JPS6067000A - マルト−スの分離法 - Google Patents
マルト−スの分離法Info
- Publication number
- JPS6067000A JPS6067000A JP17239483A JP17239483A JPS6067000A JP S6067000 A JPS6067000 A JP S6067000A JP 17239483 A JP17239483 A JP 17239483A JP 17239483 A JP17239483 A JP 17239483A JP S6067000 A JPS6067000 A JP S6067000A
- Authority
- JP
- Japan
- Prior art keywords
- maltose
- flow rate
- zone
- aqueous solution
- volumetric flow
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- OWEGMIWEEQEYGQ-UHFFFAOYSA-N 100676-05-9 Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC2C(OC(O)C(O)C2O)CO)O1 OWEGMIWEEQEYGQ-UHFFFAOYSA-N 0.000 title claims description 58
- GUBGYTABKSRVRQ-PICCSMPSSA-N Maltose Natural products O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)OC(O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-PICCSMPSSA-N 0.000 title claims description 58
- 238000000034 method Methods 0.000 title claims description 14
- 239000007864 aqueous solution Substances 0.000 claims description 27
- 229920001542 oligosaccharide Polymers 0.000 claims description 26
- 150000002482 oligosaccharides Chemical class 0.000 claims description 26
- 150000001768 cations Chemical class 0.000 claims description 16
- 238000001179 sorption measurement Methods 0.000 claims description 12
- 238000000605 extraction Methods 0.000 claims description 11
- 239000012530 fluid Substances 0.000 claims description 10
- 238000000746 purification Methods 0.000 claims description 10
- 235000000346 sugar Nutrition 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- 239000002994 raw material Substances 0.000 claims description 8
- 238000000926 separation method Methods 0.000 claims description 7
- WSWCOQWTEOXDQX-MQQKCMAXSA-M (E,E)-sorbate Chemical compound C\C=C\C=C\C([O-])=O WSWCOQWTEOXDQX-MQQKCMAXSA-M 0.000 claims description 4
- 238000003795 desorption Methods 0.000 claims description 4
- 229940075554 sorbate Drugs 0.000 claims description 4
- DBTMGCOVALSLOR-UHFFFAOYSA-N 32-alpha-galactosyl-3-alpha-galactosyl-galactose Natural products OC1C(O)C(O)C(CO)OC1OC1C(O)C(OC2C(C(CO)OC(O)C2O)O)OC(CO)C1O DBTMGCOVALSLOR-UHFFFAOYSA-N 0.000 claims description 3
- RXVWSYJTUUKTEA-UHFFFAOYSA-N D-maltotriose Natural products OC1C(O)C(OC(C(O)CO)C(O)C(O)C=O)OC(CO)C1OC1C(O)C(O)C(O)C(CO)O1 RXVWSYJTUUKTEA-UHFFFAOYSA-N 0.000 claims description 3
- GUBGYTABKSRVRQ-QUYVBRFLSA-N beta-maltose Chemical compound OC[C@H]1O[C@H](O[C@H]2[C@H](O)[C@@H](O)[C@H](O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@@H]1O GUBGYTABKSRVRQ-QUYVBRFLSA-N 0.000 claims description 3
- FYGDTMLNYKFZSV-UHFFFAOYSA-N mannotriose Natural products OC1C(O)C(O)C(CO)OC1OC1C(CO)OC(OC2C(OC(O)C(O)C2O)CO)C(O)C1O FYGDTMLNYKFZSV-UHFFFAOYSA-N 0.000 claims description 3
- FYGDTMLNYKFZSV-BYLHFPJWSA-N β-1,4-galactotrioside Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@H](CO)O[C@@H](O[C@@H]2[C@@H](O[C@@H](O)[C@H](O)[C@H]2O)CO)[C@H](O)[C@H]1O FYGDTMLNYKFZSV-BYLHFPJWSA-N 0.000 claims description 3
- 150000008163 sugars Chemical class 0.000 claims description 2
- 238000011144 upstream manufacturing Methods 0.000 claims description 2
- 238000013375 chromatographic separation Methods 0.000 claims 1
- 238000001172 liquid--solid extraction Methods 0.000 claims 1
- 239000000463 material Substances 0.000 claims 1
- 235000020357 syrup Nutrition 0.000 description 21
- 239000006188 syrup Substances 0.000 description 21
- 229920002472 Starch Polymers 0.000 description 19
- 235000019698 starch Nutrition 0.000 description 19
- 239000008107 starch Substances 0.000 description 19
- 239000007788 liquid Substances 0.000 description 12
- 238000010586 diagram Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 3
- 239000003729 cation exchange resin Substances 0.000 description 3
- 239000008103 glucose Substances 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
- 230000002378 acidificating effect Effects 0.000 description 2
- 229940023913 cation exchange resins Drugs 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- LUEWUZLMQUOBSB-UHFFFAOYSA-N UNPD55895 Natural products OC1C(O)C(O)C(CO)OC1OC1C(CO)OC(OC2C(OC(OC3C(OC(O)C(O)C3O)CO)C(O)C2O)CO)C(O)C1O LUEWUZLMQUOBSB-UHFFFAOYSA-N 0.000 description 1
- VVUBWCWVDFCEOP-UHFFFAOYSA-N benzene;styrene Chemical compound C1=CC=CC=C1.C=CC1=CC=CC=C1 VVUBWCWVDFCEOP-UHFFFAOYSA-N 0.000 description 1
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- TVWHTOUAJSGEKT-UHFFFAOYSA-N chlorine trioxide Chemical compound [O]Cl(=O)=O TVWHTOUAJSGEKT-UHFFFAOYSA-N 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- 230000002255 enzymatic effect Effects 0.000 description 1
- 210000004709 eyebrow Anatomy 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000003599 food sweetener Nutrition 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- UYQJCPNSAVWAFU-UHFFFAOYSA-N malto-tetraose Natural products OC1C(O)C(OC(C(O)CO)C(O)C(O)C=O)OC(CO)C1OC1C(O)C(O)C(OC2C(C(O)C(O)C(CO)O2)O)C(CO)O1 UYQJCPNSAVWAFU-UHFFFAOYSA-N 0.000 description 1
- LUEWUZLMQUOBSB-OUBHKODOSA-N maltotetraose Chemical compound O[C@H]1[C@H](O)[C@@H](O)[C@H](CO)O[C@H]1O[C@@H]1[C@H](CO)O[C@@H](O[C@@H]2[C@@H](O[C@@H](O[C@@H]3[C@@H](O[C@@H](O)[C@H](O)[C@H]3O)CO)[C@H](O)[C@H]2O)CO)[C@H](O)[C@H]1O LUEWUZLMQUOBSB-OUBHKODOSA-N 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 235000020374 simple syrup Nutrition 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 125000000542 sulfonic acid group Chemical group 0.000 description 1
- 239000003765 sweetening agent Substances 0.000 description 1
- 239000010457 zeolite Substances 0.000 description 1
Landscapes
- Saccharide Compounds (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP17239483A JPS6067000A (ja) | 1983-09-19 | 1983-09-19 | マルト−スの分離法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP17239483A JPS6067000A (ja) | 1983-09-19 | 1983-09-19 | マルト−スの分離法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6067000A true JPS6067000A (ja) | 1985-04-17 |
| JPH059080B2 JPH059080B2 (enrdf_load_stackoverflow) | 1993-02-03 |
Family
ID=15941116
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP17239483A Granted JPS6067000A (ja) | 1983-09-19 | 1983-09-19 | マルト−スの分離法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6067000A (enrdf_load_stackoverflow) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0198601A (ja) * | 1987-10-13 | 1989-04-17 | Gunei Kagaku Kogyo Kk | 高純度イソマルトオリゴ糖の製造方法 |
| JPH01197596A (ja) * | 1988-02-01 | 1989-08-09 | Kanegafuchi Chem Ind Co Ltd | 脂肪酸とトリグリセリドの分離方法 |
| JPH01197597A (ja) * | 1988-02-01 | 1989-08-09 | Kanegafuchi Chem Ind Co Ltd | 脂肪酸とトリグリセリドの精製方法 |
| JP2008137982A (ja) * | 2006-12-01 | 2008-06-19 | Shin Dong Bang Cp Corp | 高純度マルチトール結晶性粉末を調製するためのプロセス |
| JP2008538739A (ja) * | 2003-07-18 | 2008-11-06 | カーギル インコーポレイテッド | マルチトール強化生成物の製造方法 |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1394503A (en) * | 1972-01-26 | 1975-05-14 | Suomen Sokeri Oy | Method for separating monosaccharides fromsarch conversion syrups |
| JPS5376975A (en) * | 1976-12-21 | 1978-07-07 | Mitsubishi Chem Ind Ltd | Controlling method for pseudomoving bed |
| JPS5388335A (en) * | 1977-01-13 | 1978-08-03 | Mitsubishi Chem Ind | Production of fructose |
| JPS5548400A (en) * | 1978-10-04 | 1980-04-07 | Mitsubishi Chem Ind | Removing of oligosaccharide |
| FR2454830A1 (fr) * | 1979-04-25 | 1980-11-21 | Roquette Freres | Installation et procede pour la separation continue par adsorption selective de melanges de sucres et/ou de polyols |
| JPS57209000A (en) * | 1981-06-17 | 1982-12-22 | Organo Kk | Decomposition of maltose |
| JPS5823799A (ja) * | 1981-08-03 | 1983-02-12 | 株式会社林原生物化学研究所 | 高純度マルト−スの製造方法 |
-
1983
- 1983-09-19 JP JP17239483A patent/JPS6067000A/ja active Granted
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1394503A (en) * | 1972-01-26 | 1975-05-14 | Suomen Sokeri Oy | Method for separating monosaccharides fromsarch conversion syrups |
| JPS5376975A (en) * | 1976-12-21 | 1978-07-07 | Mitsubishi Chem Ind Ltd | Controlling method for pseudomoving bed |
| JPS5388335A (en) * | 1977-01-13 | 1978-08-03 | Mitsubishi Chem Ind | Production of fructose |
| JPS5548400A (en) * | 1978-10-04 | 1980-04-07 | Mitsubishi Chem Ind | Removing of oligosaccharide |
| FR2454830A1 (fr) * | 1979-04-25 | 1980-11-21 | Roquette Freres | Installation et procede pour la separation continue par adsorption selective de melanges de sucres et/ou de polyols |
| JPS57209000A (en) * | 1981-06-17 | 1982-12-22 | Organo Kk | Decomposition of maltose |
| JPS5823799A (ja) * | 1981-08-03 | 1983-02-12 | 株式会社林原生物化学研究所 | 高純度マルト−スの製造方法 |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0198601A (ja) * | 1987-10-13 | 1989-04-17 | Gunei Kagaku Kogyo Kk | 高純度イソマルトオリゴ糖の製造方法 |
| JPH01197596A (ja) * | 1988-02-01 | 1989-08-09 | Kanegafuchi Chem Ind Co Ltd | 脂肪酸とトリグリセリドの分離方法 |
| JPH01197597A (ja) * | 1988-02-01 | 1989-08-09 | Kanegafuchi Chem Ind Co Ltd | 脂肪酸とトリグリセリドの精製方法 |
| JP2008538739A (ja) * | 2003-07-18 | 2008-11-06 | カーギル インコーポレイテッド | マルチトール強化生成物の製造方法 |
| US7935190B2 (en) | 2003-07-18 | 2011-05-03 | Cargill, Incorporated | Process for preparing maltitol enriched products |
| JP2008137982A (ja) * | 2006-12-01 | 2008-06-19 | Shin Dong Bang Cp Corp | 高純度マルチトール結晶性粉末を調製するためのプロセス |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH059080B2 (enrdf_load_stackoverflow) | 1993-02-03 |
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