KR102057134B1 - 촉매를 사용한 탄소 재료의 제조 방법 및 탄소 재료 - Google Patents
촉매를 사용한 탄소 재료의 제조 방법 및 탄소 재료 Download PDFInfo
- Publication number
- KR102057134B1 KR102057134B1 KR1020147035288A KR20147035288A KR102057134B1 KR 102057134 B1 KR102057134 B1 KR 102057134B1 KR 1020147035288 A KR1020147035288 A KR 1020147035288A KR 20147035288 A KR20147035288 A KR 20147035288A KR 102057134 B1 KR102057134 B1 KR 102057134B1
- Authority
- KR
- South Korea
- Prior art keywords
- sulfonic acid
- cellulose
- carbon
- regenerated
- carbon material
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
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- 239000003575 carbonaceous material Substances 0.000 title claims abstract description 49
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 31
- 239000003054 catalyst Substances 0.000 title description 3
- 239000000463 material Substances 0.000 claims abstract description 106
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 claims abstract description 53
- 229920002678 cellulose Polymers 0.000 claims abstract description 53
- 239000001913 cellulose Substances 0.000 claims abstract description 53
- 239000004627 regenerated cellulose Substances 0.000 claims abstract description 33
- 239000011261 inert gas Substances 0.000 claims abstract description 15
- 238000003763 carbonization Methods 0.000 claims description 38
- 238000000034 method Methods 0.000 claims description 31
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 25
- JOXIMZWYDAKGHI-UHFFFAOYSA-N toluene-4-sulfonic acid Chemical compound CC1=CC=C(S(O)(=O)=O)C=C1 JOXIMZWYDAKGHI-UHFFFAOYSA-N 0.000 claims description 24
- 239000007864 aqueous solution Substances 0.000 claims description 21
- AFVFQIVMOAPDHO-UHFFFAOYSA-N Methanesulfonic acid Chemical compound CS(O)(=O)=O AFVFQIVMOAPDHO-UHFFFAOYSA-N 0.000 claims description 20
- 229910052799 carbon Inorganic materials 0.000 claims description 16
- 229940098779 methanesulfonic acid Drugs 0.000 claims description 10
- 239000004744 fabric Substances 0.000 claims description 9
- 239000002994 raw material Substances 0.000 claims description 7
- 238000003303 reheating Methods 0.000 claims description 5
- SRSXLGNVWSONIS-UHFFFAOYSA-N benzenesulfonic acid Chemical compound OS(=O)(=O)C1=CC=CC=C1 SRSXLGNVWSONIS-UHFFFAOYSA-N 0.000 claims description 4
- 229940092714 benzenesulfonic acid Drugs 0.000 claims description 4
- PSZYNBSKGUBXEH-UHFFFAOYSA-N naphthalene-1-sulfonic acid Chemical compound C1=CC=C2C(S(=O)(=O)O)=CC=CC2=C1 PSZYNBSKGUBXEH-UHFFFAOYSA-N 0.000 claims description 4
- MIOPJNTWMNEORI-GMSGAONNSA-N (S)-camphorsulfonic acid Chemical compound C1C[C@@]2(CS(O)(=O)=O)C(=O)C[C@@H]1C2(C)C MIOPJNTWMNEORI-GMSGAONNSA-N 0.000 claims description 3
- 239000000243 solution Substances 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 description 16
- 239000007789 gas Substances 0.000 description 14
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 12
- 238000001179 sorption measurement Methods 0.000 description 10
- 238000001035 drying Methods 0.000 description 7
- 229910052786 argon Inorganic materials 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 229920000742 Cotton Polymers 0.000 description 5
- 238000007654 immersion Methods 0.000 description 5
- 125000003118 aryl group Chemical group 0.000 description 4
- 229910002804 graphite Inorganic materials 0.000 description 4
- 239000010439 graphite Substances 0.000 description 4
- 229910052736 halogen Inorganic materials 0.000 description 4
- 150000002367 halogens Chemical class 0.000 description 4
- 244000198134 Agave sisalana Species 0.000 description 3
- 229920000049 Carbon (fiber) Polymers 0.000 description 3
- 125000000217 alkyl group Chemical group 0.000 description 3
- 125000004432 carbon atom Chemical group C* 0.000 description 3
- 239000004917 carbon fiber Substances 0.000 description 3
- 238000006297 dehydration reaction Methods 0.000 description 3
- 238000005087 graphitization Methods 0.000 description 3
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 125000000020 sulfo group Chemical group O=S(=O)([*])O[H] 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 2
- 229920002749 Bacterial cellulose Polymers 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 125000001931 aliphatic group Chemical group 0.000 description 2
- 239000005016 bacterial cellulose Substances 0.000 description 2
- 230000001580 bacterial effect Effects 0.000 description 2
- 238000010000 carbonizing Methods 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 125000000753 cycloalkyl group Chemical group 0.000 description 2
- 230000018044 dehydration Effects 0.000 description 2
- 230000001419 dependent effect Effects 0.000 description 2
- 238000006477 desulfuration reaction Methods 0.000 description 2
- 230000023556 desulfurization Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 238000000197 pyrolysis Methods 0.000 description 2
- 238000005979 thermal decomposition reaction Methods 0.000 description 2
- DIZBQMTZXOUFTD-UHFFFAOYSA-N 2-(furan-2-yl)-3h-benzimidazole-5-carboxylic acid Chemical compound N1C2=CC(C(=O)O)=CC=C2N=C1C1=CC=CO1 DIZBQMTZXOUFTD-UHFFFAOYSA-N 0.000 description 1
- 239000002028 Biomass Substances 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 241000723346 Cinnamomum camphora Species 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- 229960000846 camphor Drugs 0.000 description 1
- 229930008380 camphor Natural products 0.000 description 1
- -1 camphor sulfone Chemical class 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000004020 conductor Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- ZHGASCUQXLPSDT-UHFFFAOYSA-N cyclohexanesulfonic acid Chemical compound OS(=O)(=O)C1CCCCC1 ZHGASCUQXLPSDT-UHFFFAOYSA-N 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 239000007772 electrode material Substances 0.000 description 1
- CCIVGXIOQKPBKL-UHFFFAOYSA-M ethanesulfonate Chemical compound CCS([O-])(=O)=O CCIVGXIOQKPBKL-UHFFFAOYSA-M 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 150000004820 halides Chemical class 0.000 description 1
- 125000005843 halogen group Chemical group 0.000 description 1
- FYAQQULBLMNGAH-UHFFFAOYSA-N hexane-1-sulfonic acid Chemical compound CCCCCCS(O)(=O)=O FYAQQULBLMNGAH-UHFFFAOYSA-N 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 239000008104 plant cellulose Substances 0.000 description 1
- KCXFHTAICRTXLI-UHFFFAOYSA-N propane-1-sulfonic acid Chemical compound CCCS(O)(=O)=O KCXFHTAICRTXLI-UHFFFAOYSA-N 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000011232 storage material Substances 0.000 description 1
- 150000003460 sulfonic acids Chemical class 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- NLVXSWCKKBEXTG-UHFFFAOYSA-N vinylsulfonic acid Chemical compound OS(=O)(=O)C=C NLVXSWCKKBEXTG-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/05—Preparation or purification of carbon not covered by groups C01B32/15, C01B32/20, C01B32/25, C01B32/30
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
- D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
- D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
- D01F9/14—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
- D01F9/16—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from products of vegetable origin or derivatives thereof, e.g. from cellulose acetate
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/15—Nano-sized carbon materials
- C01B32/158—Carbon nanotubes
- C01B32/16—Preparation
- C01B32/162—Preparation characterised by catalysts
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M8/00—Fuel cells; Manufacture thereof
- H01M8/02—Details
- H01M8/0202—Collectors; Separators, e.g. bipolar separators; Interconnectors
- H01M8/023—Porous and characterised by the material
- H01M8/0234—Carbonaceous material
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/30—Hydrogen technology
- Y02E60/50—Fuel cells
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
- Y02P70/50—Manufacturing or production processes characterised by the final manufactured product
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Nanotechnology (AREA)
- General Chemical & Material Sciences (AREA)
- Textile Engineering (AREA)
- Carbon And Carbon Compounds (AREA)
- Catalysts (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JPJP-P-2012-128253 | 2012-06-05 | ||
| JP2012128253 | 2012-06-05 | ||
| PCT/JP2013/065579 WO2013183668A1 (ja) | 2012-06-05 | 2013-06-05 | 触媒を用いた炭素材料の製造方法および炭素材料 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR20150027757A KR20150027757A (ko) | 2015-03-12 |
| KR102057134B1 true KR102057134B1 (ko) | 2019-12-18 |
Family
ID=49712057
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020147035288A Active KR102057134B1 (ko) | 2012-06-05 | 2013-06-05 | 촉매를 사용한 탄소 재료의 제조 방법 및 탄소 재료 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US9523163B2 (enExample) |
| EP (1) | EP2857355B1 (enExample) |
| JP (1) | JP6156828B2 (enExample) |
| KR (1) | KR102057134B1 (enExample) |
| CN (1) | CN104428243B (enExample) |
| CA (1) | CA2875607C (enExample) |
| NO (1) | NO2857355T3 (enExample) |
| WO (1) | WO2013183668A1 (enExample) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2015193941A (ja) * | 2014-03-31 | 2015-11-05 | 日本製紙株式会社 | シート状炭素材料 |
| JP6657712B2 (ja) * | 2015-09-29 | 2020-03-04 | 日本製紙株式会社 | 炭素繊維及び炭素繊維シートの製造方法 |
| JP6604118B2 (ja) * | 2015-09-29 | 2019-11-13 | 日本製紙株式会社 | 炭素繊維シートの製造方法 |
| JP2017066540A (ja) * | 2015-09-29 | 2017-04-06 | 日本製紙株式会社 | 炭素繊維及び炭素繊維シートの製造方法 |
| JP2017101350A (ja) * | 2015-12-01 | 2017-06-08 | 旭化成株式会社 | キュプラ繊維材料を用いた炭素材料の製造方法 |
| KR102234017B1 (ko) * | 2016-12-29 | 2021-03-29 | 코오롱인더스트리 주식회사 | 펴짐성이 우수한 롤 타입 가스확산층의 제조방법 |
| JP7107801B2 (ja) * | 2018-09-27 | 2022-07-27 | 日本製紙株式会社 | 活性炭素繊維材料の製造方法 |
| JP7229788B2 (ja) * | 2019-01-22 | 2023-02-28 | 日本製紙株式会社 | 活性炭素繊維材料 |
| WO2020189632A1 (ja) * | 2019-03-20 | 2020-09-24 | ビタミンＣ６０バイオリサーチ株式会社 | 炭素クラスター製造用の成形体とその製造方法 |
| WO2022114040A1 (ja) * | 2020-11-26 | 2022-06-02 | 東レ株式会社 | ガス拡散電極基材製品および固体高分子型燃料電池 |
| CN114824343B (zh) * | 2022-04-07 | 2023-09-15 | 北京氢沄新能源科技有限公司 | 一种碳基复合材料双极板的制备方法、双极板和燃料电池 |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2009292676A (ja) * | 2008-06-04 | 2009-12-17 | Kazuo Akagi | 炭素材料の製造方法および炭素材料 |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS57188464A (en) * | 1981-05-11 | 1982-11-19 | Mitsubishi Pencil Co | Carbon spring and manufacture |
| US5102855A (en) * | 1990-07-20 | 1992-04-07 | Ucar Carbon Technology Corporation | Process for producing high surface area activated carbon |
| JPH04308670A (ja) * | 1991-04-05 | 1992-10-30 | Sanyo Electric Co Ltd | 二次電池 |
| US7541312B2 (en) * | 2004-03-18 | 2009-06-02 | Tda Research, Inc. | Porous carbons from carbohydrates |
| JP5162817B2 (ja) | 2005-08-26 | 2013-03-13 | 宇部興産株式会社 | ネットワーク状炭素材料 |
| KR100924214B1 (ko) * | 2006-12-08 | 2009-10-29 | 주식회사 엘지화학 | 분무 건조 또는 분무 열분해를 이용한 중형 다공성 탄소구조체의 제조 방법 및 분무 건조용 조성물 |
| JP5339453B2 (ja) * | 2007-05-11 | 2013-11-13 | Ｊｘ日鉱日石エネルギー株式会社 | スルホン酸基含有炭素質材料の製造方法、固体酸触媒、アルキル化反応生成物の製造方法、およびオレフィン重合体の製造方法 |
| CN101463578A (zh) * | 2007-12-19 | 2009-06-24 | 逢甲大学 | 高强度碳化纸及其制备方法与用途 |
| KR101045001B1 (ko) | 2008-09-30 | 2011-06-29 | 한국과학기술원 | 녹말을 이용한 탄소나노튜브가 강화된 다공성 탄소섬유의 제조방법 및 전기화학용 전극소재 용도 |
| JP5599029B2 (ja) * | 2009-11-25 | 2014-10-01 | 国立大学法人 筑波大学 | 燃料電池用ガス拡散層 |
-
2013
- 2013-06-05 NO NO13801452A patent/NO2857355T3/no unknown
- 2013-06-05 WO PCT/JP2013/065579 patent/WO2013183668A1/ja not_active Ceased
- 2013-06-05 JP JP2014520027A patent/JP6156828B2/ja active Active
- 2013-06-05 CN CN201380029853.1A patent/CN104428243B/zh active Active
- 2013-06-05 US US14/405,650 patent/US9523163B2/en active Active
- 2013-06-05 KR KR1020147035288A patent/KR102057134B1/ko active Active
- 2013-06-05 EP EP13801452.7A patent/EP2857355B1/en not_active Not-in-force
- 2013-06-05 CA CA2875607A patent/CA2875607C/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2009292676A (ja) * | 2008-06-04 | 2009-12-17 | Kazuo Akagi | 炭素材料の製造方法および炭素材料 |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104428243A (zh) | 2015-03-18 |
| NO2857355T3 (enExample) | 2018-10-06 |
| KR20150027757A (ko) | 2015-03-12 |
| JP6156828B2 (ja) | 2017-07-05 |
| US9523163B2 (en) | 2016-12-20 |
| JPWO2013183668A1 (ja) | 2016-02-01 |
| CA2875607A1 (en) | 2013-12-12 |
| US20150167200A1 (en) | 2015-06-18 |
| WO2013183668A1 (ja) | 2013-12-12 |
| EP2857355A4 (en) | 2016-02-24 |
| EP2857355B1 (en) | 2018-05-09 |
| CN104428243B (zh) | 2017-07-04 |
| CA2875607C (en) | 2020-05-12 |
| EP2857355A1 (en) | 2015-04-08 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PA0105 | International application |
Patent event date: 20141216 Patent event code: PA01051R01D Comment text: International Patent Application |
|
| PG1501 | Laying open of application | ||
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