KR101805632B1 - 정제 방법 - Google Patents

정제 방법 Download PDF

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Publication number
KR101805632B1
KR101805632B1 KR1020150174019A KR20150174019A KR101805632B1 KR 101805632 B1 KR101805632 B1 KR 101805632B1 KR 1020150174019 A KR1020150174019 A KR 1020150174019A KR 20150174019 A KR20150174019 A KR 20150174019A KR 101805632 B1 KR101805632 B1 KR 101805632B1
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South Korea
Prior art keywords
alcohol compound
primary alcohol
acylated
secondary alcohol
mixture
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Expired - Fee Related
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KR1020150174019A
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English (en)
Korean (ko)
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KR20160072788A (ko
Inventor
디. 길모어 크리스토퍼
이치완
트레포나스 3세 피터
윌리엄스 3세 윌리엄
지에 퀴젠
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롬 앤드 하스 일렉트로닉 머트어리얼즈 엘엘씨
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C07C41/34—Separation; Purification; Stabilisation; Use of additives
    • C07C41/44—Separation; Purification; Stabilisation; Use of additives by treatments giving rise to a chemical modification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C07C41/34—Separation; Purification; Stabilisation; Use of additives
    • C07C41/40—Separation; Purification; Stabilisation; Use of additives by change of physical state, e.g. by crystallisation
    • C07C41/42—Separation; Purification; Stabilisation; Use of additives by change of physical state, e.g. by crystallisation by distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/009—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/0201—Oxygen-containing compounds
    • B01J31/0209—Esters of carboxylic or carbonic acids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/0215—Sulfur-containing compounds
    • B01J31/0225—Sulfur-containing compounds comprising sulfonic acid groups or the corresponding salts
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/09—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis
    • C07C29/10—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of ethers, including cyclic ethers, e.g. oxiranes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/18—Polyhydroxylic acyclic alcohols
    • C07C31/20—Dihydroxylic alcohols
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C43/00—Ethers; Compounds having groups, groups or groups
    • C07C43/02—Ethers
    • C07C43/03—Ethers having all ether-oxygen atoms bound to acyclic carbon atoms
    • C07C43/04—Saturated ethers
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C43/00—Ethers; Compounds having groups, groups or groups
    • C07C43/02—Ethers
    • C07C43/03—Ethers having all ether-oxygen atoms bound to acyclic carbon atoms
    • C07C43/04—Saturated ethers
    • C07C43/13—Saturated ethers containing hydroxy or O-metal groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C43/00—Ethers; Compounds having groups, groups or groups
    • C07C43/02—Ethers
    • C07C43/20—Ethers having an ether-oxygen atom bound to a carbon atom of a six-membered aromatic ring
    • C07C43/23—Ethers having an ether-oxygen atom bound to a carbon atom of a six-membered aromatic ring containing hydroxy or O-metal groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/39—Preparation of carboxylic acid esters by oxidation of groups which are precursors for the acid moiety of the ester
    • C07C67/40—Preparation of carboxylic acid esters by oxidation of groups which are precursors for the acid moiety of the ester by oxidation of primary alcohols
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/02—Esters of acyclic saturated monocarboxylic acids having the carboxyl group bound to an acyclic carbon atom or to hydrogen
    • C07C69/12—Acetic acid esters
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2603/00—Systems containing at least three condensed rings
    • C07C2603/02—Ortho- or ortho- and peri-condensed systems
    • C07C2603/40—Ortho- or ortho- and peri-condensed systems containing four condensed rings
    • C07C2603/42—Ortho- or ortho- and peri-condensed systems containing four condensed rings containing only six-membered rings
    • C07C2603/50—Pyrenes; Hydrogenated pyrenes

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
KR1020150174019A 2014-12-15 2015-12-08 정제 방법 Expired - Fee Related KR101805632B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US14/569,813 2014-12-15
US14/569,813 US9440899B2 (en) 2014-12-15 2014-12-15 Purification method

Publications (2)

Publication Number Publication Date
KR20160072788A KR20160072788A (ko) 2016-06-23
KR101805632B1 true KR101805632B1 (ko) 2017-12-08

Family

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Family Applications (1)

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KR1020150174019A Expired - Fee Related KR101805632B1 (ko) 2014-12-15 2015-12-08 정제 방법

Country Status (5)

Country Link
US (1) US9440899B2 (https=)
JP (1) JP6246781B2 (https=)
KR (1) KR101805632B1 (https=)
CN (1) CN105693482B (https=)
TW (1) TWI631102B (https=)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102498772B1 (ko) 2021-11-29 2023-02-10 주식회사 켐트로닉스 초고순도 pgmea의 제조방법

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US11346727B2 (en) 2016-09-27 2022-05-31 Sony Corporation Sensor, electronic device, wearable terminal, and control method
WO2020043518A1 (en) * 2018-08-30 2020-03-05 Basf Se Process to produce a mono vinyl ether
JP7309907B2 (ja) * 2019-11-29 2023-07-18 富士フイルム株式会社 感活性光線性又は感放射線性樹脂組成物、パターン形成方法、及び、電子デバイスの製造方法
JPWO2021106536A1 (https=) * 2019-11-29 2021-06-03
WO2021106537A1 (ja) * 2019-11-29 2021-06-03 富士フイルム株式会社 レジスト下層膜形成用組成物、パターン形成方法、及び、電子デバイスの製造方法
KR102154356B1 (ko) * 2020-03-10 2020-09-09 주식회사 켐트로닉스 일차 알코올과 이차 알코올의 혼합물로부터 이차 알코올을 분리하여 얻는 방법
KR102889910B1 (ko) * 2020-04-03 2025-11-24 주식회사 이엔에프테크놀로지 프로필렌 글리콜 모노메틸 에테르 이성질체의 선택적 제거용 조성물 및 그 방법
IL311594A (en) * 2021-09-29 2024-05-01 Fujifilm Corp Actinic ray-sensitive or radiation-sensitive resin composition and method for producing resist pattern
WO2025205520A1 (ja) * 2024-03-29 2025-10-02 三菱瓦斯化学株式会社 溶媒およびこれを用いた半導体製造用組成物

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6846961B2 (en) 2001-12-28 2005-01-25 Basf Aktiengesellschaft Preparation of 1-methoxy-2-propanol
JP2008208035A (ja) * 2007-02-23 2008-09-11 Daicel Chem Ind Ltd １−メトキシ−２−プロパノールの製造方法
CN101985418A (zh) 2010-08-16 2011-03-16 江苏天音化工有限公司 一种制备2－甲氧基－1－丙醇醋酸酯的方法

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2072806A (en) * 1933-01-06 1937-03-02 Du Pont Process for the separation of primary from secondary alcohols
US2476053A (en) * 1947-01-02 1949-07-12 Standard Oil Dev Co Process for producing esters
US2872478A (en) * 1956-11-06 1959-02-03 Borden Company A Corp Of New J Separation of alcohols from esters
US2923733A (en) * 1957-03-28 1960-02-02 Pan American Petroleum Corp Process for separating primary from secondary alcohols
SE8305596D0 (sv) 1983-10-12 1983-10-12 Leo Ab A selective acylation method
US5723024A (en) 1996-08-26 1998-03-03 Berg; Lloyd Separation of 2-methyl-1-propanol from 1-butanol by extractive distillation
WO2003022785A2 (en) 2001-09-12 2003-03-20 Anormed Inc. Synthesis of enantiomerically pure amino-substituted fused bicyclic rings
JP2003292471A (ja) * 2002-04-03 2003-10-15 Japan Science & Technology Corp エステル縮合物の製造方法

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6846961B2 (en) 2001-12-28 2005-01-25 Basf Aktiengesellschaft Preparation of 1-methoxy-2-propanol
JP2008208035A (ja) * 2007-02-23 2008-09-11 Daicel Chem Ind Ltd １−メトキシ−２−プロパノールの製造方法
CN101985418A (zh) 2010-08-16 2011-03-16 江苏天音化工有限公司 一种制备2－甲氧基－1－丙醇醋酸酯的方法

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102498772B1 (ko) 2021-11-29 2023-02-10 주식회사 켐트로닉스 초고순도 pgmea의 제조방법

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Publication number Publication date
CN105693482B (zh) 2020-05-15
TW201638062A (zh) 2016-11-01
US20160168064A1 (en) 2016-06-16
JP6246781B2 (ja) 2017-12-13
CN105693482A (zh) 2016-06-22
TWI631102B (zh) 2018-08-01
US9440899B2 (en) 2016-09-13
KR20160072788A (ko) 2016-06-23
JP2016135756A (ja) 2016-07-28

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