JPWO2020241052A5 - - Google Patents
Download PDFInfo
- Publication number
- JPWO2020241052A5 JPWO2020241052A5 JP2021522671A JP2021522671A JPWO2020241052A5 JP WO2020241052 A5 JPWO2020241052 A5 JP WO2020241052A5 JP 2021522671 A JP2021522671 A JP 2021522671A JP 2021522671 A JP2021522671 A JP 2021522671A JP WO2020241052 A5 JPWO2020241052 A5 JP WO2020241052A5
- Authority
- JP
- Japan
- Prior art keywords
- titanium
- silicon oxide
- quaternary ammonium
- hydrocarbon group
- containing silicon
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 claims description 29
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 20
- -1 amine compound Chemical class 0.000 claims description 20
- 239000003795 chemical substances by application Substances 0.000 claims description 20
- 229910052719 titanium Inorganic materials 0.000 claims description 20
- 239000010936 titanium Substances 0.000 claims description 20
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 19
- 229910052814 silicon oxide Inorganic materials 0.000 claims description 19
- 150000003856 quaternary ammonium compounds Chemical class 0.000 claims description 17
- 239000007787 solid Substances 0.000 claims description 13
- 239000002994 raw material Substances 0.000 claims description 9
- 150000002430 hydrocarbons Chemical group 0.000 claims description 8
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 7
- 239000000203 mixture Substances 0.000 claims description 7
- 229910052710 silicon Inorganic materials 0.000 claims description 7
- 239000010703 silicon Substances 0.000 claims description 7
- 150000001336 alkenes Chemical class 0.000 claims description 6
- 238000004519 manufacturing process Methods 0.000 claims description 6
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 claims description 6
- 125000001453 quaternary ammonium group Chemical group 0.000 claims description 5
- 239000004215 Carbon black (E152) Substances 0.000 claims description 4
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 4
- 229930195733 hydrocarbon Natural products 0.000 claims description 4
- 239000002904 solvent Substances 0.000 claims description 4
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 3
- FRIBMENBGGCKPD-UHFFFAOYSA-N 3-(2,3-dimethoxyphenyl)prop-2-enal Chemical group COC1=CC=CC(C=CC=O)=C1OC FRIBMENBGGCKPD-UHFFFAOYSA-N 0.000 claims description 2
- RLGQACBPNDBWTB-UHFFFAOYSA-N cetyltrimethylammonium ion Chemical compound CCCCCCCCCCCCCCCC[N+](C)(C)C RLGQACBPNDBWTB-UHFFFAOYSA-N 0.000 claims description 2
- 150000002118 epoxides Chemical class 0.000 claims description 2
- NHLUVTZJQOJKCC-UHFFFAOYSA-N n,n-dimethylhexadecan-1-amine Chemical compound CCCCCCCCCCCCCCCCN(C)C NHLUVTZJQOJKCC-UHFFFAOYSA-N 0.000 claims description 2
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 claims description 2
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 claims description 2
- 238000006884 silylation reaction Methods 0.000 claims description 2
- 239000004711 α-olefin Substances 0.000 claims description 2
- 125000001183 hydrocarbyl group Chemical group 0.000 description 4
- 125000000217 alkyl group Chemical group 0.000 description 2
- 229940100198 alkylating agent Drugs 0.000 description 2
- 239000002168 alkylating agent Substances 0.000 description 2
- GZUXJHMPEANEGY-UHFFFAOYSA-N bromomethane Chemical compound BrC GZUXJHMPEANEGY-UHFFFAOYSA-N 0.000 description 2
- NRKYWOKHZRQRJR-UHFFFAOYSA-N 2,2,2-trifluoroacetamide Chemical compound NC(=O)C(F)(F)F NRKYWOKHZRQRJR-UHFFFAOYSA-N 0.000 description 1
- CMXKINNDZCNCEI-UHFFFAOYSA-N 2,2,3,3,4,4,4-heptafluoro-n-methyl-n-trimethylsilylbutanamide Chemical compound C[Si](C)(C)N(C)C(=O)C(F)(F)C(F)(F)C(F)(F)F CMXKINNDZCNCEI-UHFFFAOYSA-N 0.000 description 1
- XCOBLONWWXQEBS-KPKJPENVSA-N N,O-bis(trimethylsilyl)trifluoroacetamide Chemical compound C[Si](C)(C)O\C(C(F)(F)F)=N\[Si](C)(C)C XCOBLONWWXQEBS-KPKJPENVSA-N 0.000 description 1
- MSPCIZMDDUQPGJ-UHFFFAOYSA-N N-methyl-N-(trimethylsilyl)trifluoroacetamide Chemical compound C[Si](C)(C)N(C)C(=O)C(F)(F)F MSPCIZMDDUQPGJ-UHFFFAOYSA-N 0.000 description 1
- 125000003668 acetyloxy group Chemical group [H]C([H])([H])C(=O)O[*] 0.000 description 1
- 125000003342 alkenyl group Chemical group 0.000 description 1
- 125000003545 alkoxy group Chemical group 0.000 description 1
- 125000003277 amino group Chemical group 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- NEHMKBQYUWJMIP-NJFSPNSNSA-N chloro(114C)methane Chemical compound [14CH3]Cl NEHMKBQYUWJMIP-NJFSPNSNSA-N 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical group 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- INQOMBQAUSQDDS-UHFFFAOYSA-N iodomethane Chemical compound IC INQOMBQAUSQDDS-UHFFFAOYSA-N 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
- 229940102396 methyl bromide Drugs 0.000 description 1
- QHUOBLDKFGCVCG-UHFFFAOYSA-N n-methyl-n-trimethylsilylacetamide Chemical compound CC(=O)N(C)[Si](C)(C)C QHUOBLDKFGCVCG-UHFFFAOYSA-N 0.000 description 1
- LWFWUJCJKPUZLV-UHFFFAOYSA-N n-trimethylsilylacetamide Chemical compound CC(=O)N[Si](C)(C)C LWFWUJCJKPUZLV-UHFFFAOYSA-N 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- FZHAPNGMFPVSLP-UHFFFAOYSA-N silanamine Chemical class [SiH3]N FZHAPNGMFPVSLP-UHFFFAOYSA-N 0.000 description 1
- 150000003377 silicon compounds Chemical group 0.000 description 1
- 125000004469 siloxy group Chemical group [SiH3]O* 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- SIOVKLKJSOKLIF-HJWRWDBZSA-N trimethylsilyl (1z)-n-trimethylsilylethanimidate Chemical compound C[Si](C)(C)OC(/C)=N\[Si](C)(C)C SIOVKLKJSOKLIF-HJWRWDBZSA-N 0.000 description 1
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2019100506 | 2019-05-29 | ||
| JP2019100506 | 2019-05-29 | ||
| PCT/JP2020/015413 WO2020241052A1 (ja) | 2019-05-29 | 2020-04-03 | チタン含有珪素酸化物の製造方法、エポキシドの製造方法、及びチタン含有珪素酸化物 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JPWO2020241052A1 JPWO2020241052A1 (https=) | 2020-12-03 |
| JPWO2020241052A5 true JPWO2020241052A5 (https=) | 2023-03-06 |
| JP7539876B2 JP7539876B2 (ja) | 2024-08-26 |
Family
ID=73553402
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2021522671A Active JP7539876B2 (ja) | 2019-05-29 | 2020-04-03 | チタン含有珪素酸化物の製造方法、エポキシドの製造方法、及びチタン含有珪素酸化物 |
Country Status (6)
| Country | Link |
|---|---|
| EP (1) | EP3978435A4 (https=) |
| JP (1) | JP7539876B2 (https=) |
| KR (1) | KR102811135B1 (https=) |
| CN (1) | CN113905987B (https=) |
| SA (1) | SA521430687B1 (https=) |
| WO (1) | WO2020241052A1 (https=) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN118270801A (zh) * | 2022-12-30 | 2024-07-02 | 中国石油天然气集团有限公司 | 一种钛硅分子筛及其制备方法和应用 |
| WO2024262456A1 (ja) * | 2023-06-22 | 2024-12-26 | 住友化学株式会社 | チタン含有珪素酸化物 |
Family Cites Families (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5143879A (en) | 1991-07-18 | 1992-09-01 | Mobil Oil Corporation | Method to recover organic templates from freshly synthesized molecular sieves |
| JP3731384B2 (ja) * | 1998-08-04 | 2006-01-05 | 住友化学株式会社 | チタン含有珪素酸化物触媒、該触媒の製造方法及びプロピレンオキサイドの製造方法 |
| ES2160044B1 (es) * | 1999-03-16 | 2002-06-16 | Univ Valencia Politecnica | Oxidacion de *-pineno. |
| JP3797107B2 (ja) * | 2000-02-02 | 2006-07-12 | 住友化学株式会社 | 触媒成型体、該触媒成型体の製造方法及びオキシラン化合物の製造方法 |
| JP4265212B2 (ja) * | 2002-12-19 | 2009-05-20 | 住友化学株式会社 | チタン含有珪素酸化物触媒の製造方法 |
| JP4834982B2 (ja) * | 2004-12-06 | 2011-12-14 | 住友化学株式会社 | チタン含有珪素酸化物触媒の製造方法及び触媒 |
| US9096711B2 (en) * | 2009-04-29 | 2015-08-04 | Dsm Ip Assets B.V. | Powder coating composition comprising a polyester and a crosslinker with oxirane groups providing improved corrosion resistance to a substrate coated therewith |
| EP2504098B1 (en) * | 2009-11-27 | 2016-07-06 | Basf Se | Process for the preparation of a titanium zeolite catalyst |
| WO2012074033A1 (ja) * | 2010-11-30 | 2012-06-07 | 住友化学株式会社 | チタン含有珪素酸化物成形体の製造方法及びオキシラン化合物の製造方法 |
| CN102807537B (zh) * | 2011-06-02 | 2014-08-06 | 中国石油化工股份有限公司 | 制备环氧丙烷的方法 |
| EP2841383B1 (en) * | 2012-04-24 | 2016-11-09 | Basf Se | Zeolitic materials and methods for their preparation using alkenyltrialkylammonium compounds |
| CN104540931A (zh) * | 2012-05-30 | 2015-04-22 | 科莱恩金融(Bvi)有限公司 | 包含n-甲基-n-酰基葡糖胺的组合物 |
| DE102014222042A1 (de) * | 2013-10-29 | 2015-04-30 | China Petroleum And Chemical Corporation | Titansilikalit-Molekularsieb und dessen Synthese |
| CN104528761B (zh) * | 2014-12-25 | 2016-08-24 | 中国天辰工程有限公司 | 一种高骨架钛含量钛硅分子筛的合成方法 |
| CN105236442A (zh) * | 2015-08-20 | 2016-01-13 | 中国天辰工程有限公司 | 一种Ti-MWW分子筛催化剂的制备方法 |
| TWI628146B (zh) * | 2016-11-28 | 2018-07-01 | 東聯化學股份有限公司 | Preparation method and application of titanium-containing cerium oxide material with high thermal stability |
| EP3330247B1 (de) * | 2016-12-02 | 2019-05-08 | Evonik Degussa GmbH | Katalytische oxidation von 3,5,5-trimethylcyclohexa-3-en-1-on (beta-isophoron) mit wasserstoffperoxid zu 2,6,6-trimethyl-2-cyclohexene-1,4-dion (keto-isophoron) |
| KR102493560B1 (ko) * | 2017-04-07 | 2023-01-30 | 스미또모 가가꾸 가부시끼가이샤 | 티탄 함유 규소 산화물의 제조 방법, 에폭사이드의 제조 방법, 및 티탄 함유 규소 산화물 |
-
2020
- 2020-04-03 EP EP20812583.1A patent/EP3978435A4/en active Pending
- 2020-04-03 KR KR1020217037451A patent/KR102811135B1/ko active Active
- 2020-04-03 WO PCT/JP2020/015413 patent/WO2020241052A1/ja not_active Ceased
- 2020-04-03 JP JP2021522671A patent/JP7539876B2/ja active Active
- 2020-04-03 CN CN202080039822.4A patent/CN113905987B/zh active Active
-
2021
- 2021-10-25 SA SA521430687A patent/SA521430687B1/ar unknown
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JPWO2020241052A5 (https=) | ||
| US4736049A (en) | Addition reaction method | |
| Bassindale et al. | Reaction mechanisms of nucleophilic attack at silicon | |
| US4746752A (en) | Preparation of hydrogenosilanes by redistribution | |
| EP0138669B1 (fr) | Procédé de fabrication de silane à partir de méthyldichlorosilane et de chlorosilanes | |
| CA1247325A (fr) | Procede de fabrication de silanes hydrogenes par redistribution | |
| EP3096879B1 (en) | Method of preparing epoxidation catalysts | |
| CN100516075C (zh) | 制造带有氨基的硅化合物的方法 | |
| JP7539876B2 (ja) | チタン含有珪素酸化物の製造方法、エポキシドの製造方法、及びチタン含有珪素酸化物 | |
| JP2012229186A (ja) | 低分子量シロキサン化合物の製造方法 | |
| JP4803395B2 (ja) | ヒドロキシル基のシリル化方法 | |
| JPS61205287A (ja) | アミノ基含有有機ケイ素化合物の製造法 | |
| JP4527351B2 (ja) | 改善されたオルガノシラン製造方法 | |
| JP4803381B2 (ja) | アミノアルキルシラン化合物の製造方法 | |
| JP6970739B2 (ja) | チタン含有珪素酸化物の製造方法、エポキシドの製造方法、及びチタン含有珪素酸化物 | |
| JP2000169131A (ja) | シラン化合物の不均化反応生成物の製造方法 | |
| JP2585295B2 (ja) | ビニルシラン類の製造方法 | |
| JPH05286985A (ja) | 有機ケイ素化合物の製造方法 | |
| JPH01117890A (ja) | シラン化合物の製造方法 | |
| JPH0344079B2 (https=) | ||
| JP2000178019A (ja) | シラン化合物の不均化反応生成物の製造方法 | |
| JP7476777B2 (ja) | 含窒素オルガノキシシラン化合物の製造方法 | |
| JP6531656B2 (ja) | 含窒素オルガノキシシラン化合物の製造方法 | |
| JPS5924996B2 (ja) | 活性水素含有化合物のシリル化法 | |
| ATE71949T1 (de) | Verfahren zur herstellung von organohalogenensilanen. |