KR101592049B1 - 리튬, 철 및 포스페이트를 함유하는 결정질 물질의 제조 방법 - Google Patents
리튬, 철 및 포스페이트를 함유하는 결정질 물질의 제조 방법 Download PDFInfo
- Publication number
- KR101592049B1 KR101592049B1 KR1020107025278A KR20107025278A KR101592049B1 KR 101592049 B1 KR101592049 B1 KR 101592049B1 KR 1020107025278 A KR1020107025278 A KR 1020107025278A KR 20107025278 A KR20107025278 A KR 20107025278A KR 101592049 B1 KR101592049 B1 KR 101592049B1
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- South Korea
- Prior art keywords
- compound
- mixture
- carbon
- containing compound
- electrically conductive
- Prior art date
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Classifications
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/26—Phosphates
- C01B25/30—Alkali metal phosphates
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/26—Phosphates
- C01B25/45—Phosphates containing plural metal, or metal and ammonium
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B1/00—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors
- H01B1/06—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors mainly consisting of other non-metallic substances
- H01B1/08—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors mainly consisting of other non-metallic substances oxides
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
- H01M4/52—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
- H01M4/525—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
- H01M4/5825—Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/62—Selection of inactive substances as ingredients for active masses, e.g. binders, fillers
- H01M4/624—Electric conductive fillers
- H01M4/625—Carbon or graphite
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/40—Electric properties
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B1/00—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors
- H01B1/02—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors mainly consisting of metals or alloys
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/052—Li-accumulators
- H01M10/0525—Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
Landscapes
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Battery Electrode And Active Subsutance (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US4580208P | 2008-04-17 | 2008-04-17 | |
| US61/045,802 | 2008-04-17 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR20110008218A KR20110008218A (ko) | 2011-01-26 |
| KR101592049B1 true KR101592049B1 (ko) | 2016-02-11 |
Family
ID=40874939
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020107025278A Active KR101592049B1 (ko) | 2008-04-17 | 2009-04-16 | 리튬, 철 및 포스페이트를 함유하는 결정질 물질의 제조 방법 |
Country Status (8)
| Country | Link |
|---|---|
| US (2) | US20110049443A1 (https=) |
| EP (1) | EP2285740B1 (https=) |
| JP (1) | JP2011519806A (https=) |
| KR (1) | KR101592049B1 (https=) |
| CN (1) | CN102066241B (https=) |
| CA (1) | CA2721029A1 (https=) |
| TW (1) | TW201010944A (https=) |
| WO (1) | WO2009127674A1 (https=) |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101063214B1 (ko) * | 2008-11-28 | 2011-09-07 | 전자부품연구원 | 리튬이차전지용 구형 양극 활물질 제조방법 |
| TWI474970B (zh) * | 2008-12-29 | 2015-03-01 | Basf Se | 於水熱條件下合成鋰-金屬-磷酸鹽 |
| KR20110139281A (ko) | 2009-03-17 | 2011-12-28 | 바스프 에스이 | 열수 조건 하의 리튬-철-포스페이트의 합성 방법 |
| JP5886193B2 (ja) | 2009-06-24 | 2016-03-16 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | LiFePO4−炭素合成物を製造するための方法 |
| JP5729802B2 (ja) * | 2009-12-25 | 2015-06-03 | 三菱マテリアル株式会社 | Liイオン電池用正極活物質、およびその製造方法 |
| CN101989653B (zh) * | 2010-05-06 | 2012-10-31 | 黄兵 | 超微球颗粒连接的锂离子电池用球形正极材料及其制备方法 |
| FR2978137A1 (fr) * | 2011-07-21 | 2013-01-25 | Saint Gobain Ct Recherches | Produit fondu a base de lithium |
| FR2989378B1 (fr) | 2012-04-16 | 2015-10-02 | Commissariat Energie Atomique | Polymere comme materiau d'electrode pour des batteries secondaires au lithium. |
| WO2013185837A1 (en) * | 2012-06-15 | 2013-12-19 | MAX-PLANCK-Gesellschaft zur Förderung der Wissenschaften e.V. | Method of manufacture of an electrode material and an electrode material |
| US10086351B2 (en) | 2013-05-06 | 2018-10-02 | Llang-Yuh Chen | Multi-stage process for producing a material of a battery cell |
| EP2882015B1 (en) | 2013-08-28 | 2018-10-03 | LG Chem, Ltd. | Cathode active material containing lithium transition metal phosphate particles, preparation method therefor, and lithium secondary battery containing same |
| FR3012450B1 (fr) | 2013-10-30 | 2017-10-13 | Commissariat Energie Atomique | Materiau d'electrode pour batterie organique |
| CN103647080A (zh) * | 2013-11-15 | 2014-03-19 | 成都兴能新材料有限公司 | 金属离子-LiFePO4-C复合材料的制备方法 |
| CN106684379B (zh) * | 2015-11-11 | 2019-05-10 | 中国科学院金属研究所 | 合成具有超高大倍率充放电性能的超薄纳米片状LiFePO4的方法 |
| JP7280722B2 (ja) * | 2019-03-15 | 2023-05-24 | 積水化学工業株式会社 | 非水電解質二次電池用正極及びリチウムイオン二次電池 |
| US11673112B2 (en) | 2020-06-28 | 2023-06-13 | eJoule, Inc. | System and process with assisted gas flow inside a reaction chamber |
| US11376559B2 (en) | 2019-06-28 | 2022-07-05 | eJoule, Inc. | Processing system and method for producing a particulate material |
| US11121354B2 (en) | 2019-06-28 | 2021-09-14 | eJoule, Inc. | System with power jet modules and method thereof |
| WO2020264464A1 (en) | 2019-06-28 | 2020-12-30 | eJoule, Inc. | Assisted gas flow inside a reaction chamber of a processing system |
| KR20250044452A (ko) | 2022-08-18 | 2025-03-31 | 인테그랄 파워 | 리튬 이차 전지를 위한 개선된 캐소드 물질 |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2007230784A (ja) * | 2004-03-30 | 2007-09-13 | Agc Seimi Chemical Co Ltd | リチウム鉄複合酸化物の製造方法 |
Family Cites Families (33)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6514640B1 (en) * | 1996-04-23 | 2003-02-04 | Board Of Regents, The University Of Texas System | Cathode materials for secondary (rechargeable) lithium batteries |
| US5910382A (en) * | 1996-04-23 | 1999-06-08 | Board Of Regents, University Of Texas Systems | Cathode materials for secondary (rechargeable) lithium batteries |
| US20020192137A1 (en) * | 2001-04-30 | 2002-12-19 | Benjamin Chaloner-Gill | Phosphate powder compositions and methods for forming particles with complex anions |
| CA2270771A1 (fr) * | 1999-04-30 | 2000-10-30 | Hydro-Quebec | Nouveaux materiaux d'electrode presentant une conductivite de surface elevee |
| US6528033B1 (en) * | 2000-01-18 | 2003-03-04 | Valence Technology, Inc. | Method of making lithium-containing materials |
| CA2320661A1 (fr) * | 2000-09-26 | 2002-03-26 | Hydro-Quebec | Nouveau procede de synthese de materiaux limpo4 a structure olivine |
| EP1261050A1 (en) * | 2001-05-23 | 2002-11-27 | n.v. Umicore s.a. | Lithium transition-metal phosphate powder for rechargeable batteries |
| US6913855B2 (en) | 2002-07-22 | 2005-07-05 | Valence Technology, Inc. | Method of synthesizing electrochemically active materials from a slurry of precursors |
| FR2848205B1 (fr) * | 2002-12-05 | 2006-03-24 | Commissariat Energie Atomique | Composes d'insertion du lithium substitues au bore, materiaux actifs d'electrodes, accumulateurs et dispositifs electrochromes |
| FR2852148B1 (fr) | 2003-03-07 | 2014-04-11 | Batscap Sa | Materiau pour electrode composite, procede pour sa preparation |
| JP4483253B2 (ja) | 2003-09-30 | 2010-06-16 | 三菱化学株式会社 | リチウム二次電池用正極材料、リチウム二次電池用正極及びリチウム二次電池 |
| JP4522682B2 (ja) * | 2003-10-09 | 2010-08-11 | 住友大阪セメント株式会社 | 電極材料粉体の製造方法と電極材料粉体及び電極並びにリチウム電池 |
| CN1233054C (zh) | 2003-12-17 | 2005-12-21 | 北京科技大学 | 一种采用微波法制备LiFePO4材料的方法 |
| JP2006155941A (ja) * | 2004-11-25 | 2006-06-15 | Kyushu Univ | 電極活物質の製造方法 |
| DE102005012640B4 (de) * | 2005-03-18 | 2015-02-05 | Süd-Chemie Ip Gmbh & Co. Kg | Kreisprozess zur nasschemischen Herstellung von Lithiummetallphosphaten |
| DE102005015613A1 (de) | 2005-04-05 | 2006-10-12 | Süd-Chemie AG | Kristallines Ionenleitendes Nanomaterial und Verfahren zu seiner Herstellung |
| US20080305382A1 (en) | 2005-04-05 | 2008-12-11 | Byd Company Limited | Flow-Field Plate and Fuel Cell Stack Using the Same |
| WO2006116251A2 (en) * | 2005-04-26 | 2006-11-02 | The University Of Chicago | Processes for making dense, spherical, active materials for lithium-ion cells |
| JP4869629B2 (ja) * | 2005-05-30 | 2012-02-08 | 住友大阪セメント株式会社 | リチウム電池用正極活物質の製造方法及びリチウム電池用正極活物質並びにリチウム電池 |
| JP4804045B2 (ja) * | 2005-06-15 | 2011-10-26 | Agcセイミケミカル株式会社 | リチウム鉄複合酸化物の製造方法 |
| CN100420076C (zh) * | 2005-12-19 | 2008-09-17 | 南开大学 | 溶胶凝胶法合成锂离子电池正极材料磷酸钒锂的方法 |
| KR100940979B1 (ko) * | 2006-05-08 | 2010-02-05 | 주식회사 엘지화학 | LiFeP04의 제조방법 |
| JP5216960B2 (ja) * | 2006-12-26 | 2013-06-19 | 日立マクセル株式会社 | リチウムイオン二次電池用正極活物質 |
| KR101454501B1 (ko) * | 2007-04-16 | 2014-10-23 | 바스프 에스이 | 리튬 풍부 금속 산화물의 제조 방법 |
| JP5293936B2 (ja) * | 2007-05-21 | 2013-09-18 | 戸田工業株式会社 | 非水電解質二次電池用オリビン型複合酸化物及びその製造方法、並びに二次電池 |
| EP2207751B1 (en) * | 2007-10-01 | 2013-07-03 | Basf Se | Process for the preparation of porous lithium-, vanadium and phosphate-comprising materials |
| EP2212247B1 (en) * | 2007-10-01 | 2013-07-17 | Basf Se | Process for the preparation of crystalline lithium-, vanadium- and phosphate-comprising materials |
| EP2277828B1 (en) * | 2008-03-31 | 2018-08-08 | Toda Kogyo Corp. | Lithium iron phosphate powder manufacturing method, olivine structured lithium iron phosphate powder, cathode sheet using said lithium iron phosphate powder, and non-aqueous solvent secondary battery |
| JP5517032B2 (ja) * | 2008-03-31 | 2014-06-11 | 戸田工業株式会社 | 非水電解質二次電池用オリビン型複合酸化物粒子粉末及びその製造方法、並びに二次電池 |
| TW200951066A (en) * | 2008-04-17 | 2009-12-16 | Basf Se | Process for the preparation of crystalline lithium-, iron-and phosphate-comprising materials |
| TWI440597B (zh) * | 2008-08-26 | 2014-06-11 | Basf Se | 於水熱條件下合成LiFePO4 |
| TWI474970B (zh) * | 2008-12-29 | 2015-03-01 | Basf Se | 於水熱條件下合成鋰-金屬-磷酸鹽 |
| KR20110139281A (ko) | 2009-03-17 | 2011-12-28 | 바스프 에스이 | 열수 조건 하의 리튬-철-포스페이트의 합성 방법 |
-
2009
- 2009-04-14 TW TW098112365A patent/TW201010944A/zh unknown
- 2009-04-16 JP JP2011504454A patent/JP2011519806A/ja active Pending
- 2009-04-16 WO PCT/EP2009/054488 patent/WO2009127674A1/en not_active Ceased
- 2009-04-16 EP EP09732251.5A patent/EP2285740B1/en active Active
- 2009-04-16 US US12/988,418 patent/US20110049443A1/en not_active Abandoned
- 2009-04-16 CN CN200980122733XA patent/CN102066241B/zh active Active
- 2009-04-16 CA CA2721029A patent/CA2721029A1/en not_active Abandoned
- 2009-04-16 KR KR1020107025278A patent/KR101592049B1/ko active Active
-
2014
- 2014-12-08 US US14/563,290 patent/US9147877B2/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2007230784A (ja) * | 2004-03-30 | 2007-09-13 | Agc Seimi Chemical Co Ltd | リチウム鉄複合酸化物の製造方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| EP2285740B1 (en) | 2014-05-21 |
| KR20110008218A (ko) | 2011-01-26 |
| JP2011519806A (ja) | 2011-07-14 |
| WO2009127674A1 (en) | 2009-10-22 |
| US20110049443A1 (en) | 2011-03-03 |
| US20150090940A1 (en) | 2015-04-02 |
| EP2285740A1 (en) | 2011-02-23 |
| CN102066241A (zh) | 2011-05-18 |
| US9147877B2 (en) | 2015-09-29 |
| CN102066241B (zh) | 2013-11-13 |
| TW201010944A (en) | 2010-03-16 |
| CA2721029A1 (en) | 2009-10-22 |
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