JPS60130551A - 第３級アミンの製造方法 - Google Patents

第３級アミンの製造方法

Info

Publication number
JPS60130551A
JPS60130551A JP58238221A JP23822183A JPS60130551A JP S60130551 A JPS60130551 A JP S60130551A JP 58238221 A JP58238221 A JP 58238221A JP 23822183 A JP23822183 A JP 23822183A JP S60130551 A JPS60130551 A JP S60130551A
Authority
JP
Japan
Prior art keywords
catalyst
amine
reaction
palladium
primary
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP58238221A
Other languages
English (en)
Japanese (ja)
Other versions
JPH0533214B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html
Inventor
Kazuhiko Okabe
和彦 岡部
Yukinaga Yokota
行永 横田
Kazuto Matsutani
松谷　和人
Takehiro Imanaka
今中　健博
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Kao Corp
Original Assignee
Kao Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kao Corp filed Critical Kao Corp
Priority to JP58238221A priority Critical patent/JPS60130551A/ja
Priority to ES538216A priority patent/ES8600200A1/es
Priority to MX203651A priority patent/MX155563A/es
Publication of JPS60130551A publication Critical patent/JPS60130551A/ja
Priority to US06/913,621 priority patent/US4757144A/en
Publication of JPH0533214B2 publication Critical patent/JPH0533214B2/ja
Granted legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/24—Preparation of compounds containing amino groups bound to a carbon skeleton by reductive alkylation of ammonia, amines or compounds having groups reducible to amino groups, with carbonyl compounds
    • C07C209/26—Preparation of compounds containing amino groups bound to a carbon skeleton by reductive alkylation of ammonia, amines or compounds having groups reducible to amino groups, with carbonyl compounds by reduction with hydrogen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00—Compounds containing amino groups bound to a carbon skeleton
    • C07C211/01—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms
    • C07C211/02—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton
    • C07C211/03—Monoamines
    • C07C211/08—Monoamines containing alkyl groups having a different number of carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00—Compounds containing amino groups bound to a carbon skeleton
    • C07C211/01—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms
    • C07C211/02—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton
    • C07C211/09—Diamines
    • C07C211/12—1,6-Diaminohexanes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00—Compounds containing amino groups bound to a carbon skeleton
    • C07C211/33—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of rings other than six-membered aromatic rings
    • C07C211/34—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of rings other than six-membered aromatic rings of a saturated carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
    • C07C213/08—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton by reactions not involving the formation of amino groups, hydroxy groups or etherified or esterified hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C215/00—Compounds containing amino and hydroxy groups bound to the same carbon skeleton
    • C07C215/02—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C215/04—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being saturated
    • C07C215/06—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being saturated and acyclic
    • C07C215/12—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being saturated and acyclic the nitrogen atom of the amino group being further bound to hydrocarbon groups substituted by hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
    • C07D295/04—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms
    • C07D295/12—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly or doubly bound nitrogen atoms
    • C07D295/125—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly or doubly bound nitrogen atoms with the ring nitrogen atoms and the substituent nitrogen atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings
    • C07D295/13—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly or doubly bound nitrogen atoms with the ring nitrogen atoms and the substituent nitrogen atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings to an acyclic saturated chain
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B01J23/42—Platinum
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B01J23/44—Palladium

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
JP58238221A 1983-12-16 1983-12-16 第３級アミンの製造方法 Granted JPS60130551A (ja)

Priority Applications (4)

Application Number Priority Date Filing Date Title
JP58238221A JPS60130551A (ja) 1983-12-16 1983-12-16 第３級アミンの製造方法
ES538216A ES8600200A1 (es) 1983-12-16 1984-12-03 Un procedimiento para la preparacion de una amina terciaria
MX203651A MX155563A (es) 1983-12-16 1984-12-07 Procedimiento para preparar amina terciaria
US06/913,621 US4757144A (en) 1983-12-16 1986-09-30 Preparing tertiary amine from formaldehyde and primary and/or secondary amine

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP58238221A JPS60130551A (ja) 1983-12-16 1983-12-16 第３級アミンの製造方法

Publications (2)

Publication Number Publication Date
JPS60130551A true JPS60130551A (ja) 1985-07-12
JPH0533214B2 JPH0533214B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) 1993-05-19

Family

ID=17026945

Family Applications (1)

Application Number Title Priority Date Filing Date
JP58238221A Granted JPS60130551A (ja) 1983-12-16 1983-12-16 第３級アミンの製造方法

Country Status (4)

Country Link
US (1) US4757144A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
JP (1) JPS60130551A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
ES (1) ES8600200A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
MX (1) MX155563A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS62252746A (ja) * 1986-04-24 1987-11-04 Mitsubishi Chem Ind Ltd ３級アミンの製造方法
US5105013A (en) * 1988-12-19 1992-04-14 The Dow Chemical Company Method for the reductive methylation of primary amines
JP2007176897A (ja) * 2005-12-28 2007-07-12 Kao Corp ３級アミンの製造法
JP2009286747A (ja) * 2008-05-30 2009-12-10 Tosoh Corp 脂環式アミン類の製造法

Families Citing this family (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5266730A (en) * 1987-10-16 1993-11-30 Kao Corporation Process for preparing N-substituted amine
DE3741726A1 (de) * 1987-12-09 1989-06-22 Ruhrchemie Ag Verfahren zur herstellung von tertiaeren n,n-dimethylaminen
JP3174425B2 (ja) * 1993-03-19 2001-06-11 三井化学株式会社 Ｎ，ｎ−二置換アミノフェノール類の製造法
ES2117091T5 (es) * 1993-06-30 2002-02-01 Procter & Gamble Alquilacion reductora de amina para preparar aminopoliol terciario como precursor de esteres suavizantes de tejidos.
US5414087A (en) * 1993-07-07 1995-05-09 Huntsman Corporation Preparation of N-alkylpiperazines
US5646235A (en) * 1995-03-27 1997-07-08 Huntsman Petrochemical Corporation Reductive alkylation of polyamines
WO2001044162A1 (en) * 1999-12-14 2001-06-21 Celgro Process for the preparation of secondary and tertiary amines
US6107521A (en) * 1999-12-14 2000-08-22 Celgro Process for the preparation of secondary amines
ATE272662T1 (de) 2000-07-03 2004-08-15 Vantico Gmbh & Co Kg Härtbare zusammensetzungen aus glycidylverbindungen, aminischen härtern und niedrigviskosen härtungsbeschleunigern
DE10316375A1 (de) * 2003-04-10 2004-11-04 Celanese Chemicals Europe Gmbh Verfahren zur Herstellung von N-Methyl-dialkylaminen aus sekundären Dialkylaminen und Formaldehyd
EP2029521B1 (de) * 2006-05-31 2012-07-11 Basf Se Verfahren zur herstellung eines amins
BR112013000236B1 (pt) 2010-07-06 2018-11-13 Catexel Limited método de produzir um composto, e, sal protonado
FR3014100B1 (fr) * 2013-11-29 2016-01-01 IFP Energies Nouvelles Procede de synthese d'un melange de n,n,n',n'-tetramethyl-1,6-hexanediamine et de n,n,n',n'-tetramethyldiaminoethers
MX2016000701A (es) 2015-01-22 2016-11-24 Evonik Degussa Gmbh Proceso para preparar un compuesto de triacetonamina n-metil sustituida.
CN110621390A (zh) * 2017-05-15 2019-12-27 罗地亚经营管理公司 用于清除空气中甲醛的方法
CN109239208A (zh) * 2017-07-11 2019-01-18 四川科瑞德凯华制药有限公司 一种盐酸曲恩汀的质量检测方法
CN114874431B (zh) * 2022-06-13 2023-03-28 江南大学 一种端叔胺基聚醚型非离子表面活性剂的制备方法
WO2025027195A1 (en) * 2023-08-03 2025-02-06 Basf Se Process for the production of n-methylmorpholine having low hazen color number

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1305258A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * 1969-06-26 1973-01-31
JPS5781444A (en) * 1980-11-10 1982-05-21 Mitsubishi Petrochem Co Ltd Preparation of n-alkyl-substituted aromatic amino compound
JPS60112743A (ja) * 1983-11-22 1985-06-19 Nippon Oil & Fats Co Ltd 第三アミンの製造方法

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2809995A (en) * 1951-12-31 1957-10-15 Ruhrchemie Ag Production of amines
US2776313A (en) * 1955-02-02 1957-01-01 Eastman Kodak Co Process for making n, n-dialkyl-p-aminophenol
NL127232C (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * 1963-03-12 1900-01-01
US3522309A (en) * 1967-08-31 1970-07-28 Du Pont Reductive alkylation process for production of n-alkylated amines
US3597438A (en) * 1968-05-06 1971-08-03 Du Pont Reductive amination of aldehydes with rhodium catalysts
DE2816460C3 (de) * 1978-04-15 1981-11-12 Akzo Gmbh, 5600 Wuppertal Verfahren zur Herstellung von asymmetrischen N-Phenyl-N`-substituierten p-Phenylendiaminen

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1305258A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * 1969-06-26 1973-01-31
JPS5781444A (en) * 1980-11-10 1982-05-21 Mitsubishi Petrochem Co Ltd Preparation of n-alkyl-substituted aromatic amino compound
JPS60112743A (ja) * 1983-11-22 1985-06-19 Nippon Oil & Fats Co Ltd 第三アミンの製造方法

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS62252746A (ja) * 1986-04-24 1987-11-04 Mitsubishi Chem Ind Ltd ３級アミンの製造方法
US5105013A (en) * 1988-12-19 1992-04-14 The Dow Chemical Company Method for the reductive methylation of primary amines
JP2007176897A (ja) * 2005-12-28 2007-07-12 Kao Corp ３級アミンの製造法
JP2009286747A (ja) * 2008-05-30 2009-12-10 Tosoh Corp 脂環式アミン類の製造法

Also Published As

Publication number Publication date
US4757144A (en) 1988-07-12
MX155563A (es) 1988-03-25
ES538216A0 (es) 1985-10-01
ES8600200A1 (es) 1985-10-01
JPH0533214B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) 1993-05-19

Similar Documents

Publication Publication Date Title
JPS60130551A (ja) 第３級アミンの製造方法
US5773657A (en) Hydrogenation of aromatic compounds in which at least one amino group is bonded to an aromatic nucleus
JP4979877B2 (ja) ジエチレントリアミンおよび高級ポリエチレンポリアミンの製造のための方法
US4960941A (en) Hydrogenation of aromatic amines to produce their ring hydrogenated counterparts
JPH0229066B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
CN108602788B (zh) 制备高级亚乙基胺和亚乙基胺衍生物的方法
JPH0112745B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
US3644522A (en) Catalytic hydrogenation of nitrogen containing compounds over supported ruthenium catalysts
JP5426362B2 (ja) 高汚染メチレンジアニリンの水素化方法
EP0618895B1 (en) Process for the preparation of an aminonitrile by partial hydrogenation of a nitrile compound with two or more nitrile groups
US5648545A (en) Preparation of amines from nitriles by alkylation with a nitrogen compound in the presence of a copper oxide/zirconium oxide catalyst
JP4142861B2 (ja) 環状脂肪族の第１級ビシナルジアミンのシアノエチル化
US5364971A (en) Decolorization of polyethylene polyamines using ruthenium
US6248925B1 (en) Selective reductive amination of nitriles
EP0618188B1 (en) Process for the preparation of cyclohexylamines by catalytic hydrogenation of anilines
JPH0417942B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
JPH06239809A (ja) 第３級アミンの製造方法
US6140540A (en) Hydrogenation of aromatic amines to produce their ring hydrogenated counterparts
US6121493A (en) Isomerization of cyclohexylamines to produce their thermodynamic isomeric form
JP4070859B2 (ja) 高品質ポリアミンの製造方法
JPS60112743A (ja) 第三アミンの製造方法
JPH10506386A (ja) 芳香族アミンの水素化速度を増す方法
CN1308285C (zh) 制备乙基二甲胺和三乙胺的方法
JP3012399B2 (ja) ジシクロヘキシルアミン類の製造方法
JP3973719B2 (ja) 第１級アミンの製法