JPWO2016002752A1 - 水性化粧料 - Google Patents
水性化粧料 Download PDFInfo
- Publication number
- JPWO2016002752A1 JPWO2016002752A1 JP2016531380A JP2016531380A JPWO2016002752A1 JP WO2016002752 A1 JPWO2016002752 A1 JP WO2016002752A1 JP 2016531380 A JP2016531380 A JP 2016531380A JP 2016531380 A JP2016531380 A JP 2016531380A JP WO2016002752 A1 JPWO2016002752 A1 JP WO2016002752A1
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- Prior art keywords
- powder
- hydrophobic
- mass
- aqueous
- water
- Prior art date
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Abstract
Description
この組成物においては、ポリエーテル変性シリコーンはシリコーン油と疎水性粉末粒子を含む油相をゲル化するためのゲル化剤として作用し、油相中の疎水性粉末粒子からのイオン溶出を防ぐことによって水相中のイオン性高分子による増粘を安定化している。しかし、油相中での粉末の分散は従来の機械力によって行われているため、疎水性粉末粒子を十分に分散させるためには、分散媒として多量のシリコーン油を配合しなければならず、総油分量が増えてみずみずしい使用性を実現しにくいのは特許文献1と同様である。さらに、疎水性粉末粒子が油相中の油を吸収することで疎水性粉末特有のなめらかな使用感が損なわれる場合がある。
しかし、特許文献3〜5のいずれにも、疎水化処理金属酸化物を高配合する方法については何ら教示されていない。逆に、特許文献3には、疎水化処理を施したタルクを配合した場合には疎水化処理していないタルクを配合した場合に比較して乳化安定性が悪くなることが示され(比較例4)、特許文献5では、微粒子酸化チタンを配合すると使用性が低下することが記載されている(比較例2)。
(A)0.1〜5質量%のHLB(Si)が5〜14のポリエーテル変性シリコーン、
(B)親水性増粘剤の1種又は2種以上、
(C)ポリオール及び/又はエチルアルコール、
(D)金属石鹸以外で疎水化処理された金属酸化物、疎水性の有機粉末、シリコーン粉末から選ばれる1種又は2種以上の疎水性粉末を含有し、
(D)疎水性粉末が水相に分散していることを特徴とする水性化粧料、を要旨とするものである。
なお、本発明において、水性化粧料とは、化粧料全体の50質量%以上を水が占める化粧料を意味し、(1)基剤が水性成分のみからなる化粧料(実質的に水性成分と粉末成分とからなる化粧料)の態様、及び、(2)水性成分を外相とする水中油型乳化化粧料の態様を含む。即ち、「粉末が水相に分散している」とは、前記(1)の態様では化粧料全体に分散していること、前記(2)の態様では外相(水相)に分散していることを意味する。
本発明の水性化粧料における(A)ポリエーテル変性シリコーンは、ポリオキシエチレン(POE)及びポリオキシプロピレン(POP)から選択されるポリオキシアルキレン基を有するシリコーン誘導体である。特に、下記一般式で表されるポリエーテル変性シリコーンが好ましい。
・商品名BY11−030(東レ・ダウコーニング社製:PEG/PPG−19/19ジメチコン、HLB(Si)=7.7)、
・商品名SH3773M(東レ・ダウコーニング社製:PEG−12ジメチコン、HLB(Si)=7.7)、
・商品名BY25−339(東レ・ダウコーニング社製:PEG/PPG−30/10ジメチコン、HLB(Si)=12.2)、
・商品名KF6011(信越化学工業株式会社製:PEG−11メチルエーテルジメチコン、HLB(Si)=12.7)
等を挙げることができる。
本発明の水性化粧料における(B)親水性増粘剤は、化粧品に通常使用されるものであれば特に限定されない。例えば、天然又は半合成の水溶性高分子、合成の水溶性高分子、無機の水溶性高分子等を挙げることができる。
このようなポリアクリルアミド化合物の具体例としては、ビニルピロリドン/2−アクリルアミド−2−メチルプロパンスルホン酸(塩)共重合体、ジメチルアクリルアミド/2−アクリルアミド−2−メチルプロパンスルホン酸(塩)共重合体、アクリルアミド/2−アクリルアミド−2−メチルプロパンスルホン酸共重合体、メチレンビスアクリルアミドでクロスリンクさせたジメチルアクリルアミド/2−アクリルアミド−2−メチルプロパンスルホン酸のクロスポリマー、ポリアクリルアミドとポリアクリル酸ナトリウムの混合物、アクリル酸ナトリウム/2−アクリルアミド−2−メチルプロパンスルホン酸共重合体、アクリル酸ヒドロキシエチル/2−アクリルアミド−2−メチルプロパンスルホン酸(塩)共重合体、ポリアクリル酸アンモニウム、ポリアクリルアミド/アクリル酸アンモニウム共重合体、アクリルアミド/アクリル酸ナトリウム共重合体等が挙げられる。ただし、これらの例示に限定されるものではない。
本発明の水性化粧料は、さらに(C)ポリオール及び/又はエチルアルコールを必須成分として含有する。
本発明で使用されるポリオールは、化粧品に通常用いられるものであれば特に限定されないが、例えば、グリセリン、1,3−ブチレングリコール、ジプロピレングリコール、プロピレングリコール等を挙げることができる。
本発明の水性化粧料に配合する(D)疎水性粉末は、(D1)金属石鹸以外で疎水化処理された金属酸化物、(D2)疎水性の有機粉末、(D3)シリコーン粉末から選択される1種又は2種以上である。
疎水化処理金属酸化物の基材としては、例えば、酸化チタン、酸化鉄、酸化マグネシウム、酸化亜鉛、酸化カルシウム、酸化アルミニウム等が挙げられる。また、複数の基材からなる複合粉末粒子も用いることができる。
シリコーン処理としては、メチルハイドロゲンポリシロキサン、ジメチルポリシロキサン(ジメチコン)、メチルフェニルポリシロキサン等のシリコーンオイル;メチルトリエトキシシラン、エチルトリエトキシシラン、ヘキシルトリエトキシシラン、オクチルトリエトキシシラン等のアルキルシラン;トリフルオロメチルエチルトリメトキシシラン、ヘプタデカフルオロデシルトリメトキシシラン等のフルオロアルキルシラン等による処理が挙げられる。
(D2)疎水性の有機粉末の市販品として、例えば、マツモトマイクロスフェアーM−330(松本油脂製薬株式会社製)、プラスティックパウダーD−400、プラスティックパウダーD−800(東色ピグメント株式会社製)等が挙げられる。
また、水性化粧料が水中油型乳化組成物の形態である場合には、(B)親水性増粘剤を含む水相部と、油相部とをそれぞれ調製し、油相部を水相部に加えて乳化して水中油型乳化組成物(基剤)を調製し、一方で、(A)ポリエーテル変性シリコーン、(C)ポリオール及び/又はエチルアルコール、(D)疎水性粉末を攪拌混合して粉末部を調製し、これを前記乳化物(基剤)に混合することによって調製することができる。
下記の表1に掲げた組成を有する水相部、粉末部をそれぞれ均一になるまで攪拌混合し、粉末部を水相部に添加することにより水性化粧料を調製した。得られた化粧料を外観観察及び光学顕微鏡(400倍)を用いて観察することにより、以下の基準に従って粉末の分散安定性を評価した。
<評価基準>
A:疎水性粉末が油分中に均一に分散していた
B:疎水性粉末が外観上は均一に分散していたが、光学顕微鏡を用いて調べると凝集した部分がわずかに観察された
C:疎水性粉末の一部の凝集が外観上で観察された
D:疎水性粉末のほとんどが凝集した
下記表2及び表3に掲げる組成を有する水性化粧料を上記実施例1と同様の方法で調製し、前記基準に従って各化粧料の分散安定性を評価した。それらの結果を表2及び表3に併せて示す。
下記表4に掲げる水相部、油相部をそれぞれ70℃に加熱して完全溶解した。油相部を水相部に加えて、乳化機で乳化し冷却した。この時、比較例5では乳化前に粉末部を水相に混合したが、実施例14では冷却後の水中油型乳化組成物に攪拌混合した粉末部を混合した。
得られた組成物を化粧下地として使用し、その際のみずみずしさ、なめらかさ、のびの軽さ、化粧もちを専門評価パネル10名により、以下の基準で評価した。
<評価基準>
A:優れていると回答したパネルが8〜10名。
B:優れていると回答したパネルが5〜7名。
C:優れていると回答したパネルが4名以下。
(成分名) 配合量(%)
イオン交換水 残量
グリセリン 5.0
ジプロピレングリコール 2.0
1,3−ブチレングリコール 5.0
カルボキシビニルポリマー 0.2
キサンタンガム 0.05
トラネキサム酸 2.0
4−メトキシサリチル酸カリウム塩 1.0
グリチルリチン酸ジカリウム 0.1
酢酸トコフェロール 0.1
PEG−11メチルエーテルジメチコン*4 1.0
球状ポリメチルシルセスキオキサン粉末 5.0
トリエタノールアミン 適量
酸化防止剤 適量
防腐剤 適量
(成分名) 配合量(%)
イオン交換水 残量
エチルアルコール 5.0
グリセリン 3.0
1,3−ブチレングリコール 5.0
(ジメチルアクリルアミド/アクリロイルジメチルタウリンNa)
クロスポリマー 0.4
サクシノグリカン 0.1
PEG−12ジメチコン*3 1.0
オクチルトリエトキシシラン処理酸化チタン 4.0
球状ポリメタクリル酸メチル粉末 1.0
キレート剤 適量
緩衝剤 適量
防腐剤 適量
香料 適量
(成分名) 配合量(%)
イオン交換水 残量
エチルアルコール 3.0
(アクリル酸Na/アクリロイルジメチルタウリンNa)コポリマー
0.4
カルボキシメチルセルロース 0.05
グリセリン 5.0
エリスリトール 2.0
ジプロピレングリコール 7.0
ベヘニルアルコール 1.0
バチルアルコール 0.5
スクワラン 6.0
ジメチルポリシロキサン 2.0
マカデミアナッツ脂肪酸フィトステリル 0.5
イソステアリン酸ポリオキシエチレングリセリル 1.0
モノステアリン酸ポリオキシエチレングリセリン 1.0
ヘキサメタリン酸ナトリウム 0.05
PEG−12ジメチコン*3 1.0
球状ナイロン粉末 3.0
ウレタン樹脂粉末 3.0
防腐剤 適量
香料 適量
Claims (5)
- (A)0.1〜5質量%のHLB(Si)が5〜14のポリエーテル変性シリコーン、
(B)親水性増粘剤の1種又は2種以上、
(C)ポリオール及び/又はエチルアルコール、
(D)金属石鹸以外で疎水化処理された金属酸化物、疎水性の有機粉末、シリコーン粉末から選ばれる1種又は2種以上の疎水性粉末を含有し、
(D)疎水性粉末が水相に分散していることを特徴とする水性化粧料。 - (B)親水性増粘剤が、多糖類及びその誘導体、及びポリアクリルアミド化合物からなる群から選択される少なくとも1種を含むことを特徴とする請求項1に記載の化粧料。
- (B)親水性増粘剤が、ポリアクリルアミド化合物を含み、さらに多糖類又はその誘導体を含む、請求項1に記載の化粧料。
- 疎水性された金属酸化物が、シリコーン処理又は脂肪酸デキストリン処理によって疎水化されていることを特徴とする請求項1から3のいずれか一項に記載の化粧料。
- 疎水性の有機粉末が、ポリメタクリル酸メチル粉末、ナイロン粉末、ポリウレタン粉末、ポリエチレン粉末、ポリスチレン粉末からなる群から選択される、請求項1から4のいずれか一項に記載の化粧料。
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EP3466399B1 (en) * | 2016-05-27 | 2021-05-12 | Sakai Chemical Industry Co., Ltd. | Liquid dispersion and uses thereof |
CN117017832A (zh) * | 2017-11-17 | 2023-11-10 | 株式会社高丝 | 固态粉末化妆品 |
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JP7044132B2 (ja) * | 2020-06-11 | 2022-03-30 | 日清紡ホールディングス株式会社 | 両親媒性アルギン酸粒子群及びその製造方法 |
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JPWO2016002751A1 (ja) * | 2014-06-30 | 2017-04-27 | 株式会社 資生堂 | 水中油型乳化組成物 |
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JPWO2016002751A1 (ja) * | 2014-06-30 | 2017-04-27 | 株式会社 資生堂 | 水中油型乳化組成物 |
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EP3162355A1 (en) | 2017-05-03 |
US20170128352A1 (en) | 2017-05-11 |
CN106232084A (zh) | 2016-12-14 |
JP6543247B2 (ja) | 2019-07-10 |
WO2016002752A1 (ja) | 2016-01-07 |
EP3162355A4 (en) | 2018-02-21 |
CN115444785A (zh) | 2022-12-09 |
US10300008B2 (en) | 2019-05-28 |
TW201607561A (zh) | 2016-03-01 |
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