KR101749561B1 - 5-플루오로-1-알킬-3-플루오로알킬-1ｈ-피라졸-4-카보닐 클로라이드의 제조방법 - Google Patents

5-플루오로-1-알킬-3-플루오로알킬-1ｈ-피라졸-4-카보닐 클로라이드의 제조방법 Download PDF

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Publication number
KR101749561B1
KR101749561B1 KR1020167011442A KR20167011442A KR101749561B1 KR 101749561 B1 KR101749561 B1 KR 101749561B1 KR 1020167011442 A KR1020167011442 A KR 1020167011442A KR 20167011442 A KR20167011442 A KR 20167011442A KR 101749561 B1 KR101749561 B1 KR 101749561B1
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South Korea
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pyrazole
alkyl
fluoroalkyl
carbaldehyde
fluoro
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Korean (ko)
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KR20160054041A (ko
Inventor
세르기이 파제녹
노르베르트 루이
마르크 코슈텐
귄터 바르텔스
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바이엘 인텔렉쳐 프로퍼티 게엠베하
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/16—Halogen atoms or nitro radicals
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
    • A01N43/56—1,2-Diazoles; Hydrogenated 1,2-diazoles

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Diaphragms For Electromechanical Transducers (AREA)
  • Finger-Pressure Massage (AREA)
  • Vehicle Interior And Exterior Ornaments, Soundproofing, And Insulation (AREA)
KR1020167011442A 2009-11-19 2010-11-17 5-플루오로-1-알킬-3-플루오로알킬-1ｈ-피라졸-4-카보닐 클로라이드의 제조방법 Active KR101749561B1 (ko)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US26264109P 2009-11-19 2009-11-19
EP09176426.6 2009-11-19
US61/262,641 2009-11-19
EP09176426A EP2325173A1 (de) 2009-11-19 2009-11-19 Verfahren zum Herstellen von 5-Fluor-1-alkyl-3-fluoralkyl-1H-pyrazol-4-carbonsäurechloriden
PCT/EP2010/067630 WO2011061205A1 (de) 2009-11-19 2010-11-17 Verfahren zum herstellen von 5-fluor-1-alkyl-3-fluoralkyl-1h-pyrazol-4-carbonsäurechloriden

Related Parent Applications (1)

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KR1020127015772A Division KR101635046B1 (ko) 2009-11-19 2010-11-17 5-플루오로-1-알킬-3-플루오로알킬-1ｈ-피라졸-4-카보닐 클로라이드의 제조방법

Publications (2)

Publication Number Publication Date
KR20160054041A KR20160054041A (ko) 2016-05-13
KR101749561B1 true KR101749561B1 (ko) 2017-06-21

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KR1020127015772A Active KR101635046B1 (ko) 2009-11-19 2010-11-17 5-플루오로-1-알킬-3-플루오로알킬-1ｈ-피라졸-4-카보닐 클로라이드의 제조방법
KR1020167011442A Active KR101749561B1 (ko) 2009-11-19 2010-11-17 5-플루오로-1-알킬-3-플루오로알킬-1ｈ-피라졸-4-카보닐 클로라이드의 제조방법

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KR1020127015772A Active KR101635046B1 (ko) 2009-11-19 2010-11-17 5-플루오로-1-알킬-3-플루오로알킬-1ｈ-피라졸-4-카보닐 클로라이드의 제조방법

Country Status (13)

Country Link
US (2) US8436191B2 (enExample)
EP (2) EP2325173A1 (enExample)
JP (1) JP5802213B2 (enExample)
KR (2) KR101635046B1 (enExample)
CN (1) CN102666492B (enExample)
BR (1) BR112012011961B1 (enExample)
DK (1) DK2501682T3 (enExample)
ES (1) ES2600864T3 (enExample)
IL (1) IL219682A (enExample)
IN (1) IN2012DN04414A (enExample)
MX (2) MX344246B (enExample)
TW (1) TWI510473B (enExample)
WO (1) WO2011061205A1 (enExample)

Families Citing this family (14)

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AR076839A1 (es) * 2009-05-15 2011-07-13 Bayer Cropscience Ag Derivados fungicidas de pirazol carboxamidas
EP2325173A1 (de) 2009-11-19 2011-05-25 Bayer CropScience AG Verfahren zum Herstellen von 5-Fluor-1-alkyl-3-fluoralkyl-1H-pyrazol-4-carbonsäurechloriden
EP2560961B1 (de) 2010-04-23 2016-11-16 Bayer Intellectual Property GmbH Verfahren zum herstellen von 5-fluor-1-alkyl-3-fluoralkyl-1h-pyrazol-4-carbonsäurechloriden und -fluoriden
JP6101345B2 (ja) 2012-05-14 2017-03-22 バイエル・クロップサイエンス・アクチェンゲゼルシャフト １−アルキル−３−フルオロアルキル−１ｈ−ピラゾール−４−カルボニルクロライド類の製造方法
US9617220B2 (en) 2012-08-07 2017-04-11 Bayer Cropscience Ag Method for the preparation of perfluoroalkyl containing pyrazoles carboxylates
BR112015015833B1 (pt) * 2013-01-17 2020-05-19 Bayer Cropscience Ag processo de preparação de 5-fluoro-1 -metil-3-difluorometil-1 h-pirazol-4-carbaldeído
ES2641217T3 (es) * 2013-09-20 2017-11-08 Bayer Cropscience Aktiengesellschaft Procedimiento de preparación de 5-fluoro-1-alquil-3-fluoroalquil-1H-pirazol-4-carbaldehído
KR102319577B1 (ko) * 2014-01-24 2021-10-29 바이엘 크롭사이언스 악티엔게젤샤프트 １-알킬-３-디플루오로메틸-５-플루오르-１ｈ-피라졸-４-카르브알데히드 및 １-알킬-３-디플루오로메틸-５-플루오르-１ｈ-피라졸-４-카르복실레이트의 제조 방법
EP3015458A1 (en) * 2014-11-03 2016-05-04 Bayer CropScience AG Process for preparing 3,5-bis(haloalkyl)pyrazole derivatives from a,a-dihaloamines and ketimines
JP6431088B2 (ja) 2014-03-24 2018-11-28 バイエル・クロップサイエンス・アクチェンゲゼルシャフト α，α−ジハロアミン類およびケチミン類からの３，５−ビス（ハロアルキル）ピラゾール誘導体の製造方法
TWI705055B (zh) 2015-04-29 2020-09-21 德商拜耳作物科學公司 製備5-氟-1h-吡唑-4-羰基氟化物之方法
JP6911143B2 (ja) 2018-11-07 2021-07-28 福建永晶科技股▲ふん▼有限公司Ｆｕｊｉａｎ Ｙｏｎｇｊｉｎｇ Ｔｅｃｈｎｏｌｏｇｙ Ｃｏ．， Ｌｔｄ ピラゾール又はピリミジノンの新しい製造方法
CN112745260B (zh) 2019-10-29 2022-11-15 沈阳中化农药化工研发有限公司 一种含取代苯乙酮结构片段的酰胺类化合物及其制备方法和用途
WO2022233129A1 (en) 2021-05-05 2022-11-10 Fujian Yongjing Technology Co., Ltd New process for the synthesis of 5-fluoro-3- (difuoromethyl) -5-fluoro-1-methyl-1h-pyrazole-4-carboxylic acid derivatives and the free acid thereof

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1993011117A1 (en) * 1991-12-06 1993-06-10 Monsanto Company Pyrazole carboxanilide fungicides

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DE19544800A1 (de) 1995-12-01 1997-06-05 Bayer Ag Verfahren zur Herstellung von 1,3-Dimethyl-5-fluor-pyrazol-4-carboxaniliden
JP4465133B2 (ja) * 2001-02-08 2010-05-19 クミアイ化学工業株式会社 イソオキサゾリン誘導体及びこれを有効成分とする除草剤
DE60238194D1 (de) * 2001-06-21 2010-12-16 Kumiai Chemical Industry Co Isoxazolinderivate und herbizide
UA78071C2 (en) 2002-08-07 2007-02-15 Kumiai Chemical Industry Co Herbicidal composition
RU2346996C2 (ru) 2004-06-29 2009-02-20 ЮРОПИЭН НИКЕЛЬ ПиЭлСи Усовершенствованное выщелачивание основных металлов
CA2577525C (en) 2004-08-18 2010-03-30 Pfizer Inc. Inhibitors of hepatitis c virus rna-dependent rna polymerase, and compositions and treatments using the same
WO2007000020A1 (en) 2005-06-29 2007-01-04 Compumedics Limited Sensor assembly with conductive bridge
DE102005044451A1 (de) 2005-09-17 2007-03-22 Bayer Cropscience Gmbh Verfahren zum Herstellen von 5-Fluor-1,3-dialkyl-1H-pyrazol-4-carbonsäurefluoriden
US7833689B2 (en) * 2005-09-27 2010-11-16 Fujifilm Corporation Lithographic printing plate precursor and lithographic printing method
AR056882A1 (es) 2006-02-01 2007-10-31 Bayer Cropscience Sa Derivados del fungicida n- cicloalquil- bencil- amida
DE102007002674A1 (de) * 2007-01-18 2008-07-24 Bayer Cropscience Ag Verfahren zum Herstellen von substituierten Pyrazolcarbonsäurechloriden
EP2325173A1 (de) 2009-11-19 2011-05-25 Bayer CropScience AG Verfahren zum Herstellen von 5-Fluor-1-alkyl-3-fluoralkyl-1H-pyrazol-4-carbonsäurechloriden

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1993011117A1 (en) * 1991-12-06 1993-06-10 Monsanto Company Pyrazole carboxanilide fungicides

Also Published As

Publication number Publication date
US20110207940A1 (en) 2011-08-25
BR112012011961A2 (pt) 2015-09-08
CN102666492A (zh) 2012-09-12
KR101635046B1 (ko) 2016-07-01
WO2011061205A1 (de) 2011-05-26
IN2012DN04414A (enExample) 2015-08-07
US8436191B2 (en) 2013-05-07
MX344246B (es) 2016-12-07
JP5802213B2 (ja) 2015-10-28
US8765971B2 (en) 2014-07-01
BR112012011961B1 (pt) 2018-05-08
TW201127817A (en) 2011-08-16
US20130165664A1 (en) 2013-06-27
ES2600864T3 (es) 2017-02-13
KR20160054041A (ko) 2016-05-13
EP2325173A1 (de) 2011-05-25
KR20120084325A (ko) 2012-07-27
EP2501682B1 (de) 2016-08-03
IL219682A (en) 2016-08-31
MX2012005676A (es) 2012-06-19
TWI510473B (zh) 2015-12-01
DK2501682T3 (en) 2016-11-14
JP2013511485A (ja) 2013-04-04
IL219682A0 (en) 2012-07-31
CN102666492B (zh) 2016-03-23
EP2501682A1 (de) 2012-09-26

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