KR101818094B1 - 방향족 아민을 주성분으로 하는 개선된 다공성 물질 - Google Patents

방향족 아민을 주성분으로 하는 개선된 다공성 물질 Download PDF

Info

Publication number
KR101818094B1
KR101818094B1 KR1020127017952A KR20127017952A KR101818094B1 KR 101818094 B1 KR101818094 B1 KR 101818094B1 KR 1020127017952 A KR1020127017952 A KR 1020127017952A KR 20127017952 A KR20127017952 A KR 20127017952A KR 101818094 B1 KR101818094 B1 KR 101818094B1
Authority
KR
South Korea
Prior art keywords
porous material
gel
component
diaminodiphenylmethane
amine
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
KR1020127017952A
Other languages
English (en)
Korean (ko)
Other versions
KR20120103700A (ko
Inventor
마르크 프릭케
마르크 엘빙
Original Assignee
바스프 에스이
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 바스프 에스이 filed Critical 바스프 에스이
Publication of KR20120103700A publication Critical patent/KR20120103700A/ko
Application granted granted Critical
Publication of KR101818094B1 publication Critical patent/KR101818094B1/ko
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30—Low-molecular-weight compounds
    • C08G18/32—Polyhydroxy compounds; Polyamines; Hydroxyamines
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30—Low-molecular-weight compounds
    • C08G18/32—Polyhydroxy compounds; Polyamines; Hydroxyamines
    • C08G18/3225—Polyamines
    • C08G18/3237—Polyamines aromatic
    • C08G18/3243—Polyamines aromatic containing two or more aromatic rings
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • C08J9/28—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof by elimination of a liquid phase from a macromolecular composition or article, e.g. drying of coagulum
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • C08J9/28—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof by elimination of a liquid phase from a macromolecular composition or article, e.g. drying of coagulum
    • C08J9/286—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof by elimination of a liquid phase from a macromolecular composition or article, e.g. drying of coagulum the liquid phase being a solvent for the monomers but not for the resulting macromolecular composition, i.e. macroporous or macroreticular polymers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00—Foam properties
    • C08G2110/0091—Aerogels; Xerogels
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2330/00—Thermal insulation material
    • C08G2330/50—Evacuated open-celled polymer material
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2201/00—Foams characterised by the foaming process
    • C08J2201/04—Foams characterised by the foaming process characterised by the elimination of a liquid or solid component, e.g. precipitation, leaching out, evaporation
    • C08J2201/05—Elimination by evaporation or heat degradation of a liquid phase
    • C08J2201/0502—Elimination by evaporation or heat degradation of a liquid phase the liquid phase being organic
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2375/00—Characterised by the use of polyureas or polyurethanes; Derivatives of such polymers
    • C08J2375/02—Polyureas

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
KR1020127017952A 2009-12-11 2010-12-06 방향족 아민을 주성분으로 하는 개선된 다공성 물질 Expired - Fee Related KR101818094B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP09178783 2009-12-11
EP09178783.8 2009-12-11
PCT/EP2010/068962 WO2011069959A2 (de) 2009-12-11 2010-12-06 Verbesserte poröse materialien auf basis von aromatischen aminen

Publications (2)

Publication Number Publication Date
KR20120103700A KR20120103700A (ko) 2012-09-19
KR101818094B1 true KR101818094B1 (ko) 2018-01-12

Family

ID=44065451

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020127017952A Expired - Fee Related KR101818094B1 (ko) 2009-12-11 2010-12-06 방향족 아민을 주성분으로 하는 개선된 다공성 물질

Country Status (14)

Country Link
US (1) US11078320B2 (enExample)
EP (1) EP2510026B1 (enExample)
JP (1) JP5770202B2 (enExample)
KR (1) KR101818094B1 (enExample)
CN (1) CN102652145B (enExample)
AU (1) AU2010330056B2 (enExample)
CA (1) CA2783139C (enExample)
DK (1) DK2510026T3 (enExample)
ES (1) ES2454615T3 (enExample)
MX (1) MX2012006475A (enExample)
PL (1) PL2510026T3 (enExample)
PT (1) PT2510026E (enExample)
RU (1) RU2544242C2 (enExample)
WO (1) WO2011069959A2 (enExample)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ES2439047T3 (es) * 2009-06-29 2014-01-21 Basf Se Geles porosos a base de poliurea aromática
US9260580B2 (en) 2010-06-28 2016-02-16 Basf Se Process for producing porous materials based on polyurea
PL2635616T3 (pl) * 2010-11-04 2018-01-31 Basf Se Sposób wytwarzania aerożeli lub kserożeli
US8697766B2 (en) 2011-02-24 2014-04-15 Basf Se Process for producing pulverulent porous materials
US20120235070A1 (en) 2011-03-18 2012-09-20 Basf Se Process for producing flame-retardant porous materials based on polyurea
US9188384B2 (en) 2011-03-31 2015-11-17 Basf Se Dynamically evacuable devices comprising organic aerogels or xerogels
US9321876B2 (en) 2012-09-27 2016-04-26 Basf Se Process for producing porous materials based on isocyanate
WO2014048778A1 (de) 2012-09-27 2014-04-03 Basf Se Verfahren zur herstellung von porösen materialien auf basis von isocyanat
CN105408381B (zh) * 2013-05-24 2018-04-24 巴斯夫欧洲公司 制备多孔材料的方法
WO2015144698A1 (en) 2014-03-24 2015-10-01 Basf Se Process for producing porous materials
CN106795315B (zh) 2014-07-18 2020-08-14 巴斯夫欧洲公司 制备多孔材料的方法
CA2962110C (en) 2014-09-25 2023-03-21 Basf Se Method for manufacturing a composite element for vacuum insulation elements
US10907024B2 (en) 2015-03-24 2021-02-02 Basf Se Process for producing porous materials
EP3288996B2 (en) 2015-04-27 2022-11-30 Huntsman International LLC Functionalized isocyanate based porous materials
BR112018002411A2 (pt) * 2015-08-06 2018-09-18 Huntsman Int Llc método de síntese para fabricar um xerogel orgânico com base em isocianato, e, uso do xerogel orgânico com base em isocianato
US10759893B2 (en) 2015-10-16 2020-09-01 Basf Se Process for producing isocyanate-based xerogels and aerogels with mineral acids
KR20180103131A (ko) 2016-01-18 2018-09-18 바스프 에스이 다공성 재료의 제조 방법
CN108473658B (zh) 2016-01-18 2022-08-26 巴斯夫欧洲公司 制备多孔材料的方法
EP3652231A1 (en) 2017-07-13 2020-05-20 Basf Se Porous materials with superior reversible water uptake
KR102781225B1 (ko) 2017-07-17 2025-03-12 에어로젤-잇 게엠베하 다공성 물질의 제조 방법
KR20210116570A (ko) 2019-01-17 2021-09-27 바스프 에스이 다공성 물질의 제조 방법

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2008138978A1 (de) * 2007-05-16 2008-11-20 Basf Se Xerogele auf basis von aromatischem polyharnstoff
WO2009027310A1 (de) * 2007-08-28 2009-03-05 Basf Se Xerogele auf basis von polyharnstoff

Family Cites Families (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE791310A (fr) * 1971-11-13 1973-05-14 Bayer Ag Procede de preparation de pieces moulees en mousse
DE3613973A1 (de) * 1986-04-25 1987-10-29 Bayer Ag Verfahren zur herstellung von polyharnstoffschaum-formteilen
JPH06102710B2 (ja) * 1987-04-07 1994-12-14 ザ ダウ ケミカル カンパニー 高当量アミン末端化合物より製造された軟質ポリウレアもしくはポリウレア‐ポリウレタンフォームおよびその製造方法
EP0288067A1 (en) 1987-04-24 1988-10-26 Asahi Glass Company Ltd. Process for producing polyurethane elastomer and compositon as starting material therefor
US4950404A (en) * 1989-08-30 1990-08-21 Allied-Signal Inc. High flux semipermeable membranes
US5478867A (en) 1993-07-07 1995-12-26 The Dow Chemical Company Microporous isocyanate-based polymer compositions and method of preparation
US5622777A (en) * 1995-05-17 1997-04-22 Bayer Corporation Heat-resistant reinforced foam
BR9611205A (pt) * 1995-11-01 1999-03-30 Basf Corp Processo de produção de uma espuma de célula fechada rígida à base de poliisocianato e composição de poliol estável em armazenamento
JP3112250B2 (ja) * 1996-07-31 2000-11-27 アイシーケイ株式会社 現場施工用ポリウレタン系防水塗膜形成材料
JPH10195163A (ja) * 1996-11-14 1998-07-28 Asahi Glass Co Ltd 二液型硬化性組成物
US5762829A (en) * 1997-03-05 1998-06-09 Armstrong World Industries, Inc. Wet silica gels for aerogel and xerogel thermal insulation and processes for the wet gels
US5821275A (en) * 1997-11-10 1998-10-13 Bayer Corporation Flexible foams and flexible molded foams based on liquid isocyanate-terminated allophanate-modified MDI prepolymer blends and processes for the production of these foams
JP2001329037A (ja) * 2000-05-24 2001-11-27 Matsushita Refrig Co Ltd 有機多孔体断熱材とその製造方法、および、断熱箱体
EP1178063A1 (en) * 2000-08-01 2002-02-06 Huntsman International Llc Process for preparing a polyurethane material
RU2184126C2 (ru) * 2000-08-15 2002-06-27 Хозин Вадим Григорьевич Связующее для теплоизоляционного материала и способ изготовления теплоизоляционного материала
DE502008001415D1 (de) * 2007-05-16 2010-11-04 Basf Se Verfahren zur herstellung von organischen xerogelen
KR20110117084A (ko) 2009-01-20 2011-10-26 바스프 에스이 경질 폴리우레탄 폼의 제조 방법
JP2012520386A (ja) 2009-03-16 2012-09-06 ビーエーエスエフ ソシエタス・ヨーロピア キセロゲル複合材料の製造方法
ES2439047T3 (es) 2009-06-29 2014-01-21 Basf Se Geles porosos a base de poliurea aromática

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2008138978A1 (de) * 2007-05-16 2008-11-20 Basf Se Xerogele auf basis von aromatischem polyharnstoff
WO2009027310A1 (de) * 2007-08-28 2009-03-05 Basf Se Xerogele auf basis von polyharnstoff

Also Published As

Publication number Publication date
JP5770202B2 (ja) 2015-08-26
EP2510026B1 (de) 2014-02-26
ES2454615T3 (es) 2014-04-11
RU2012128928A (ru) 2014-01-20
MX2012006475A (es) 2012-06-28
RU2544242C2 (ru) 2015-03-20
PT2510026E (pt) 2014-04-02
CA2783139C (en) 2018-01-09
US20120305827A1 (en) 2012-12-06
WO2011069959A3 (de) 2011-12-01
US11078320B2 (en) 2021-08-03
JP2013513675A (ja) 2013-04-22
CN102652145B (zh) 2014-04-16
AU2010330056B2 (en) 2015-03-26
DK2510026T3 (da) 2014-05-26
WO2011069959A2 (de) 2011-06-16
EP2510026A2 (de) 2012-10-17
CN102652145A (zh) 2012-08-29
CA2783139A1 (en) 2011-06-16
AU2010330056A1 (en) 2012-07-05
KR20120103700A (ko) 2012-09-19
PL2510026T3 (pl) 2014-07-31

Similar Documents

Publication Publication Date Title
KR101818094B1 (ko) 방향족 아민을 주성분으로 하는 개선된 다공성 물질
KR101883022B1 (ko) 에어로겔 또는 크세로겔을 제조하는 방법
KR101832504B1 (ko) 방향족 폴리우레아에 기초한 다공성 겔
KR101870463B1 (ko) 다공성 폴리우레아계 재료의 제조 방법
US9505900B2 (en) Method for producing xerogel composites
US8741976B2 (en) Process for producing aerogels or xerogels
US20100148109A1 (en) Xerogels made from aromatic polyureas
KR101755053B1 (ko) 방향족 및 지환족 아민에 기초한 다공성 겔
KR20160057461A (ko) 이소시아네이트계 유기 에어로겔의 제조 방법

Legal Events

Date Code Title Description
PA0105 International application

St.27 status event code: A-0-1-A10-A15-nap-PA0105

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

PG1501 Laying open of application

St.27 status event code: A-1-1-Q10-Q12-nap-PG1501

R17-X000 Change to representative recorded

St.27 status event code: A-3-3-R10-R17-oth-X000

A201 Request for examination
P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

PA0201 Request for examination

St.27 status event code: A-1-2-D10-D11-exm-PA0201

P22-X000 Classification modified

St.27 status event code: A-2-2-P10-P22-nap-X000

P22-X000 Classification modified

St.27 status event code: A-2-2-P10-P22-nap-X000

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

St.27 status event code: A-1-2-D10-D21-exm-PE0902

T11-X000 Administrative time limit extension requested

St.27 status event code: U-3-3-T10-T11-oth-X000

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

R18-X000 Changes to party contact information recorded

St.27 status event code: A-3-3-R10-R18-oth-X000

E701 Decision to grant or registration of patent right
PE0701 Decision of registration

St.27 status event code: A-1-2-D10-D22-exm-PE0701

GRNT Written decision to grant
PR0701 Registration of establishment

St.27 status event code: A-2-4-F10-F11-exm-PR0701

PR1002 Payment of registration fee

St.27 status event code: A-2-2-U10-U12-oth-PR1002

Fee payment year number: 1

PG1601 Publication of registration

St.27 status event code: A-4-4-Q10-Q13-nap-PG1601

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 4

P22-X000 Classification modified

St.27 status event code: A-4-4-P10-P22-nap-X000

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 5

PC1903 Unpaid annual fee

St.27 status event code: A-4-4-U10-U13-oth-PC1903

Not in force date: 20230109

Payment event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

PC1903 Unpaid annual fee

St.27 status event code: N-4-6-H10-H13-oth-PC1903

Ip right cessation event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

Not in force date: 20230109