KR101818094B1 - 방향족 아민을 주성분으로 하는 개선된 다공성 물질 - Google Patents

방향족 아민을 주성분으로 하는 개선된 다공성 물질 Download PDF

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Publication number
KR101818094B1
KR101818094B1 KR1020127017952A KR20127017952A KR101818094B1 KR 101818094 B1 KR101818094 B1 KR 101818094B1 KR 1020127017952 A KR1020127017952 A KR 1020127017952A KR 20127017952 A KR20127017952 A KR 20127017952A KR 101818094 B1 KR101818094 B1 KR 101818094B1
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KR
South Korea
Prior art keywords
porous material
gel
component
diaminodiphenylmethane
amine
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Expired - Fee Related
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KR1020127017952A
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English (en)
Korean (ko)
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KR20120103700A (ko
Inventor
마르크 프릭케
마르크 엘빙
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바스프 에스이
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30—Low-molecular-weight compounds
    • C08G18/32—Polyhydroxy compounds; Polyamines; Hydroxyamines
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30—Low-molecular-weight compounds
    • C08G18/32—Polyhydroxy compounds; Polyamines; Hydroxyamines
    • C08G18/3225—Polyamines
    • C08G18/3237—Polyamines aromatic
    • C08G18/3243—Polyamines aromatic containing two or more aromatic rings
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • C08J9/28—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof by elimination of a liquid phase from a macromolecular composition or article, e.g. drying of coagulum
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • C08J9/28—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof by elimination of a liquid phase from a macromolecular composition or article, e.g. drying of coagulum
    • C08J9/286—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof by elimination of a liquid phase from a macromolecular composition or article, e.g. drying of coagulum the liquid phase being a solvent for the monomers but not for the resulting macromolecular composition, i.e. macroporous or macroreticular polymers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00—Foam properties
    • C08G2110/0091—Aerogels; Xerogels
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2330/00—Thermal insulation material
    • C08G2330/50—Evacuated open-celled polymer material
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2201/00—Foams characterised by the foaming process
    • C08J2201/04—Foams characterised by the foaming process characterised by the elimination of a liquid or solid component, e.g. precipitation, leaching out, evaporation
    • C08J2201/05—Elimination by evaporation or heat degradation of a liquid phase
    • C08J2201/0502—Elimination by evaporation or heat degradation of a liquid phase the liquid phase being organic
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2375/00—Characterised by the use of polyureas or polyurethanes; Derivatives of such polymers
    • C08J2375/02—Polyureas

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
KR1020127017952A 2009-12-11 2010-12-06 방향족 아민을 주성분으로 하는 개선된 다공성 물질 Expired - Fee Related KR101818094B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP09178783 2009-12-11
EP09178783.8 2009-12-11
PCT/EP2010/068962 WO2011069959A2 (de) 2009-12-11 2010-12-06 Verbesserte poröse materialien auf basis von aromatischen aminen

Publications (2)

Publication Number Publication Date
KR20120103700A KR20120103700A (ko) 2012-09-19
KR101818094B1 true KR101818094B1 (ko) 2018-01-12

Family

ID=44065451

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020127017952A Expired - Fee Related KR101818094B1 (ko) 2009-12-11 2010-12-06 방향족 아민을 주성분으로 하는 개선된 다공성 물질

Country Status (14)

Country Link
US (1) US11078320B2 (enExample)
EP (1) EP2510026B1 (enExample)
JP (1) JP5770202B2 (enExample)
KR (1) KR101818094B1 (enExample)
CN (1) CN102652145B (enExample)
AU (1) AU2010330056B2 (enExample)
CA (1) CA2783139C (enExample)
DK (1) DK2510026T3 (enExample)
ES (1) ES2454615T3 (enExample)
MX (1) MX2012006475A (enExample)
PL (1) PL2510026T3 (enExample)
PT (1) PT2510026E (enExample)
RU (1) RU2544242C2 (enExample)
WO (1) WO2011069959A2 (enExample)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2448986B1 (de) * 2009-06-29 2013-11-20 Basf Se Poröse gele auf basis von aromatischem polyharnstoff
US9260580B2 (en) 2010-06-28 2016-02-16 Basf Se Process for producing porous materials based on polyurea
KR101883022B1 (ko) * 2010-11-04 2018-07-27 바스프 에스이 에어로겔 또는 크세로겔을 제조하는 방법
US8697766B2 (en) 2011-02-24 2014-04-15 Basf Se Process for producing pulverulent porous materials
US20120235070A1 (en) 2011-03-18 2012-09-20 Basf Se Process for producing flame-retardant porous materials based on polyurea
US9188384B2 (en) 2011-03-31 2015-11-17 Basf Se Dynamically evacuable devices comprising organic aerogels or xerogels
US9321876B2 (en) 2012-09-27 2016-04-26 Basf Se Process for producing porous materials based on isocyanate
WO2014048778A1 (de) 2012-09-27 2014-04-03 Basf Se Verfahren zur herstellung von porösen materialien auf basis von isocyanat
WO2014187710A1 (en) 2013-05-24 2014-11-27 Basf Se Process for producing porous materials
US10717841B2 (en) 2014-03-24 2020-07-21 Basf Se Process for producing porous materials
EP3169724B1 (en) * 2014-07-18 2021-05-26 Basf Se Process for producing porous materials
CN115816812A (zh) 2014-09-25 2023-03-21 巴斯夫欧洲公司 用于真空绝热元件的复合元件的制造方法
US10907024B2 (en) 2015-03-24 2021-02-02 Basf Se Process for producing porous materials
RU2677891C1 (ru) 2015-04-27 2019-01-22 Хантсмэн Интернэшнл Ллс Функционализированные пористые материалы на основе изоцианата
MX2018001399A (es) * 2015-08-06 2018-04-13 Huntsman Int Llc Xerogeles organicos a base de isocianato con densidad reducida.
KR20180069864A (ko) 2015-10-16 2018-06-25 바스프 에스이 무기산을 사용한 이소시아네이트에 기초한 크세로겔 및 에어로겔의 제조 방법
EP3405508A1 (en) 2016-01-18 2018-11-28 Basf Se Process for producing porous materials
WO2017125414A1 (en) 2016-01-18 2017-07-27 Basf Se Process for producing porous materials
US20210139662A1 (en) 2017-07-13 2021-05-13 Basf Se Porous materials with superior reversible water uptake
US12054578B2 (en) 2017-07-17 2024-08-06 Aerogel-It Gmbh Process for producing porous materials
CN113302232A (zh) 2019-01-17 2021-08-24 巴斯夫欧洲公司 制备多孔材料的方法

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2008138978A1 (de) * 2007-05-16 2008-11-20 Basf Se Xerogele auf basis von aromatischem polyharnstoff
WO2009027310A1 (de) * 2007-08-28 2009-03-05 Basf Se Xerogele auf basis von polyharnstoff

Family Cites Families (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE791310A (fr) * 1971-11-13 1973-05-14 Bayer Ag Procede de preparation de pieces moulees en mousse
DE3613973A1 (de) * 1986-04-25 1987-10-29 Bayer Ag Verfahren zur herstellung von polyharnstoffschaum-formteilen
AU605860B2 (en) * 1987-04-07 1991-01-24 Dow Chemical Company, The Flexible polyurea or polyurea-polyurethane foams prepared from high equivalent weight amine-terminated compounds and process for preparing the same
EP0288067A1 (en) * 1987-04-24 1988-10-26 Asahi Glass Company Ltd. Process for producing polyurethane elastomer and compositon as starting material therefor
US4950404A (en) * 1989-08-30 1990-08-21 Allied-Signal Inc. High flux semipermeable membranes
US5478867A (en) 1993-07-07 1995-12-26 The Dow Chemical Company Microporous isocyanate-based polymer compositions and method of preparation
US5622777A (en) * 1995-05-17 1997-04-22 Bayer Corporation Heat-resistant reinforced foam
NZ320275A (en) * 1995-11-01 1999-09-29 Basf Corp A method of making insulating polyisocyanate rigid foams, and polyol composition
JP3112250B2 (ja) * 1996-07-31 2000-11-27 アイシーケイ株式会社 現場施工用ポリウレタン系防水塗膜形成材料
JPH10195163A (ja) * 1996-11-14 1998-07-28 Asahi Glass Co Ltd 二液型硬化性組成物
US5762829A (en) * 1997-03-05 1998-06-09 Armstrong World Industries, Inc. Wet silica gels for aerogel and xerogel thermal insulation and processes for the wet gels
US5821275A (en) * 1997-11-10 1998-10-13 Bayer Corporation Flexible foams and flexible molded foams based on liquid isocyanate-terminated allophanate-modified MDI prepolymer blends and processes for the production of these foams
JP2001329037A (ja) * 2000-05-24 2001-11-27 Matsushita Refrig Co Ltd 有機多孔体断熱材とその製造方法、および、断熱箱体
EP1178063A1 (en) * 2000-08-01 2002-02-06 Huntsman International Llc Process for preparing a polyurethane material
RU2184126C2 (ru) * 2000-08-15 2002-06-27 Хозин Вадим Григорьевич Связующее для теплоизоляционного материала и способ изготовления теплоизоляционного материала
ATE482245T1 (de) * 2007-05-16 2010-10-15 Basf Se Verfahren zur herstellung von organischen xerogelen
US20120022179A1 (en) 2009-01-20 2012-01-26 Basf Se Process for producing rigid polyurethane foams
JP2012520386A (ja) 2009-03-16 2012-09-06 ビーエーエスエフ ソシエタス・ヨーロピア キセロゲル複合材料の製造方法
EP2448986B1 (de) 2009-06-29 2013-11-20 Basf Se Poröse gele auf basis von aromatischem polyharnstoff

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2008138978A1 (de) * 2007-05-16 2008-11-20 Basf Se Xerogele auf basis von aromatischem polyharnstoff
WO2009027310A1 (de) * 2007-08-28 2009-03-05 Basf Se Xerogele auf basis von polyharnstoff

Also Published As

Publication number Publication date
AU2010330056B2 (en) 2015-03-26
EP2510026B1 (de) 2014-02-26
CN102652145A (zh) 2012-08-29
RU2544242C2 (ru) 2015-03-20
RU2012128928A (ru) 2014-01-20
WO2011069959A3 (de) 2011-12-01
CN102652145B (zh) 2014-04-16
JP5770202B2 (ja) 2015-08-26
DK2510026T3 (da) 2014-05-26
ES2454615T3 (es) 2014-04-11
CA2783139A1 (en) 2011-06-16
JP2013513675A (ja) 2013-04-22
MX2012006475A (es) 2012-06-28
CA2783139C (en) 2018-01-09
US20120305827A1 (en) 2012-12-06
WO2011069959A2 (de) 2011-06-16
AU2010330056A1 (en) 2012-07-05
US11078320B2 (en) 2021-08-03
PL2510026T3 (pl) 2014-07-31
EP2510026A2 (de) 2012-10-17
PT2510026E (pt) 2014-04-02
KR20120103700A (ko) 2012-09-19

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