续制备聚合物多元醇的方法
WO2011152036A1 (ja) ポリマーポリオール及びポリウレタンの製造方法
JP2010031202A (ja) 重合体ポリオール、およびポリウレタン樹脂の製造方法

Legal Events

Date Code Title Description
PA0105 International application

St.27 status event code: A-0-1-A10-A15-nap-PA0105

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

PG1501 Laying open of application

St.27 status event code: A-1-1-Q10-Q12-nap-PG1501

R18-X000 Changes to party contact information recorded

St.27 status event code: A-3-3-R10-R18-oth-X000

R18-X000 Changes to party contact information recorded

St.27 status event code: A-3-3-R10-R18-oth-X000

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

PA0201 Request for examination

St.27 status event code: A-1-2-D10-D11-exm-PA0201

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

St.27 status event code: A-1-2-D10-D21-exm-PE0902

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

St.27 status event code: A-1-2-D10-D21-exm-PE0902

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

E701 Decision to grant or registration of patent right
PE0701 Decision of registration

St.27 status event code: A-1-2-D10-D22-exm-PE0701

GRNT Written decision to grant
PR0701 Registration of establishment

St.27 status event code: A-2-4-F10-F11-exm-PR0701

PR1002 Payment of registration fee

St.27 status event code: A-2-2-U10-U12-oth-PR1002

Fee payment year number: 1

PG1601 Publication of registration

St.27 status event code: A-4-4-Q10-Q13-nap-PG1601

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 4

U11 Full renewal or maintenance fee paid

Free format text: ST27 STATUS EVENT CODE: A-4-4-U10-U11-OTH-PR1001 (AS PROVIDED BY THE NATIONAL OFFICE)

Year of fee payment: 4