KR100966215B1 - 전기투석에 의한 오늄 하이드록사이드의 정제 - Google Patents

전기투석에 의한 오늄 하이드록사이드의 정제 Download PDF

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Publication number
KR100966215B1
KR100966215B1 KR1020047010494A KR20047010494A KR100966215B1 KR 100966215 B1 KR100966215 B1 KR 100966215B1 KR 1020047010494 A KR1020047010494 A KR 1020047010494A KR 20047010494 A KR20047010494 A KR 20047010494A KR 100966215 B1 KR100966215 B1 KR 100966215B1
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South Korea
Prior art keywords
quaternary ammonium
hydroxide
compartment
membrane
cathode
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KR1020047010494A
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English (en)
Korean (ko)
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KR20040082383A (ko
Inventor
로버트 제이. 레이터
켈리 헤프너
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사켐,인코포레이티드
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D61/00Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/42Electrodialysis; Electro-osmosis ; Electro-ultrafiltration; Membrane capacitive deionization
    • B01D61/44Ion-selective electrodialysis
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/82Purification; Separation; Stabilisation; Use of additives
    • C07C209/84Purification
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D61/00Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/42Electrodialysis; Electro-osmosis ; Electro-ultrafiltration; Membrane capacitive deionization
    • B01D61/44Ion-selective electrodialysis
    • B01D61/445Ion-selective electrodialysis with bipolar membranes; Water splitting
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/46Treatment of water, waste water, or sewage by electrochemical methods
    • C02F1/461Treatment of water, waste water, or sewage by electrochemical methods by electrolysis
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/46Treatment of water, waste water, or sewage by electrochemical methods
    • C02F1/469Treatment of water, waste water, or sewage by electrochemical methods by electrochemical separation, e.g. by electro-osmosis, electrodialysis, electrophoresis
    • C02F1/4693Treatment of water, waste water, or sewage by electrochemical methods by electrochemical separation, e.g. by electro-osmosis, electrodialysis, electrophoresis electrodialysis
    • C02F1/4695Treatment of water, waste water, or sewage by electrochemical methods by electrochemical separation, e.g. by electro-osmosis, electrodialysis, electrophoresis electrodialysis electrodeionisation
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/46Treatment of water, waste water, or sewage by electrochemical methods
    • C02F1/461Treatment of water, waste water, or sewage by electrochemical methods by electrolysis
    • C02F1/46104Devices therefor; Their operating or servicing
    • C02F1/46109Electrodes
    • C02F2001/46128Bipolar electrodes

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Water Supply & Treatment (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Urology & Nephrology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Electrochemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Environmental & Geological Engineering (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
  • Water Treatment By Electricity Or Magnetism (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Battery Electrode And Active Subsutance (AREA)
KR1020047010494A 2002-01-03 2002-11-27 전기투석에 의한 오늄 하이드록사이드의 정제 Expired - Fee Related KR100966215B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US10/038,537 US6787021B2 (en) 2002-01-03 2002-01-03 Purification of onium hydroxides by electrodialysis
US10/038,537 2002-01-03
PCT/US2002/038159 WO2003059824A1 (en) 2002-01-03 2002-11-27 Purification of onium hydroxides by electrodialysis

Publications (2)

Publication Number Publication Date
KR20040082383A KR20040082383A (ko) 2004-09-24
KR100966215B1 true KR100966215B1 (ko) 2010-06-25

Family

ID=21900512

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020047010494A Expired - Fee Related KR100966215B1 (ko) 2002-01-03 2002-11-27 전기투석에 의한 오늄 하이드록사이드의 정제

Country Status (13)

Country Link
US (1) US6787021B2 (https=)
EP (1) EP1472188B1 (https=)
JP (1) JP2005514447A (https=)
KR (1) KR100966215B1 (https=)
CN (1) CN1293231C (https=)
AT (1) ATE483514T1 (https=)
AU (1) AU2002346578A1 (https=)
CA (1) CA2478768C (https=)
DE (1) DE60237921D1 (https=)
IL (2) IL162691A0 (https=)
MY (1) MY122894A (https=)
TW (1) TWI230631B (https=)
WO (1) WO2003059824A1 (https=)

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US6582513B1 (en) * 1998-05-15 2003-06-24 Apollo Diamond, Inc. System and method for producing synthetic diamond
EP1856027B1 (en) * 2005-03-04 2016-04-20 Honeywell International Inc. Method for purifying quaternary onium salts
US7572379B2 (en) * 2005-09-02 2009-08-11 Sachem, Inc. Removal of metal ions from onium hydroxides and onium salt solutions
DE102009037954A1 (de) * 2009-08-18 2011-02-24 Voith Patent Gmbh Verfahren zur Rückgwinnung von Chemikalien aus bei der Erzeugung lignozellulosischer Faserstoffe anfallendem Abwasser
JP5909190B2 (ja) * 2009-11-04 2016-04-26 カウンスィル オブ サイエンティフィック アンド インダストリアル リサーチCouncil Of Scientific & Industrial Research 工業廃水からのジメチルスルホキシド(dmso)溶媒の回収のための電気透析−蒸留ハイブリッドプロセス
CN102373341A (zh) * 2010-08-12 2012-03-14 独立行政法人日本原子力研究开发机构 锂的回收方法及锂的回收装置
WO2012059133A1 (de) * 2010-11-05 2012-05-10 Voith Patent Gmbh Verfahren zur rückgewinnung von chemikalien aus bei der erzeugung lignozellulosischer faserstoffe anfallendem abwasser
CN102531927B (zh) * 2011-12-28 2013-09-11 浙江工业大学 一种利用双极膜电渗析制备四丙基氢氧化铵的方法
CN104292114B (zh) * 2013-07-19 2016-05-04 广州众合环保工程技术服务有限公司 一种鎓氢氧化物的制备方法
US9115050B2 (en) 2013-12-30 2015-08-25 Sachem, Inc. Process for improved recovery of onium hydroxide from compositions containing process residues
JP6197235B2 (ja) * 2014-06-26 2017-09-20 国立大学法人 奈良先端科学技術大学院大学 ナノ材料−ドーパント組成物複合体の製造方法、ナノ材料−ドーパント組成物複合体およびドーパント組成物
SG11201803576SA (en) * 2015-10-30 2018-05-30 China Petroleum & Chem Corp Method for wastewater treatment and the treatment system thereof, and method for the preparation of a molecular sieve and the preparation system
TWI622428B (zh) 2017-03-31 2018-05-01 財團法人工業技術研究院 電透析模組及電透析系統
CN108299209A (zh) * 2018-01-20 2018-07-20 盐城泛安化学有限公司 一种利用膜集成技术制备并浓缩四乙基氢氧化铵的方法
CN110318066B (zh) * 2019-06-20 2024-08-02 青岛鼎海电化学科技有限公司 一种四烷基氢氧化铵的制备方法
US12195370B2 (en) 2020-10-14 2025-01-14 Duke University Methods and systems for wastewater treatment

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20000035915A (ko) * 1996-08-30 2000-06-26 세이켐, 인코포레이티드. 전기화학 전지 내에서 오늄 히드록시드의 제조

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US4536269A (en) * 1983-05-02 1985-08-20 Allied Corporation Multichamber two-compartment electrodialytic water splitter and method of using same for acidification of aqueous soluble salts
JPS60131985A (ja) 1983-12-19 1985-07-13 Showa Denko Kk 高純度第4級アンモニウム水酸化物の製造法
US4714530A (en) 1986-07-11 1987-12-22 Southwestern Analytical Chemicals, Inc. Method for producing high purity quaternary ammonium hydroxides
US4938854A (en) 1988-11-28 1990-07-03 Southwestern Analytical Chemicals, Inc. Method for purifying quaternary ammonium hydroxides
US5135626A (en) * 1988-12-01 1992-08-04 Allied-Signal Inc. Method for purification of bases from materials comprising base and salt
JP3151043B2 (ja) * 1992-04-03 2001-04-03 株式会社トクヤマ 酸及びアルカリの製造方法
JPH06299385A (ja) * 1992-08-28 1994-10-25 Mitsubishi Gas Chem Co Inc 水酸化第四級アンモニウム水溶液および有機カルボン 酸の製造方法
KR100264643B1 (ko) 1992-11-10 2000-09-01 쓰라히데 죠오 수산화유기사급암모늄을 함유하는 폐액의 처리방법
US5753097A (en) 1996-10-03 1998-05-19 Sachem, Inc. Process for purifying hydroxide compounds
US5709790A (en) 1996-10-03 1998-01-20 Sachem, Inc. Electrochemical process for purifying hydroxide compounds
US5709789A (en) 1996-10-23 1998-01-20 Sachem, Inc. Electrochemical conversion of nitrogen containing gas to hydroxylamine and hydroxylammonium salts
US6217743B1 (en) * 1997-02-12 2001-04-17 Sachem, Inc. Process for recovering organic hydroxides from waste solutions
US5868916A (en) 1997-02-12 1999-02-09 Sachem, Inc. Process for recovering organic hydroxides from waste solutions
US5853555A (en) 1997-04-03 1998-12-29 Sachem, Inc. Synthesis of onium hydroxides from onium salts
US5959845A (en) 1997-09-18 1999-09-28 International Business Machines Corporation Universal chip carrier connector
JPH11106977A (ja) * 1997-09-30 1999-04-20 Asahi Glass Co Ltd 複極型イオン交換膜電解槽
GB2332210B (en) * 1997-12-10 2000-07-19 Toshiba Kk Processing method of waste water and processing apparatus thereof
US5968338A (en) * 1998-01-20 1999-10-19 Sachem, Inc. Process for recovering onium hydroxides from solutions containing onium compounds
US6207039B1 (en) 1998-04-07 2001-03-27 Sachem, Inc. Process for recovering onium hydroxides or onium salts from solutions containing onium compounds using electrochemical ion exchange
DE19856376A1 (de) * 1998-12-07 2000-06-08 Basf Ag Verfahren zur Herstellung oder Reinigung von Oniumhydroxiden mittels Elektrodialyse

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20000035915A (ko) * 1996-08-30 2000-06-26 세이켐, 인코포레이티드. 전기화학 전지 내에서 오늄 히드록시드의 제조

Also Published As

Publication number Publication date
TWI230631B (en) 2005-04-11
IL162691A0 (en) 2005-11-20
KR20040082383A (ko) 2004-09-24
CA2478768A1 (en) 2003-07-24
CN1612844A (zh) 2005-05-04
CN1293231C (zh) 2007-01-03
EP1472188B1 (en) 2010-10-06
EP1472188A4 (en) 2005-05-04
TW200302128A (en) 2003-08-01
IL162691A (en) 2006-12-31
US20030121787A1 (en) 2003-07-03
ATE483514T1 (de) 2010-10-15
DE60237921D1 (de) 2010-11-18
EP1472188A1 (en) 2004-11-03
US6787021B2 (en) 2004-09-07
JP2005514447A (ja) 2005-05-19
WO2003059824A1 (en) 2003-07-24
MY122894A (en) 2006-05-31
AU2002346578A1 (en) 2003-07-30
CA2478768C (en) 2008-10-21

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KR100462248B1 (ko) 오늄 화합물을 함유하는 용액으로부터 오늄 히드록시드를회수하는 방법
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