CN113905987B - 含钛的硅氧化物的制造方法、环氧化物的制造方法和含钛的硅氧化物 - Google Patents

含钛的硅氧化物的制造方法、环氧化物的制造方法和含钛的硅氧化物 Download PDF

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Publication number
CN113905987B
CN113905987B CN202080039822.4A CN202080039822A CN113905987B CN 113905987 B CN113905987 B CN 113905987B CN 202080039822 A CN202080039822 A CN 202080039822A CN 113905987 B CN113905987 B CN 113905987B
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Prior art keywords
titanium
silicon oxide
containing silicon
template
quaternary ammonium
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CN113905987A (zh
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的场元志
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Sumitomo Chemical Co Ltd
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Sumitomo Chemical Co Ltd
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0018—Addition of a binding agent or of material, later completely removed among others as result of heat treatment, leaching or washing,(e.g. forming of pores; protective layer, desintegrating by heat)
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B01J21/063—Titanium; Oxides or hydroxides thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B01J21/08—Silica
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/03—Catalysts comprising molecular sieves not having base-exchange properties
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/89—Silicates, aluminosilicates or borosilicates of titanium, zirconium or hafnium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/03—Precipitation; Co-precipitation
    • B01J37/031—Precipitation
    • B01J37/033—Using Hydrolysis
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/04—Mixing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
    • C01B37/005—Silicates, i.e. so-called metallosilicalites or metallozeosilites
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/19—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with organic hydroperoxides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
    • C07D303/02—Compounds containing oxirane rings
    • C07D303/04—Compounds containing oxirane rings containing only hydrogen and carbon atoms in addition to the ring oxygen atoms
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/10—After treatment, characterised by the effect to be obtained
    • B01J2229/12—After treatment, characterised by the effect to be obtained to alter the outside of the crystallites, e.g. selectivation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/32—Reaction with silicon compounds, e.g. TEOS, siliconfluoride

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Epoxy Compounds (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Catalysts (AREA)
CN202080039822.4A 2019-05-29 2020-04-03 含钛的硅氧化物的制造方法、环氧化物的制造方法和含钛的硅氧化物 Active CN113905987B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2019-100506 2019-05-29
JP2019100506 2019-05-29
PCT/JP2020/015413 WO2020241052A1 (ja) 2019-05-29 2020-04-03 チタン含有珪素酸化物の製造方法、エポキシドの製造方法、及びチタン含有珪素酸化物

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CN113905987A CN113905987A (zh) 2022-01-07
CN113905987B true CN113905987B (zh) 2024-10-18

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EP (1) EP3978435A4 (https=)
JP (1) JP7539876B2 (https=)
KR (1) KR102811135B1 (https=)
CN (1) CN113905987B (https=)
SA (1) SA521430687B1 (https=)
WO (1) WO2020241052A1 (https=)

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CN118270801A (zh) * 2022-12-30 2024-07-02 中国石油天然气集团有限公司 一种钛硅分子筛及其制备方法和应用
WO2024262456A1 (ja) * 2023-06-22 2024-12-26 住友化学株式会社 チタン含有珪素酸化物

Citations (1)

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JP2001286768A (ja) * 2000-02-02 2001-10-16 Sumitomo Chem Co Ltd 触媒成型体、該触媒成型体の製造方法及びオキシラン化合物の製造方法

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US5143879A (en) 1991-07-18 1992-09-01 Mobil Oil Corporation Method to recover organic templates from freshly synthesized molecular sieves
JP3731384B2 (ja) * 1998-08-04 2006-01-05 住友化学株式会社 チタン含有珪素酸化物触媒、該触媒の製造方法及びプロピレンオキサイドの製造方法
ES2160044B1 (es) * 1999-03-16 2002-06-16 Univ Valencia Politecnica Oxidacion de *-pineno.
JP4265212B2 (ja) * 2002-12-19 2009-05-20 住友化学株式会社 チタン含有珪素酸化物触媒の製造方法
JP4834982B2 (ja) * 2004-12-06 2011-12-14 住友化学株式会社 チタン含有珪素酸化物触媒の製造方法及び触媒
US9096711B2 (en) * 2009-04-29 2015-08-04 Dsm Ip Assets B.V. Powder coating composition comprising a polyester and a crosslinker with oxirane groups providing improved corrosion resistance to a substrate coated therewith
EP2504098B1 (en) * 2009-11-27 2016-07-06 Basf Se Process for the preparation of a titanium zeolite catalyst
WO2012074033A1 (ja) * 2010-11-30 2012-06-07 住友化学株式会社 チタン含有珪素酸化物成形体の製造方法及びオキシラン化合物の製造方法
CN102807537B (zh) * 2011-06-02 2014-08-06 中国石油化工股份有限公司 制备环氧丙烷的方法
EP2841383B1 (en) * 2012-04-24 2016-11-09 Basf Se Zeolitic materials and methods for their preparation using alkenyltrialkylammonium compounds
CN104540931A (zh) * 2012-05-30 2015-04-22 科莱恩金融(Bvi)有限公司 包含n-甲基-n-酰基葡糖胺的组合物
DE102014222042A1 (de) * 2013-10-29 2015-04-30 China Petroleum And Chemical Corporation Titansilikalit-Molekularsieb und dessen Synthese
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CN105236442A (zh) * 2015-08-20 2016-01-13 中国天辰工程有限公司 一种Ti-MWW分子筛催化剂的制备方法
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KR102493560B1 (ko) * 2017-04-07 2023-01-30 스미또모 가가꾸 가부시끼가이샤 티탄 함유 규소 산화물의 제조 방법, 에폭사이드의 제조 방법, 및 티탄 함유 규소 산화물

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Publication number Publication date
CN113905987A (zh) 2022-01-07
EP3978435A4 (en) 2023-06-14
EP3978435A1 (en) 2022-04-06
JPWO2020241052A1 (https=) 2020-12-03
JP7539876B2 (ja) 2024-08-26
WO2020241052A1 (ja) 2020-12-03
SA521430687B1 (ar) 2024-06-02
KR102811135B1 (ko) 2025-05-21
KR20220014870A (ko) 2022-02-07

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