KR101208324B1 - 클로로실란의 반응성 증류 - Google Patents

클로로실란의 반응성 증류 Download PDF

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KR101208324B1
KR101208324B1 KR1020077022338A KR20077022338A KR101208324B1 KR 101208324 B1 KR101208324 B1 KR 101208324B1 KR 1020077022338 A KR1020077022338 A KR 1020077022338A KR 20077022338 A KR20077022338 A KR 20077022338A KR 101208324 B1 KR101208324 B1 KR 101208324B1
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hydrochloric acid
distillation column
acid distillation
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subazeotropic
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KR20070114793A (ko
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앤드류 브루스 개미
크리스토퍼 대런 갓티
롤랜드 리 함
크리스토퍼 제임스 코젠스키
퀘버링 데니스 진 반
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다우 코닝 코포레이션
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/0834—Compounds having one or more O-Si linkage
    • C07F7/0838—Compounds with one or more Si-O-Si sequences
    • C07F7/0872—Preparation and treatment thereof
    • C07F7/0874—Reactions involving a bond of the Si-O-Si linkage
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/18—Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/12—Organo silicon halides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/21—Cyclic compounds having at least one ring containing silicon, but no carbon in the ring
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Silicon Polymers (AREA)
KR1020077022338A 2005-03-29 2006-03-15 클로로실란의 반응성 증류 Active KR101208324B1 (ko)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US66613905P 2005-03-29 2005-03-29
US60/666,139 2005-03-29
US67321305P 2005-04-20 2005-04-20
US60/673,213 2005-04-20

Publications (2)

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KR20070114793A KR20070114793A (ko) 2007-12-04
KR101208324B1 true KR101208324B1 (ko) 2012-12-05

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KR1020077022338A Active KR101208324B1 (ko) 2005-03-29 2006-03-15 클로로실란의 반응성 증류

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Country Link
US (1) US7479567B2 (enExample)
EP (1) EP1863823B1 (enExample)
JP (1) JP4388588B2 (enExample)
KR (1) KR101208324B1 (enExample)
CN (1) CN101133068B (enExample)
WO (1) WO2006104702A1 (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106006557A (zh) * 2016-05-18 2016-10-12 昆明理工大学 一种氯硅烷残液生产氯化氢气体的方法

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2007064888A2 (en) * 2005-11-30 2007-06-07 University Of Akron Synthesis of cycloaliphatic substituted silane monomers and polysiloxanes for photo-curing
CN102382305B (zh) * 2010-09-02 2013-01-02 上海安赐机械设备有限公司 一种烷基氯硅烷水解装置及其水解工艺
KR20130140827A (ko) * 2011-01-25 2013-12-24 다우 코닝 코포레이션 다이오르가노다이할로실란의 제조 방법
DE102013201851A1 (de) 2013-02-05 2014-08-21 Wacker Chemie Ag Hydrolyse von Organochlorsilanen im Rohrbündelreaktor
EP3473328A1 (en) * 2014-03-25 2019-04-24 Dow Silicones Corporation Method of separating volatile siloxane from a liquid feed mixture
CN106397474B (zh) * 2016-08-29 2018-11-09 山东东岳有机硅材料股份有限公司 一种降低二甲基二氯硅烷水解物中含酸量的方法
KR102269810B1 (ko) * 2017-05-16 2021-06-29 와커 헤미 아게 유기폴리실록산 수지의 제조 방법
CN112076529A (zh) * 2020-09-24 2020-12-15 南通星球石墨股份有限公司 一种脱除有机硅副产盐酸中硅氧烷的装置及方法
CN115197423A (zh) * 2021-04-09 2022-10-18 江西蓝星星火有机硅有限公司 有机硅线性体生产工艺
CN113880877B (zh) * 2021-11-12 2023-10-24 新疆晶硕新材料有限公司 二甲基二氯硅烷水解产物的处理方法和装置
CN113996256B (zh) * 2021-11-12 2023-11-14 新疆晶硕新材料有限公司 二甲基二氯硅烷水解产物的处理方法和装置
CN114011356B (zh) * 2021-11-12 2023-05-26 新疆晶硕新材料有限公司 二甲基二氯硅烷水解产物的处理方法和装置
CN115069182B (zh) * 2022-05-26 2024-02-27 中国化学赛鼎宁波工程有限公司 一种有机硅高沸物的处理系统及方法
CN115193146B (zh) * 2022-07-14 2024-01-12 内蒙古恒业成有机硅有限公司 一种二甲基二氯硅烷水解油水分层罐

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4382145A (en) 1981-09-02 1983-05-03 General Electric Company Method of hydrolyzing organochlorosilanes
US6225490B1 (en) 1997-05-28 2001-05-01 Shin-Etsu Chemical Co., Ltd. Continuous hydrolysis of organochlorosilanes
US7208617B2 (en) 2004-10-05 2007-04-24 Dow Corning Corporation Hydrolysis of chlorosilanes

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2719859A (en) * 1950-09-21 1955-10-04 Wacker Chemie Gmbh Method for the hydrolysis of organosilicon compounds
US3983148A (en) * 1975-08-29 1976-09-28 Union Carbide Corporation Process for producing cyclic siloxanes
US4609751A (en) * 1981-12-14 1986-09-02 General Electric Company Method of hydrolyzing chlorosilanes
GB2112407B (en) 1981-12-14 1985-06-19 Gen Electric Method of hydrolyzing chlorosilanes
JPH028223A (ja) * 1988-06-27 1990-01-11 Toshiba Silicone Co Ltd オルガノクロロシランの加水分解方法
US5075479A (en) * 1991-05-20 1991-12-24 Dow Corning Corporation Anhydrous hydrogen chloride evolving one-step process for producing siloxanes

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4382145A (en) 1981-09-02 1983-05-03 General Electric Company Method of hydrolyzing organochlorosilanes
US6225490B1 (en) 1997-05-28 2001-05-01 Shin-Etsu Chemical Co., Ltd. Continuous hydrolysis of organochlorosilanes
US7208617B2 (en) 2004-10-05 2007-04-24 Dow Corning Corporation Hydrolysis of chlorosilanes

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106006557A (zh) * 2016-05-18 2016-10-12 昆明理工大学 一种氯硅烷残液生产氯化氢气体的方法

Also Published As

Publication number Publication date
US20080154055A1 (en) 2008-06-26
WO2006104702A1 (en) 2006-10-05
KR20070114793A (ko) 2007-12-04
CN101133068A (zh) 2008-02-27
EP1863823A1 (en) 2007-12-12
US7479567B2 (en) 2009-01-20
JP2008534590A (ja) 2008-08-28
EP1863823B1 (en) 2012-09-26
JP4388588B2 (ja) 2009-12-24
CN101133068B (zh) 2012-11-07

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