KR101790254B1 - 에폭시화 스타트업 방법 - Google Patents
에폭시화 스타트업 방법 Download PDFInfo
- Publication number
- KR101790254B1 KR101790254B1 KR1020127018627A KR20127018627A KR101790254B1 KR 101790254 B1 KR101790254 B1 KR 101790254B1 KR 1020127018627 A KR1020127018627 A KR 1020127018627A KR 20127018627 A KR20127018627 A KR 20127018627A KR 101790254 B1 KR101790254 B1 KR 101790254B1
- Authority
- KR
- South Korea
- Prior art keywords
- ethylene
- temperature
- catalyst
- volume
- epoxidation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/02—Synthesis of the oxirane ring
- C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
- C07D301/04—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen
- C07D301/08—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C11/00—Aliphatic unsaturated hydrocarbons
- C07C11/02—Alkenes
- C07C11/04—Ethylene
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/02—Synthesis of the oxirane ring
- C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
- C07D301/04—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen
- C07D301/08—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase
- C07D301/10—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase with catalysts containing silver or gold
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
- C07D303/02—Compounds containing oxirane rings
- C07D303/04—Compounds containing oxirane rings containing only hydrogen and carbon atoms in addition to the ring oxygen atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Epoxy Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US28739309P | 2009-12-17 | 2009-12-17 | |
| US61/287,393 | 2009-12-17 | ||
| PCT/US2010/060769 WO2011084600A2 (en) | 2009-12-17 | 2010-12-16 | Process for epoxidation start-up |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR20120106809A KR20120106809A (ko) | 2012-09-26 |
| KR101790254B1 true KR101790254B1 (ko) | 2017-10-26 |
Family
ID=44152004
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020127018627A Expired - Fee Related KR101790254B1 (ko) | 2009-12-17 | 2010-12-16 | 에폭시화 스타트업 방법 |
Country Status (13)
Families Citing this family (38)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103599798B (zh) | 2007-05-09 | 2015-11-18 | 国际壳牌研究有限公司 | 环氧化催化剂及其制备方法和生产环氧烷、1,2-二醇、1,2-二醇醚、1,2-碳酸酯或烷醇胺的方法 |
| MX2012007043A (es) * | 2009-12-17 | 2012-07-20 | Scient Design Co | Proceso para el arranque de epoxidacion. |
| US20110152073A1 (en) | 2009-12-23 | 2011-06-23 | Scientific Design Company, Inc. | Epoxidation process and microstructure |
| WO2012141942A1 (en) | 2011-04-11 | 2012-10-18 | Dow Technology Investments Llc | Process for conditioning a high efficiency ethylene oxide catalyst |
| KR102187425B1 (ko) | 2011-12-30 | 2020-12-09 | 생-고뱅 세라믹스 앤드 플라스틱스, 인코포레이티드 | 형상화 연마입자 및 이의 형성방법 |
| US8753742B2 (en) | 2012-01-10 | 2014-06-17 | Saint-Gobain Ceramics & Plastics, Inc. | Abrasive particles having complex shapes and methods of forming same |
| CN110013795A (zh) | 2012-05-23 | 2019-07-16 | 圣戈本陶瓷及塑料股份有限公司 | 成形磨粒及其形成方法 |
| RU2614488C2 (ru) | 2012-10-15 | 2017-03-28 | Сен-Гобен Абразивс, Инк. | Абразивные частицы, имеющие определенные формы, и способы формирования таких частиц |
| CN104884443B (zh) * | 2012-12-31 | 2017-07-04 | 科学设计公司 | 用于环氧乙烷催化剂的启动方法 |
| EP2943477B1 (en) * | 2013-01-11 | 2018-03-07 | Scientific Design Company Inc. | Epoxidation process with post-conditioning step |
| WO2014161001A1 (en) | 2013-03-29 | 2014-10-02 | Saint-Gobain Abrasives, Inc. | Abrasive particles having particular shapes and methods of forming such particles |
| CN110591645A (zh) | 2013-09-30 | 2019-12-20 | 圣戈本陶瓷及塑料股份有限公司 | 成形磨粒及其形成方法 |
| US9221776B2 (en) | 2013-12-23 | 2015-12-29 | Scientific Design Company, Inc. | Epoxidation process |
| KR101870617B1 (ko) | 2013-12-31 | 2018-06-26 | 생-고뱅 어브레이시브즈, 인코포레이티드 | 형상화 연마 입자들을 포함하는 연마 물품 |
| US9771507B2 (en) | 2014-01-31 | 2017-09-26 | Saint-Gobain Ceramics & Plastics, Inc. | Shaped abrasive particle including dopant material and method of forming same |
| CA3123554A1 (en) | 2014-04-14 | 2015-10-22 | Saint-Gobain Ceramics & Plastics, Inc. | Abrasive article including shaped abrasive particles |
| US9914864B2 (en) | 2014-12-23 | 2018-03-13 | Saint-Gobain Ceramics & Plastics, Inc. | Shaped abrasive particles and method of forming same |
| TWI634200B (zh) | 2015-03-31 | 2018-09-01 | 聖高拜磨料有限公司 | 固定磨料物品及其形成方法 |
| CN107636109A (zh) | 2015-03-31 | 2018-01-26 | 圣戈班磨料磨具有限公司 | 固定磨料制品和其形成方法 |
| TWI712577B (zh) * | 2015-06-02 | 2020-12-11 | 美商科學設計有限公司 | 具有增強的孔結構的多孔體 |
| WO2016201104A1 (en) | 2015-06-11 | 2016-12-15 | Saint-Gobain Ceramics & Plastics, Inc. | Abrasive article including shaped abrasive particles |
| EP3455320A4 (en) | 2016-05-10 | 2019-11-20 | Saint-Gobain Ceramics&Plastics, Inc. | GRINDING PARTICLES AND METHOD FOR FORMING THEREOF |
| EP4071224A3 (en) | 2016-05-10 | 2023-01-04 | Saint-Gobain Ceramics and Plastics, Inc. | Methods of forming abrasive articles |
| EP4349896A3 (en) | 2016-09-29 | 2024-06-12 | Saint-Gobain Abrasives, Inc. | Fixed abrasive articles and methods of forming same |
| TWI774707B (zh) | 2016-12-02 | 2022-08-21 | 荷蘭商蜆殼國際研究所 | 用於調節乙烯環氧化催化劑之方法及用於製造環氧乙烷之相關方法 |
| US10563105B2 (en) | 2017-01-31 | 2020-02-18 | Saint-Gobain Ceramics & Plastics, Inc. | Abrasive article including shaped abrasive particles |
| US10865148B2 (en) | 2017-06-21 | 2020-12-15 | Saint-Gobain Ceramics & Plastics, Inc. | Particulate materials and methods of forming same |
| WO2019055773A1 (en) | 2017-09-15 | 2019-03-21 | MultiPhase Solutions, Inc. | GAS PHASE CHROMATOGRAPHY OF SELECTIVE HALOGEN DETECTION FOR ONLINE ANALYSIS AND CONTROL OF SELECTIVE OXIDATION CHEMICAL PRODUCTION PROCESSES |
| WO2019154863A1 (en) * | 2018-02-07 | 2019-08-15 | Basf Se | Method for preparing a silver impregnation solution |
| US11926019B2 (en) | 2019-12-27 | 2024-03-12 | Saint-Gobain Ceramics & Plastics, Inc. | Abrasive articles and methods of forming same |
| WO2021133876A1 (en) | 2019-12-27 | 2021-07-01 | Saint-Gobain Ceramics & Plastics, Inc. | Abrasive articles and methods of forming same |
| CN114845838B (zh) | 2019-12-27 | 2024-10-25 | 圣戈本陶瓷及塑料股份有限公司 | 磨料制品及其形成方法 |
| CN113121474A (zh) * | 2019-12-30 | 2021-07-16 | 中国石油化工股份有限公司 | 乙烯环氧化银催化剂的开车方法 |
| CN114057669B (zh) * | 2020-07-29 | 2023-12-08 | 中国石油化工股份有限公司 | 一种乙烯环氧化恒温开车方法 |
| CN114436998A (zh) * | 2020-11-05 | 2022-05-06 | 中国石油化工股份有限公司 | 一种乙烯环氧化开车方法 |
| US12496686B2 (en) | 2021-12-30 | 2025-12-16 | Saint-Gobain Abrasives, Inc. | Abrasive articles and methods of forming same |
| WO2023130052A1 (en) | 2021-12-30 | 2023-07-06 | Saint-Gobain Abrasives, Inc. | Abrasive articles and methods of forming same |
| CN118541242A (zh) | 2021-12-30 | 2024-08-23 | 圣戈班磨料磨具有限公司 | 磨料制品及其形成方法 |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2002248351A (ja) | 2001-02-27 | 2002-09-03 | Mitsubishi Chemicals Corp | レニウム含有触媒を用いるオレフィンオキシドの製造方法 |
| US20070032670A1 (en) | 2003-09-29 | 2007-02-08 | Liping Zhang | Process for the production of alkylene oxide using a gas-phase promoter system |
| WO2008140714A1 (en) | 2007-05-11 | 2008-11-20 | Billig Barry J | Start-up of high selectivity catalysts in olefin oxide plants |
| WO2009042300A1 (en) * | 2007-09-26 | 2009-04-02 | Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg | Process for initiating a highly selective ethylene oxide catalyst |
Family Cites Families (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1170663A (en) | 1967-03-22 | 1969-11-12 | Shell Int Research | Process for preparing Silver Catalysts |
| US3702259A (en) | 1970-12-02 | 1972-11-07 | Shell Oil Co | Chemical production of metallic silver deposits |
| US4766105A (en) | 1986-10-31 | 1988-08-23 | Shell Oil Company | Ethylene oxide catalyst and process for preparing the catalyst |
| US4761394A (en) | 1986-10-31 | 1988-08-02 | Shell Oil Company | Ethylene oxide catalyst and process for preparing the catalyst |
| US4908343A (en) | 1987-02-20 | 1990-03-13 | Union Carbide Chemicals And Plastics Company Inc. | Catalyst composition for oxidation of ethylene to ethylene oxide |
| US5057481A (en) | 1987-02-20 | 1991-10-15 | Union Carbide Chemicals And Plastics Technology Corporation | Catalyst composition for oxidation of ethylene to ethylene oxide |
| US4874879A (en) | 1988-07-25 | 1989-10-17 | Shell Oil Company | Process for starting-up an ethylene oxide reactor |
| DE68925767T2 (de) | 1988-08-30 | 1996-08-14 | Union Carbide Corp | Katalysatoren für die Herstellung von Ethylenoxid und Verfahren zur deren Herstellung |
| US5187140A (en) | 1989-10-18 | 1993-02-16 | Union Carbide Chemicals & Plastics Technology Corporation | Alkylene oxide catalysts containing high silver content |
| US5102848A (en) | 1990-09-28 | 1992-04-07 | Union Carbide Chemicals & Plastics Technology Corporation | Catalyst composition for oxidation of ethylene to ethylene oxide |
| US5155242A (en) | 1991-12-05 | 1992-10-13 | Shell Oil Company | Process for starting-up an ethylene oxide reactor |
| US5407888A (en) | 1992-05-12 | 1995-04-18 | Basf Aktiengesellschaft | Silver catalyst |
| US5856534A (en) * | 1997-12-18 | 1999-01-05 | Arco Chemical Technology, L.P. | Epoxidation process using supported silver catalysts treated with carbon dioxide |
| EP1517901B1 (en) * | 2002-06-28 | 2010-07-07 | Shell Internationale Research Maatschappij B.V. | A method for the start-up of an epoxidation process and a process for the epoxidation of an olefin |
| JP4537848B2 (ja) | 2002-06-28 | 2010-09-08 | シエル・インターナシヨナル・リサーチ・マートスハツペイ・ベー・ヴエー | 触媒の選択性を改善する方法及びオレフィンのエポキシ化方法 |
| CA2490892C (en) * | 2002-06-28 | 2012-03-20 | Shell Internationale Research Maatschappij B.V. | A method for the start-up of an epoxidation process, a catalyst and a process for the epoxidation of an olefin |
| US8791280B2 (en) | 2005-08-10 | 2014-07-29 | Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg | Process for preparation of catalyst carrier and its use in catalyst preparation |
| CN102056909B (zh) * | 2008-05-07 | 2014-03-05 | 国际壳牌研究有限公司 | 环氧化工艺的开车方法及环氧乙烷、1,2-二醇、1,2-二醇醚、1,2-碳酸酯或链烷醇胺的制备方法 |
| MX2012007043A (es) * | 2009-12-17 | 2012-07-20 | Scient Design Co | Proceso para el arranque de epoxidacion. |
| US20110152073A1 (en) * | 2009-12-23 | 2011-06-23 | Scientific Design Company, Inc. | Epoxidation process and microstructure |
-
2010
- 2010-12-16 MX MX2012007043A patent/MX2012007043A/es active IP Right Grant
- 2010-12-16 WO PCT/US2010/060769 patent/WO2011084600A2/en not_active Ceased
- 2010-12-16 JP JP2012544826A patent/JP5946772B2/ja not_active Expired - Fee Related
- 2010-12-16 MY MYPI2012002389A patent/MY157612A/en unknown
- 2010-12-16 CN CN201080057763.XA patent/CN102666514B/zh not_active Expired - Fee Related
- 2010-12-16 EP EP10842602.4A patent/EP2513077B1/en not_active Revoked
- 2010-12-16 BR BR112012014695A patent/BR112012014695A2/pt not_active IP Right Cessation
- 2010-12-16 CA CA2783604A patent/CA2783604C/en not_active Expired - Fee Related
- 2010-12-16 IN IN5178DEN2012 patent/IN2012DN05178A/en unknown
- 2010-12-16 TW TW099144226A patent/TWI485141B/zh not_active IP Right Cessation
- 2010-12-16 RU RU2012130065/04A patent/RU2542978C2/ru not_active IP Right Cessation
- 2010-12-16 EP EP20140171850 patent/EP2778157A1/en not_active Withdrawn
- 2010-12-16 US US12/970,392 patent/US8530682B2/en not_active Expired - Fee Related
- 2010-12-16 KR KR1020127018627A patent/KR101790254B1/ko not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2002248351A (ja) | 2001-02-27 | 2002-09-03 | Mitsubishi Chemicals Corp | レニウム含有触媒を用いるオレフィンオキシドの製造方法 |
| US20070032670A1 (en) | 2003-09-29 | 2007-02-08 | Liping Zhang | Process for the production of alkylene oxide using a gas-phase promoter system |
| WO2008140714A1 (en) | 2007-05-11 | 2008-11-20 | Billig Barry J | Start-up of high selectivity catalysts in olefin oxide plants |
| WO2009042300A1 (en) * | 2007-09-26 | 2009-04-02 | Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg | Process for initiating a highly selective ethylene oxide catalyst |
Also Published As
| Publication number | Publication date |
|---|---|
| CA2783604A1 (en) | 2011-07-14 |
| MX2012007043A (es) | 2012-07-20 |
| JP2013514387A (ja) | 2013-04-25 |
| BR112012014695A2 (pt) | 2015-09-15 |
| IN2012DN05178A (cg-RX-API-DMAC10.html) | 2015-10-23 |
| EP2513077A2 (en) | 2012-10-24 |
| WO2011084600A3 (en) | 2011-11-17 |
| MY157612A (en) | 2016-06-30 |
| EP2513077B1 (en) | 2014-06-11 |
| RU2012130065A (ru) | 2014-01-27 |
| TWI485141B (zh) | 2015-05-21 |
| US8530682B2 (en) | 2013-09-10 |
| RU2542978C2 (ru) | 2015-02-27 |
| EP2778157A1 (en) | 2014-09-17 |
| JP5946772B2 (ja) | 2016-07-06 |
| US20110152548A1 (en) | 2011-06-23 |
| CA2783604C (en) | 2018-05-01 |
| EP2513077A4 (en) | 2013-05-22 |
| TW201136906A (en) | 2011-11-01 |
| WO2011084600A2 (en) | 2011-07-14 |
| CN102666514A (zh) | 2012-09-12 |
| KR20120106809A (ko) | 2012-09-26 |
| CN102666514B (zh) | 2015-11-25 |
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