CN101133068B - 反应性蒸馏氯代硅烷 - Google Patents

反应性蒸馏氯代硅烷 Download PDF

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Publication number
CN101133068B
CN101133068B CN2006800071072A CN200680007107A CN101133068B CN 101133068 B CN101133068 B CN 101133068B CN 2006800071072 A CN2006800071072 A CN 2006800071072A CN 200680007107 A CN200680007107 A CN 200680007107A CN 101133068 B CN101133068 B CN 101133068B
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CN
China
Prior art keywords
column
tower
fed
hcl
chlorosilanes
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CN2006800071072A
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English (en)
Chinese (zh)
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CN101133068A (zh
Inventor
A·B·甘米
C·D·加蒂
R·L·赫尔姆
C·J·科兹恩斯奇
D·G·万科沃林
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Dow Silicones Corp
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Dow Corning Corp
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Publication of CN101133068A publication Critical patent/CN101133068A/zh
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/0834—Compounds having one or more O-Si linkage
    • C07F7/0838—Compounds with one or more Si-O-Si sequences
    • C07F7/0872—Preparation and treatment thereof
    • C07F7/0874—Reactions involving a bond of the Si-O-Si linkage
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/18—Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/12—Organo silicon halides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/21—Cyclic compounds having at least one ring containing silicon, but no carbon in the ring
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Silicon Polymers (AREA)
CN2006800071072A 2005-03-29 2006-03-15 反应性蒸馏氯代硅烷 Active CN101133068B (zh)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US66613905P 2005-03-29 2005-03-29
US60/666,139 2005-03-29
US67321305P 2005-04-20 2005-04-20
US60/673,213 2005-04-20
PCT/US2006/009508 WO2006104702A1 (en) 2005-03-29 2006-03-15 Reactive distillation of chlorosilanes

Publications (2)

Publication Number Publication Date
CN101133068A CN101133068A (zh) 2008-02-27
CN101133068B true CN101133068B (zh) 2012-11-07

Family

ID=36617096

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2006800071072A Active CN101133068B (zh) 2005-03-29 2006-03-15 反应性蒸馏氯代硅烷

Country Status (6)

Country Link
US (1) US7479567B2 (enExample)
EP (1) EP1863823B1 (enExample)
JP (1) JP4388588B2 (enExample)
KR (1) KR101208324B1 (enExample)
CN (1) CN101133068B (enExample)
WO (1) WO2006104702A1 (enExample)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2007064888A2 (en) * 2005-11-30 2007-06-07 University Of Akron Synthesis of cycloaliphatic substituted silane monomers and polysiloxanes for photo-curing
CN102382305B (zh) * 2010-09-02 2013-01-02 上海安赐机械设备有限公司 一种烷基氯硅烷水解装置及其水解工艺
KR20130140827A (ko) * 2011-01-25 2013-12-24 다우 코닝 코포레이션 다이오르가노다이할로실란의 제조 방법
DE102013201851A1 (de) 2013-02-05 2014-08-21 Wacker Chemie Ag Hydrolyse von Organochlorsilanen im Rohrbündelreaktor
EP3473328A1 (en) * 2014-03-25 2019-04-24 Dow Silicones Corporation Method of separating volatile siloxane from a liquid feed mixture
CN106006557B (zh) * 2016-05-18 2018-06-15 昆明理工大学 一种氯硅烷残液生产氯化氢气体的方法
CN106397474B (zh) * 2016-08-29 2018-11-09 山东东岳有机硅材料股份有限公司 一种降低二甲基二氯硅烷水解物中含酸量的方法
KR102269810B1 (ko) * 2017-05-16 2021-06-29 와커 헤미 아게 유기폴리실록산 수지의 제조 방법
CN112076529A (zh) * 2020-09-24 2020-12-15 南通星球石墨股份有限公司 一种脱除有机硅副产盐酸中硅氧烷的装置及方法
CN115197423A (zh) * 2021-04-09 2022-10-18 江西蓝星星火有机硅有限公司 有机硅线性体生产工艺
CN113880877B (zh) * 2021-11-12 2023-10-24 新疆晶硕新材料有限公司 二甲基二氯硅烷水解产物的处理方法和装置
CN113996256B (zh) * 2021-11-12 2023-11-14 新疆晶硕新材料有限公司 二甲基二氯硅烷水解产物的处理方法和装置
CN114011356B (zh) * 2021-11-12 2023-05-26 新疆晶硕新材料有限公司 二甲基二氯硅烷水解产物的处理方法和装置
CN115069182B (zh) * 2022-05-26 2024-02-27 中国化学赛鼎宁波工程有限公司 一种有机硅高沸物的处理系统及方法
CN115193146B (zh) * 2022-07-14 2024-01-12 内蒙古恒业成有机硅有限公司 一种二甲基二氯硅烷水解油水分层罐

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3983148A (en) * 1975-08-29 1976-09-28 Union Carbide Corporation Process for producing cyclic siloxanes
US4382145A (en) * 1981-09-02 1983-05-03 General Electric Company Method of hydrolyzing organochlorosilanes

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2719859A (en) * 1950-09-21 1955-10-04 Wacker Chemie Gmbh Method for the hydrolysis of organosilicon compounds
US4609751A (en) * 1981-12-14 1986-09-02 General Electric Company Method of hydrolyzing chlorosilanes
GB2112407B (en) 1981-12-14 1985-06-19 Gen Electric Method of hydrolyzing chlorosilanes
JPH028223A (ja) * 1988-06-27 1990-01-11 Toshiba Silicone Co Ltd オルガノクロロシランの加水分解方法
US5075479A (en) * 1991-05-20 1991-12-24 Dow Corning Corporation Anhydrous hydrogen chloride evolving one-step process for producing siloxanes
JP3436075B2 (ja) 1997-05-28 2003-08-11 信越化学工業株式会社 オルガノクロロシランの連続加水分解方法
US7208617B2 (en) 2004-10-05 2007-04-24 Dow Corning Corporation Hydrolysis of chlorosilanes

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3983148A (en) * 1975-08-29 1976-09-28 Union Carbide Corporation Process for producing cyclic siloxanes
US4382145A (en) * 1981-09-02 1983-05-03 General Electric Company Method of hydrolyzing organochlorosilanes

Also Published As

Publication number Publication date
US20080154055A1 (en) 2008-06-26
WO2006104702A1 (en) 2006-10-05
KR101208324B1 (ko) 2012-12-05
KR20070114793A (ko) 2007-12-04
CN101133068A (zh) 2008-02-27
EP1863823A1 (en) 2007-12-12
US7479567B2 (en) 2009-01-20
JP2008534590A (ja) 2008-08-28
EP1863823B1 (en) 2012-09-26
JP4388588B2 (ja) 2009-12-24

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Address after: michigan

Patentee after: Dow organosilicon company

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Patentee before: Dow Corning Corporation

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