JPS637224B2 - - Google Patents
Info
- Publication number
- JPS637224B2 JPS637224B2 JP54102311A JP10231179A JPS637224B2 JP S637224 B2 JPS637224 B2 JP S637224B2 JP 54102311 A JP54102311 A JP 54102311A JP 10231179 A JP10231179 A JP 10231179A JP S637224 B2 JPS637224 B2 JP S637224B2
- Authority
- JP
- Japan
- Prior art keywords
- transformation
- relative intensities
- dyeing
- modification
- dye
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000004043 dyeing Methods 0.000 claims description 18
- 238000012986 modification Methods 0.000 claims description 12
- 238000010438 heat treatment Methods 0.000 claims description 6
- 238000000034 method Methods 0.000 claims description 6
- 238000002441 X-ray diffraction Methods 0.000 claims description 4
- 238000010586 diagram Methods 0.000 claims description 4
- 239000002270 dispersing agent Substances 0.000 claims description 4
- 150000001875 compounds Chemical class 0.000 claims description 3
- 230000009466 transformation Effects 0.000 claims description 3
- 125000000129 anionic group Chemical group 0.000 claims description 2
- 125000002091 cationic group Chemical group 0.000 claims description 2
- 239000003960 organic solvent Substances 0.000 claims description 2
- 239000003945 anionic surfactant Substances 0.000 claims 1
- 239000003093 cationic surfactant Substances 0.000 claims 1
- 239000002736 nonionic surfactant Substances 0.000 claims 1
- 239000000725 suspension Substances 0.000 claims 1
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 12
- 239000000975 dye Substances 0.000 description 12
- 238000002360 preparation method Methods 0.000 description 9
- 238000010186 staining Methods 0.000 description 9
- 239000007900 aqueous suspension Substances 0.000 description 7
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 6
- 239000007859 condensation product Substances 0.000 description 5
- 159000000000 sodium salts Chemical class 0.000 description 5
- NYGZLYXAPMMJTE-UHFFFAOYSA-M metanil yellow Chemical group [Na+].[O-]S(=O)(=O)C1=CC=CC(N=NC=2C=CC(NC=3C=CC=CC=3)=CC=2)=C1 NYGZLYXAPMMJTE-UHFFFAOYSA-M 0.000 description 4
- PSZYNBSKGUBXEH-UHFFFAOYSA-N naphthalene-1-sulfonic acid Chemical class C1=CC=C2C(S(=O)(=O)O)=CC=CC2=C1 PSZYNBSKGUBXEH-UHFFFAOYSA-N 0.000 description 4
- KBLAMUYRMZPYLS-UHFFFAOYSA-N 2,3-bis(2-methylpropyl)naphthalene-1-sulfonic acid Chemical compound C1=CC=C2C(S(O)(=O)=O)=C(CC(C)C)C(CC(C)C)=CC2=C1 KBLAMUYRMZPYLS-UHFFFAOYSA-N 0.000 description 3
- QTWJRLJHJPIABL-UHFFFAOYSA-N 2-methylphenol;3-methylphenol;4-methylphenol Chemical compound CC1=CC=C(O)C=C1.CC1=CC=CC(O)=C1.CC1=CC=CC=C1O QTWJRLJHJPIABL-UHFFFAOYSA-N 0.000 description 3
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 3
- DWAQJAXMDSEUJJ-UHFFFAOYSA-M Sodium bisulfite Chemical compound [Na+].OS([O-])=O DWAQJAXMDSEUJJ-UHFFFAOYSA-M 0.000 description 3
- 229920002678 cellulose Polymers 0.000 description 3
- 229930003836 cresol Natural products 0.000 description 3
- 239000006185 dispersion Substances 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 235000010267 sodium hydrogen sulphite Nutrition 0.000 description 3
- NPCCPMHHNIOSHL-UHFFFAOYSA-N 3-(n-ethyl-3-methylanilino)propanenitrile Chemical compound N#CCCN(CC)C1=CC=CC(C)=C1 NPCCPMHHNIOSHL-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 2
- 229920001732 Lignosulfonate Polymers 0.000 description 2
- AFVFQIVMOAPDHO-UHFFFAOYSA-N Methanesulfonic acid Chemical compound CS(O)(=O)=O AFVFQIVMOAPDHO-UHFFFAOYSA-N 0.000 description 2
- LSNNMFCWUKXFEE-UHFFFAOYSA-N Sulfurous acid Chemical compound OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 description 2
- 239000001913 cellulose Substances 0.000 description 2
- 150000008049 diazo compounds Chemical class 0.000 description 2
- LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical compound CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 2
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 229920002554 vinyl polymer Polymers 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- LOCWBQIWHWIRGN-UHFFFAOYSA-N 2-chloro-4-nitroaniline Chemical compound NC1=CC=C([N+]([O-])=O)C=C1Cl LOCWBQIWHWIRGN-UHFFFAOYSA-N 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 239000002202 Polyethylene glycol Substances 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 150000001447 alkali salts Chemical class 0.000 description 1
- 239000012736 aqueous medium Substances 0.000 description 1
- 235000013351 cheese Nutrition 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 150000001805 chlorine compounds Chemical class 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- -1 formaldehyde, alkali salts Chemical class 0.000 description 1
- 150000002334 glycols Chemical class 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229940098779 methanesulfonic acid Drugs 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- GOQYKNQRPGWPLP-UHFFFAOYSA-N n-heptadecyl alcohol Natural products CCCCCCCCCCCCCCCCCO GOQYKNQRPGWPLP-UHFFFAOYSA-N 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 150000003014 phosphoric acid esters Chemical class 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 229920001223 polyethylene glycol Polymers 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- PYODKQIVQIVELM-UHFFFAOYSA-M sodium;2,3-bis(2-methylpropyl)naphthalene-1-sulfonate Chemical compound [Na+].C1=CC=C2C(S([O-])(=O)=O)=C(CC(C)C)C(CC(C)C)=CC2=C1 PYODKQIVQIVELM-UHFFFAOYSA-M 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 1
- 150000003871 sulfonates Chemical class 0.000 description 1
- KKEYFWRCBNTPAC-UHFFFAOYSA-L terephthalate(2-) Chemical compound [O-]C(=O)C1=CC=C(C([O-])=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-L 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B29/00—Monoazo dyes prepared by diazotising and coupling
- C09B29/06—Monoazo dyes prepared by diazotising and coupling from coupling components containing amino as the only directing group
- C09B29/08—Amino benzenes
- C09B29/0805—Amino benzenes free of acid groups
- C09B29/0807—Amino benzenes free of acid groups characterised by the amino group
- C09B29/0809—Amino benzenes free of acid groups characterised by the amino group substituted amino group
- C09B29/0811—Amino benzenes free of acid groups characterised by the amino group substituted amino group further substituted alkylamino, alkenylamino, alkynylamino, cycloalkylamino aralkylamino or arylamino
- C09B29/0823—Amino benzenes free of acid groups characterised by the amino group substituted amino group further substituted alkylamino, alkenylamino, alkynylamino, cycloalkylamino aralkylamino or arylamino substituted by CN
- C09B29/0825—Amino benzenes free of acid groups characterised by the amino group substituted amino group further substituted alkylamino, alkenylamino, alkynylamino, cycloalkylamino aralkylamino or arylamino substituted by CN having N(-alkenylene-CN/-alkynylene-CN)(-aliphatic residue-CN)
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B29/00—Monoazo dyes prepared by diazotising and coupling
- C09B29/06—Monoazo dyes prepared by diazotising and coupling from coupling components containing amino as the only directing group
- C09B29/08—Amino benzenes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0001—Post-treatment of organic pigments or dyes
- C09B67/0014—Influencing the physical properties by treatment with a liquid, e.g. solvents
- C09B67/0015—Influencing the physical properties by treatment with a liquid, e.g. solvents of azoic pigments
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0025—Crystal modifications; Special X-ray patterns
- C09B67/0028—Crystal modifications; Special X-ray patterns of azo compounds
- C09B67/0029—Crystal modifications; Special X-ray patterns of azo compounds of monoazo compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Coloring (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2835544A DE2835544B1 (de) | 1978-08-14 | 1978-08-14 | Faerbestabiler Monoazofarbstoff,dessen Herstellung und Verwendung |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5525497A JPS5525497A (en) | 1980-02-23 |
| JPS637224B2 true JPS637224B2 (pt) | 1988-02-16 |
Family
ID=6046988
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP10231179A Granted JPS5525497A (en) | 1978-08-14 | 1979-08-13 | Stable monoazo dyestuff * production and dyeing method |
Country Status (8)
| Country | Link |
|---|---|
| JP (1) | JPS5525497A (pt) |
| BE (1) | BE878252A (pt) |
| BR (1) | BR7905189A (pt) |
| DE (1) | DE2835544B1 (pt) |
| FR (1) | FR2433559A1 (pt) |
| GB (1) | GB2028857B (pt) |
| IT (1) | IT1122483B (pt) |
| MX (1) | MX150601A (pt) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS58225156A (ja) * | 1982-06-21 | 1983-12-27 | Gosei Senriyou Gijutsu Kenkyu Kumiai | モノアゾ染料及びその製法 |
-
1978
- 1978-08-14 DE DE2835544A patent/DE2835544B1/de not_active Ceased
-
1979
- 1979-07-13 MX MX178483A patent/MX150601A/es unknown
- 1979-08-10 IT IT25072/79A patent/IT1122483B/it active
- 1979-08-13 BR BR7905189A patent/BR7905189A/pt unknown
- 1979-08-13 JP JP10231179A patent/JPS5525497A/ja active Granted
- 1979-08-14 FR FR7920654A patent/FR2433559A1/fr active Granted
- 1979-08-14 GB GB7928179A patent/GB2028857B/en not_active Expired
- 1979-08-14 BE BE0/196743A patent/BE878252A/fr not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| GB2028857A (en) | 1980-03-12 |
| IT1122483B (it) | 1986-04-23 |
| DE2835544B1 (de) | 1979-05-31 |
| BR7905189A (pt) | 1980-05-06 |
| FR2433559B1 (pt) | 1983-09-09 |
| JPS5525497A (en) | 1980-02-23 |
| MX150601A (es) | 1984-06-06 |
| FR2433559A1 (fr) | 1980-03-14 |
| IT7925072A0 (it) | 1979-08-10 |
| BE878252A (fr) | 1980-02-14 |
| GB2028857B (en) | 1983-03-09 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| EP0019831B1 (de) | Färbestabile kristallographische Modifikation eines Monoazofarbstoffs, dessen Herstellung und Verwendung zum Färben von Fasermaterialien | |
| US4074965A (en) | Stable monoazo dyestuff | |
| JPS5945697B2 (ja) | 染色安定性の分散染料および合成および半合成織物材料の染色またはなつ染へのその使用 | |
| KR890001782B1 (ko) | 분산염료의 염색-안정성 변형체의 제조방법 | |
| EP0031478B1 (de) | Färbestabiler Monoazofarbstoff, dessen Herstellung und Verwendung | |
| CA1183309A (en) | Easily dispersing phthalocyanine blue | |
| JP2628363B2 (ja) | 染料の結晶変態及びその製造法 | |
| JPS637224B2 (pt) | ||
| JPH0430426B2 (pt) | ||
| US4453944A (en) | Dye stable to dyeing, processes for producing it, and its use for dyeing and printing synthetic and semi-synthetic fibre materials | |
| US5069682A (en) | Color-stable beta-modification of a monoazo dye, a process for its preparation, and its use | |
| JPS6047310B2 (ja) | 混合染料の染色に安定な変態 | |
| US5037962A (en) | β-modification of 1-(2,4-dinitro-6-chloro-phenylazo)-2-propionylamino-4-N-ethylamino-5-(2-methoxy-ethoxy)benzene, its preparation and its use | |
| JPS598303B2 (ja) | 染色安定性モノアゾ染料の製法 | |
| KR840000808B1 (ko) | 모노아조 염료의 결정성 변체의 제조방법 | |
| US5917121A (en) | Monoazo dyes which are stable under dyeing conditions, their preparation and their use | |
| JP2772998B2 (ja) | 染料の熱に安定な結晶変態 | |
| US6673906B1 (en) | β modified monoazo dye resistant to dyeing, its preparation and use | |
| JPH08231876A (ja) | 染色に安定なモノアゾ染料、その製造方法及びその使用方法 | |
| KR20010014082A (ko) | 염색중에 안정한 모노아조 염료, 그의 제조방법 및 용도 | |
| DE2520577C3 (de) | Färbestabiler Monoazofarbstoff, dessen Herstellung und Verwendung | |
| JP2628383B2 (ja) | 染料の熱に安定な結晶変態及びその製造法 | |
| JPH05222316A (ja) | 熱に安定な結晶変態及びこれを用いる染色法 | |
| JPH02185570A (ja) | 染料の熱に安定な結晶変態及びその製造法 | |
| JPS591749B2 (ja) | 染色安定性の分散染料及びその製法 |