KR100729320B1 - 고순도 인산 및 그 제조 방법 - Google Patents

고순도 인산 및 그 제조 방법 Download PDF

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Publication number
KR100729320B1
KR100729320B1 KR1020057011686A KR20057011686A KR100729320B1 KR 100729320 B1 KR100729320 B1 KR 100729320B1 KR 1020057011686 A KR1020057011686 A KR 1020057011686A KR 20057011686 A KR20057011686 A KR 20057011686A KR 100729320 B1 KR100729320 B1 KR 100729320B1
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phosphoric acid
high purity
hydrogen sulfide
crude
gas
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Korean (ko)
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KR20050099497A (ko
Inventor
겐이찌 이시까와
게이조 요꼬이
고스께 다께우찌
유따까 구리따
헤이지 우찌야마
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니폰 가가쿠 고교 가부시키가이샤
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/18—Phosphoric acid
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/18—Phosphoric acid
    • C01B25/234—Purification; Stabilisation; Concentration
    • C01B25/237—Selective elimination of impurities
    • C01B25/238—Cationic impurities, e.g. arsenic compounds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/18—Phosphoric acid
    • C01B25/20—Preparation from elemental phosphorus or phosphoric anhydride
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/18—Phosphoric acid
    • C01B25/234—Purification; Stabilisation; Concentration
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/18—Phosphoric acid
    • C01B25/234—Purification; Stabilisation; Concentration
    • C01B25/235—Clarification; Stabilisation to prevent post-precipitation of dissolved impurities

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Weting (AREA)
  • Glass Compositions (AREA)
KR1020057011686A 2003-07-01 2004-06-28 고순도 인산 및 그 제조 방법 Expired - Lifetime KR100729320B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JPJP-P-2003-00189631 2003-07-01
JP2003189631A JP4316946B2 (ja) 2003-07-01 2003-07-01 高純度リン酸及びその製造方法

Publications (2)

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KR20050099497A KR20050099497A (ko) 2005-10-13
KR100729320B1 true KR100729320B1 (ko) 2007-06-15

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KR1020057011686A Expired - Lifetime KR100729320B1 (ko) 2003-07-01 2004-06-28 고순도 인산 및 그 제조 방법

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Country Link
US (1) US7470414B2 (https=)
EP (1) EP1640340B1 (https=)
JP (1) JP4316946B2 (https=)
KR (1) KR100729320B1 (https=)
CN (1) CN100340474C (https=)
TW (1) TWI272246B (https=)
WO (1) WO2005003026A1 (https=)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101955186B1 (ko) 2017-09-07 2019-03-07 손원일 초고순도 인산 제조용 반응기

Families Citing this family (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7824633B2 (en) * 2006-11-21 2010-11-02 Freeport-Mcmoran Corporation System and method for conversion of molybdenite to one or more molybdenum oxides
JP5242061B2 (ja) * 2007-02-08 2013-07-24 日本リファイン株式会社 複数の金属イオンを含むリン酸水溶液から精製リン酸を得る方法及び装置
JP2008247733A (ja) * 2007-03-14 2008-10-16 Niro Process Technology Bv リン酸リッチストリームの精製
TWI391320B (zh) * 2008-10-16 2013-04-01 Ecophos S A 高純度磷酸生產之製程
CN101531353B (zh) * 2009-04-28 2013-09-25 云南省化工研究院 一种用黄磷直接制取电子级磷酸的方法
CN101691213B (zh) * 2009-10-10 2011-07-20 武汉工程大学 脱除湿法磷酸中金属离子的工艺
JP5554165B2 (ja) * 2010-07-09 2014-07-23 日本化学工業株式会社 高純度元素リンの製造方法および高純度リン酸の製造方法
WO2013142022A1 (en) 2012-03-23 2013-09-26 Kennecott Utah Copper Llc Process for the conversion of molybdenite to molybdenum oxide
DE102014006278B3 (de) * 2014-05-02 2015-02-26 Remondis Aqua Gmbh & Co. Kg Verfahren zur Reinigung von Roh-Phosphorsäure (z.B. MGA-Säure) durch Zugabe von Aschen aus Abfall-Verbrennungsanlagen umfassend die Gewinnung von reiner Phosphorsäure, Kalziumsulfat, wasserlöslichen Kalziumhydrogenphosphaten und Metallsalz-Lösung
CN104588381A (zh) * 2014-12-30 2015-05-06 铜陵鑫克精细化工有限责任公司 溶剂萃取法净化湿法磷酸的萃取装置的清洗方法
KR102633772B1 (ko) * 2018-04-12 2024-02-05 오씨아이 주식회사 고순도 인산의 제조 방법
KR102818597B1 (ko) 2018-09-12 2025-06-10 후지필름 일렉트로닉 머티리얼스 유.에스.에이., 아이엔씨. 식각 조성물
CN108910850A (zh) * 2018-09-25 2018-11-30 湖北兴福电子材料有限公司 一种热法电子级磷酸脱砷方法
CN112279230A (zh) * 2019-07-23 2021-01-29 东泰高科装备科技有限公司 磷酸的制备方法
CN113955731B (zh) * 2021-12-08 2024-03-01 昆明云盘山农牧科技有限公司 一种含有颗粒状饲料级磷酸二氢钙制备方法
PL440852A1 (pl) * 2022-04-04 2023-10-09 Alventa Spółka Akcyjna Sposób oczyszczania kwasu fosforowego(V) na potrzeby krystalizacji statycznej do otrzymywania kwasu jakości odpowiedniej dla branży półprzewodników
CN117963858A (zh) * 2024-02-01 2024-05-03 云南云天化股份有限公司 一种以工业黄磷制备的高纯多聚磷酸方法
CN119797293A (zh) * 2025-01-14 2025-04-11 广西钦州澄星化工科技有限公司 一种铁离子低含量的磷酸生产方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS62191409A (ja) 1986-02-13 1987-08-21 ヘキスト・アクチエンゲゼルシヤフト 無機酸から重金属を除去する方法
JPH01131009A (ja) * 1987-10-13 1989-05-23 Fmc Corp 電気半導体用りん酸の精製法
JPH06171913A (ja) * 1992-12-10 1994-06-21 Mitsui Toatsu Chem Inc 燐酸液の改質方法

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2174158A (en) 1937-11-11 1939-09-26 Du Pont Phosphoric acid purification
JPS4414692Y1 (https=) 1966-12-15 1969-06-23
DE2109970C3 (de) 1971-03-03 1980-03-20 Hoechst Ag, 6000 Frankfurt Verfahren und Vorrichtung zur Entarsenierung von Polyphosphorsäure
JPS5673608A (en) * 1979-11-20 1981-06-18 Mitsui Toatsu Chem Inc Removing method for organic matter in wet process phosphoric acid
DE3134847A1 (de) * 1981-09-03 1983-03-17 Hoechst Ag, 6000 Frankfurt "verfahren zur gewinnung cadmium-freier rohphosphorsaeure"
US4816241A (en) * 1982-02-16 1989-03-28 J. R. Simplot Co. Gaseous reduction of phosphoric acid
JPH0648712A (ja) 1992-07-31 1994-02-22 Mitsui Toatsu Chem Inc 燐酸液の精製法
CN1139072A (zh) * 1995-06-26 1997-01-01 广东湛化企业集团公司 湿法磷酸净化脱氟、除重金属技术
CN1180658A (zh) * 1997-11-18 1998-05-06 张瑞宁 高纯磷酸生产新工艺
DE69932857T2 (de) * 1998-12-28 2007-03-01 Toyo Boseki K.K. Verfahren zur reinigung von phosphorsäure

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS62191409A (ja) 1986-02-13 1987-08-21 ヘキスト・アクチエンゲゼルシヤフト 無機酸から重金属を除去する方法
JPH01131009A (ja) * 1987-10-13 1989-05-23 Fmc Corp 電気半導体用りん酸の精製法
JPH06171913A (ja) * 1992-12-10 1994-06-21 Mitsui Toatsu Chem Inc 燐酸液の改質方法

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101955186B1 (ko) 2017-09-07 2019-03-07 손원일 초고순도 인산 제조용 반응기

Also Published As

Publication number Publication date
US7470414B2 (en) 2008-12-30
CN1717366A (zh) 2006-01-04
WO2005003026A1 (ja) 2005-01-13
EP1640340B1 (en) 2012-08-01
JP2005022919A (ja) 2005-01-27
CN100340474C (zh) 2007-10-03
EP1640340A4 (en) 2007-07-18
KR20050099497A (ko) 2005-10-13
TW200502163A (en) 2005-01-16
US20060073088A1 (en) 2006-04-06
JP4316946B2 (ja) 2009-08-19
TWI272246B (en) 2007-02-01
EP1640340A1 (en) 2006-03-29

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