KR101903362B1 - 전이 금속 수산화물의 제조 방법 - Google Patents

전이 금속 수산화물의 제조 방법 Download PDF

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KR101903362B1
KR101903362B1 KR1020137021135A KR20137021135A KR101903362B1 KR 101903362 B1 KR101903362 B1 KR 101903362B1 KR 1020137021135 A KR1020137021135 A KR 1020137021135A KR 20137021135 A KR20137021135 A KR 20137021135A KR 101903362 B1 KR101903362 B1 KR 101903362B1
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transition metal
present
range
suspension
metal hydroxide
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KR20140047577A (ko
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우베 클리펠스
지몬 슈뢰들레
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바스프 에스이
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B13/00—Oxygen; Ozone; Oxides or hydroxides in general
    • C01B13/14—Methods for preparing oxides or hydroxides in general
    • C01B13/36—Methods for preparing oxides or hydroxides in general by precipitation reactions in aqueous solutions
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/80—Compounds containing nickel, with or without oxygen or hydrogen, and containing one or more other elements
    • C01G53/82—Compounds containing nickel, with or without oxygen or hydrogen, and containing two or more other elements
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G51/00—Compounds of cobalt
    • C01G51/80—Compounds containing cobalt, with or without oxygen or hydrogen, and containing one or more other elements
    • C01G51/82—Compounds containing cobalt, with or without oxygen or hydrogen, and containing two or more other elements
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/50—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
    • H01M4/505—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/52—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
    • H01M4/525—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/50—Solid solutions
    • C01P2002/52—Solid solutions containing elements as dopants
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/30—Particle morphology extending in three dimensions
    • C01P2004/32—Spheres
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/51—Particles with a specific particle size distribution
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/11—Powder tap density
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/16—Pore diameter
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Oxygen, Ozone, And Oxides In General (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
KR1020137021135A 2011-01-10 2012-01-09 전이 금속 수산화물의 제조 방법 Active KR101903362B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP11150470.0 2011-01-10
EP11150470 2011-01-10
PCT/EP2012/050219 WO2012095381A2 (de) 2011-01-10 2012-01-09 Verfahren zur herstellung von übergangsmetallhydroxiden

Publications (2)

Publication Number Publication Date
KR20140047577A KR20140047577A (ko) 2014-04-22
KR101903362B1 true KR101903362B1 (ko) 2018-10-02

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KR1020137021135A Active KR101903362B1 (ko) 2011-01-10 2012-01-09 전이 금속 수산화물의 제조 방법

Country Status (6)

Country Link
EP (1) EP2663527B1 (cg-RX-API-DMAC7.html)
JP (1) JP5872587B2 (cg-RX-API-DMAC7.html)
KR (1) KR101903362B1 (cg-RX-API-DMAC7.html)
CN (1) CN103282310B (cg-RX-API-DMAC7.html)
TW (1) TW201236978A (cg-RX-API-DMAC7.html)
WO (1) WO2012095381A2 (cg-RX-API-DMAC7.html)

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8394299B2 (en) * 2008-04-03 2013-03-12 Lg Chem, Ltd. Precursor for the preparation of a lithium composite transition metal oxide
KR101575024B1 (ko) * 2013-02-13 2015-12-07 주식회사 엘지화학 낮은 탭 밀도를 갖는 전이금속 전구체 및 높은 입자 강도를 가진 리튬 전이금속 산화물
WO2017119451A1 (ja) * 2016-01-06 2017-07-13 住友金属鉱山株式会社 非水系電解質二次電池用正極活物質前駆体、非水系電解質二次電池用正極活物質、非水系電解質二次電池用正極活物質前駆体の製造方法、非水系電解質二次電池用正極活物質の製造方法
US20190013519A1 (en) 2016-01-06 2019-01-10 Sumitomo Metal Mining Co., Ltd. Positive-electrode active material precursor for nonaqueous electrolyte secondary battery, positive-electrode active material for nonaqueous electrolyte secondary battery, method for manufacturing positive-electrode active material precursor for nonaqueous electrolyte secondary battery, and method for manufacturing positive-electrode active material for nonaqueous electrolyte secondary battery
EP3281915B1 (en) * 2016-08-10 2019-02-20 Umicore Precursors for lithium transition metal oxide cathode materials for rechargeable batteries
US11919783B2 (en) 2017-06-23 2024-03-05 Umicore Beta-nickel hydroxide doped with aluminum
CN108511671B (zh) * 2018-03-12 2021-04-06 中国科学院长春应用化学研究所 一种柔性电极及其制备方法、巨能柔性即用即制储电器件
FI3774018T3 (fi) 2018-03-27 2023-10-17 Basf Se Menetelmä karbonaatin tai (oksi)hydroksidin saostamiseksi
CN109354077B (zh) * 2018-10-16 2021-05-07 中伟新材料股份有限公司 一种多结晶形态的三元前驱体及其制备方法
EP3659974A1 (en) * 2018-11-27 2020-06-03 Basf Se Process for making a nickel composite hydroxide
EP3659975A1 (en) * 2018-11-28 2020-06-03 Basf Se Process for the manufacture of a nickel composite hydroxide
JP7721450B2 (ja) 2019-04-10 2025-08-12 ビーエーエスエフ ソシエタス・ヨーロピア 混合水酸化物を沈殿させる方法、及びその水酸化物から製造した正極活物質
EP4038019B1 (en) 2019-10-01 2023-11-08 Basf Se Process for precipitating a mixed carbonate or mixed (oxy)hydroxide
KR20230051180A (ko) 2020-08-13 2023-04-17 바스프 에스이 혼합 수산화물을 침전시키기 위한 방법
PL4229008T3 (pl) 2020-10-13 2024-11-25 Basf Se Sposób wytwarzania (tleno)wodorotlenku w postaci cząstek i (tleno)wodorotlenek i jego zastosowanie
CA3204235A1 (en) * 2021-01-20 2022-07-28 Benjamin Johannes Herbert BERGNER Process for making a particulate (oxy)hydroxide

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009531173A (ja) * 2006-03-31 2009-09-03 ハー．ツェー．スタルク ゲゼルシャフト ミット ベシュレンクテル ハフツング 沈殿により化合物を製造するための装置及び方法
CN101857278A (zh) 2010-06-25 2010-10-13 浙江华友钴业股份有限公司 一种球形碳酸盐的制备方法

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3092222B2 (ja) * 1991-07-08 2000-09-25 松下電器産業株式会社 水酸化ニッケル活物質およびニッケル正極とこれを用いたアルカリ蓄電池
JP3136668B2 (ja) * 1991-07-08 2001-02-19 松下電器産業株式会社 水酸化ニッケル活物質粉末およびニッケル正極とこれを用いたアルカリ蓄電池
US5700596A (en) * 1991-07-08 1997-12-23 Matsushita Electric Industrial Co., Ltd. Nickel hydroxide active material powder and nickel positive electrode and alkali storage battery using them
JP3644186B2 (ja) * 1997-03-24 2005-04-27 松下電器産業株式会社 電池構成用金属水酸化物製造装置
US6660432B2 (en) 2000-09-14 2003-12-09 Ilion Technology Corporation Lithiated oxide materials and methods of manufacture
CN1798699B (zh) * 2003-05-30 2010-11-10 杰富意矿物股份有限公司 金属复合氧化物的制造方法
JP4929674B2 (ja) * 2004-10-27 2012-05-09 住友化学株式会社 球状ニッケル酸リチウム粒子の製造方法および球状の複合酸化物粒子の製造方法
DE102006049107A1 (de) * 2006-10-13 2008-04-17 H.C. Starck Gmbh Pulverförmige Verbindungen, Verfahren zu deren Herstellung sowie deren Verwendung in elektrochemischen Anwendungen
JP5251332B2 (ja) * 2007-07-30 2013-07-31 住友金属鉱山株式会社 非水系電解質二次電池用正極活物質およびその製造方法、並びにこれを用いた非水系電解質二次電池
DE102007039471A1 (de) * 2007-08-21 2009-02-26 H.C. Starck Gmbh Pulverförmige Verbindungen, Verfahren zu deren Herstellung sowie deren Verwendung in Lithium-Sekundärbatterien
JP4877660B2 (ja) * 2008-09-30 2012-02-15 株式会社Ｇｓユアサ リチウム二次電池用活物質、その製造方法及びリチウム二次電池
WO2009063838A1 (ja) * 2007-11-12 2009-05-22 Gs Yuasa Corporation リチウム二次電池用活物質、リチウム二次電池及びその製造方法
JP2011057518A (ja) * 2009-09-11 2011-03-24 Kansai Shokubai Kagaku Kk 高密度ニッケル・コバルト・マンガン共沈水酸化物及びその製造方法

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009531173A (ja) * 2006-03-31 2009-09-03 ハー．ツェー．スタルク ゲゼルシャフト ミット ベシュレンクテル ハフツング 沈殿により化合物を製造するための装置及び方法
CN101857278A (zh) 2010-06-25 2010-10-13 浙江华友钴业股份有限公司 一种球形碳酸盐的制备方法

Also Published As

Publication number Publication date
CN103282310A (zh) 2013-09-04
KR20140047577A (ko) 2014-04-22
JP2014510004A (ja) 2014-04-24
WO2012095381A3 (de) 2012-11-15
CN103282310B (zh) 2015-04-29
EP2663527A2 (de) 2013-11-20
TW201236978A (en) 2012-09-16
WO2012095381A2 (de) 2012-07-19
JP5872587B2 (ja) 2016-03-01
EP2663527B1 (de) 2014-11-19

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