JPS6363388A - 低分子量キトサンの製法 - Google Patents
低分子量キトサンの製法Info
- Publication number
- JPS6363388A JPS6363388A JP61208435A JP20843586A JPS6363388A JP S6363388 A JPS6363388 A JP S6363388A JP 61208435 A JP61208435 A JP 61208435A JP 20843586 A JP20843586 A JP 20843586A JP S6363388 A JPS6363388 A JP S6363388A
- Authority
- JP
- Japan
- Prior art keywords
- molecular weight
- chitosan
- low molecular
- weight chitosan
- aqueous solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229920001661 Chitosan Polymers 0.000 title claims abstract description 62
- 238000004519 manufacturing process Methods 0.000 title claims description 8
- 239000007864 aqueous solution Substances 0.000 claims abstract description 17
- 239000004365 Protease Substances 0.000 claims abstract description 12
- 238000000354 decomposition reaction Methods 0.000 claims abstract description 11
- 108010059892 Cellulase Proteins 0.000 claims abstract description 6
- 108090000526 Papain Proteins 0.000 claims abstract description 6
- 108091005804 Peptidases Proteins 0.000 claims abstract description 6
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 claims abstract description 6
- 230000002378 acidificating effect Effects 0.000 claims abstract description 6
- 229940106157 cellulase Drugs 0.000 claims abstract description 6
- 229940055729 papain Drugs 0.000 claims abstract description 6
- 235000019834 papain Nutrition 0.000 claims abstract description 6
- 235000019419 proteases Nutrition 0.000 claims abstract description 6
- 108090000790 Enzymes Proteins 0.000 abstract description 14
- 102000004190 Enzymes Human genes 0.000 abstract description 14
- 229940088598 enzyme Drugs 0.000 abstract description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 10
- 229920002101 Chitin Polymers 0.000 abstract description 4
- 238000003381 deacetylation reaction Methods 0.000 abstract description 2
- 230000006196 deacetylation Effects 0.000 abstract 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 9
- 239000000243 solution Substances 0.000 description 9
- 238000006243 chemical reaction Methods 0.000 description 7
- 238000012360 testing method Methods 0.000 description 7
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 6
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 6
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 5
- 150000007524 organic acids Chemical class 0.000 description 5
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 4
- 241000238557 Decapoda Species 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 4
- 238000012790 confirmation Methods 0.000 description 4
- 235000005985 organic acids Nutrition 0.000 description 4
- 239000000843 powder Substances 0.000 description 4
- 239000002244 precipitate Substances 0.000 description 4
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 235000019253 formic acid Nutrition 0.000 description 3
- 239000004310 lactic acid Substances 0.000 description 3
- 235000014655 lactic acid Nutrition 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- 239000000758 substrate Substances 0.000 description 3
- 235000001674 Agaricus brunnescens Nutrition 0.000 description 2
- 241000238424 Crustacea Species 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 230000001580 bacterial effect Effects 0.000 description 2
- 210000002421 cell wall Anatomy 0.000 description 2
- 230000000850 deacetylating effect Effects 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 239000012153 distilled water Substances 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 150000002772 monosaccharides Chemical class 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- 102000004169 proteins and genes Human genes 0.000 description 2
- 108090000623 proteins and genes Proteins 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- 235000011054 acetic acid Nutrition 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000002255 enzymatic effect Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Landscapes
- Jellies, Jams, And Syrups (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Cosmetics (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- General Preparation And Processing Of Foods (AREA)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP61208435A JPS6363388A (ja) | 1986-09-04 | 1986-09-04 | 低分子量キトサンの製法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP61208435A JPS6363388A (ja) | 1986-09-04 | 1986-09-04 | 低分子量キトサンの製法 |
Related Child Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP31224790A Division JPH03164191A (ja) | 1990-11-17 | 1990-11-17 | 低分子量キトサンの製法 |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS6363388A true JPS6363388A (ja) | 1988-03-19 |
JPH0157958B2 JPH0157958B2 (enrdf_load_stackoverflow) | 1989-12-08 |
Family
ID=16556159
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP61208435A Granted JPS6363388A (ja) | 1986-09-04 | 1986-09-04 | 低分子量キトサンの製法 |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS6363388A (enrdf_load_stackoverflow) |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0220292A (ja) * | 1988-07-06 | 1990-01-23 | Agency Of Ind Science & Technol | 低分子化キトサンの製造方法 |
JPH02200196A (ja) * | 1989-01-31 | 1990-08-08 | Nippon Kayaku Co Ltd | 低分子量キトサンの製造方法 |
JPH03164191A (ja) * | 1990-11-17 | 1991-07-16 | Nitta Gelatin Inc | 低分子量キトサンの製法 |
US5762992A (en) * | 1991-08-01 | 1998-06-09 | San-Ei Chemical Industries, Ltd. | Method of preventing a decrease in sweetness of thaumatin |
KR100367992B1 (ko) * | 1998-06-15 | 2003-05-16 | 주식회사 태평양 | 올리고키토산의제조방법 |
KR100473445B1 (ko) * | 2001-05-10 | 2005-03-08 | 씨제이 주식회사 | 저분자 키토산과 ε-폴리라이신을 주원료로 하는 콜레스테롤 저하제 및 건강 보조 식품 |
CN115521960A (zh) * | 2022-09-20 | 2022-12-27 | 山东海锋生物工程有限公司 | 一种减少壳寡糖非酶褐变的生产工艺 |
JP2023135748A (ja) * | 2022-03-16 | 2023-09-29 | 株式会社ショウワ | キトサンオリゴマー分画方法 |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH07246933A (ja) * | 1994-03-08 | 1995-09-26 | Kyosan Electric Mfg Co Ltd | 転てつ装置 |
-
1986
- 1986-09-04 JP JP61208435A patent/JPS6363388A/ja active Granted
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0220292A (ja) * | 1988-07-06 | 1990-01-23 | Agency Of Ind Science & Technol | 低分子化キトサンの製造方法 |
JPH02200196A (ja) * | 1989-01-31 | 1990-08-08 | Nippon Kayaku Co Ltd | 低分子量キトサンの製造方法 |
JPH03164191A (ja) * | 1990-11-17 | 1991-07-16 | Nitta Gelatin Inc | 低分子量キトサンの製法 |
US5762992A (en) * | 1991-08-01 | 1998-06-09 | San-Ei Chemical Industries, Ltd. | Method of preventing a decrease in sweetness of thaumatin |
KR100367992B1 (ko) * | 1998-06-15 | 2003-05-16 | 주식회사 태평양 | 올리고키토산의제조방법 |
KR100473445B1 (ko) * | 2001-05-10 | 2005-03-08 | 씨제이 주식회사 | 저분자 키토산과 ε-폴리라이신을 주원료로 하는 콜레스테롤 저하제 및 건강 보조 식품 |
JP2023135748A (ja) * | 2022-03-16 | 2023-09-29 | 株式会社ショウワ | キトサンオリゴマー分画方法 |
CN115521960A (zh) * | 2022-09-20 | 2022-12-27 | 山东海锋生物工程有限公司 | 一种减少壳寡糖非酶褐变的生产工艺 |
Also Published As
Publication number | Publication date |
---|---|
JPH0157958B2 (enrdf_load_stackoverflow) | 1989-12-08 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
JPH0220292A (ja) | 低分子化キトサンの製造方法 | |
CN107201387A (zh) | 一种右旋糖酐铁的制备方法 | |
JPS6363388A (ja) | 低分子量キトサンの製法 | |
JPS63225602A (ja) | 易溶性キトサン | |
CN109721740B (zh) | 一种连续制备不同脱乙酰度的甲壳素/壳聚糖溶液的方法 | |
CN106519060A (zh) | 一种羧甲基可得然胶的制备 | |
JP2004501235A (ja) | キトサン粒子の調製プロセス | |
JP2901176B2 (ja) | 低粘度キトサン及びその製造方法 | |
JPH0421477B2 (enrdf_load_stackoverflow) | ||
US20070129326A1 (en) | Methods for producing modified microcrystalline chitosan and uses therefor | |
WO2025036462A1 (zh) | 一种壳寡糖硫酸盐及其制备方法 | |
CN111035581B (zh) | 一种维持唾液酸溶液高温时稳定的方法及其应用 | |
CN106310348B (zh) | 一种淀粉/泊洛沙姆复合止血粉及其制备方法 | |
CN102422848B (zh) | 一种在面包制作过程中具有强筋作用的固定化葡萄糖氧化酶的制备方法 | |
JPH03164191A (ja) | 低分子量キトサンの製法 | |
CN111675773B (zh) | 一种可控分子量范围的壳聚糖制备方法及其应用 | |
CN115806680A (zh) | 一种瓜尔胶与卡拉胶复合物及其制备方法和应用 | |
JPS6134004A (ja) | 新規カチオン化キチンの製造方法 | |
JPS62184002A (ja) | 水溶性低分子化キトサンの製造方法 | |
JP2009209376A (ja) | 多糖類複合体及びその製造方法 | |
CN102634074B (zh) | 甲壳素浆及其生产方法 | |
KR100252704B1 (ko) | 고순도 결정성 nocc의 제조방법 및 효소를 이용한 수용성키토산의 분자량 조절방법 | |
JP5179847B2 (ja) | 新規な可溶性卵殻膜の製造方法 | |
CN105085940A (zh) | 壳聚糖的快速溶解方法 | |
JPS6363701A (ja) | 水溶性低分子化キトサンの製造方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
EXPY | Cancellation because of completion of term |