JPS59128340A - ２，３−ジクロル−１−プロパノ−ルの製造法 - Google Patents
２，３−ジクロル−１−プロパノ−ルの製造法Info
- Publication number
- JPS59128340A JPS59128340A JP110083A JP110083A JPS59128340A JP S59128340 A JPS59128340 A JP S59128340A JP 110083 A JP110083 A JP 110083A JP 110083 A JP110083 A JP 110083A JP S59128340 A JPS59128340 A JP S59128340A
- Authority
- JP
- Japan
- Prior art keywords
- reaction
- solvent
- hydrogen chloride
- aqueous solution
- hydrochloric acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- ZXCYIJGIGSDJQQ-UHFFFAOYSA-N 2,3-dichloropropan-1-ol Chemical compound OCC(Cl)CCl ZXCYIJGIGSDJQQ-UHFFFAOYSA-N 0.000 title description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims abstract description 40
- XXROGKLTLUQVRX-UHFFFAOYSA-N allyl alcohol Chemical compound OCC=C XXROGKLTLUQVRX-UHFFFAOYSA-N 0.000 claims abstract description 22
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 claims abstract description 18
- 229910000041 hydrogen chloride Inorganic materials 0.000 claims abstract description 18
- 238000006243 chemical reaction Methods 0.000 claims abstract description 17
- 239000002904 solvent Substances 0.000 claims abstract description 15
- 239000007864 aqueous solution Substances 0.000 claims abstract description 12
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000000460 chlorine Substances 0.000 claims abstract description 10
- 229910052801 chlorine Inorganic materials 0.000 claims abstract description 10
- 238000004519 manufacturing process Methods 0.000 claims description 6
- XEPXTKKIWBPAEG-UHFFFAOYSA-N 1,1-dichloropropan-1-ol Chemical compound CCC(O)(Cl)Cl XEPXTKKIWBPAEG-UHFFFAOYSA-N 0.000 claims 1
- 238000000034 method Methods 0.000 abstract description 10
- 239000000243 solution Substances 0.000 abstract description 8
- 239000003960 organic solvent Substances 0.000 abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 6
- 238000000926 separation method Methods 0.000 abstract description 3
- BRLQWZUYTZBJKN-UHFFFAOYSA-N Epichlorohydrin Chemical compound ClCC1CO1 BRLQWZUYTZBJKN-UHFFFAOYSA-N 0.000 abstract description 2
- 238000004821 distillation Methods 0.000 abstract description 2
- 239000007795 chemical reaction product Substances 0.000 abstract 3
- 239000000126 substance Substances 0.000 abstract 3
- 239000006227 byproduct Substances 0.000 description 8
- 239000000047 product Substances 0.000 description 4
- QGJOPFRUJISHPQ-UHFFFAOYSA-N Carbon disulfide Chemical compound S=C=S QGJOPFRUJISHPQ-UHFFFAOYSA-N 0.000 description 3
- 238000005660 chlorination reaction Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 229920006395 saturated elastomer Polymers 0.000 description 3
- BDERNNFJNOPAEC-UHFFFAOYSA-N 1-propanol Substances CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 238000004811 liquid chromatography Methods 0.000 description 2
- NQCBIMOYRRMVNA-UHFFFAOYSA-N propane-1,2,3-triol;hydrochloride Chemical compound Cl.OCC(O)CO NQCBIMOYRRMVNA-UHFFFAOYSA-N 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 description 1
- RZWHKKIXMPLQEM-UHFFFAOYSA-N 1-chloropropan-1-ol Chemical compound CCC(O)Cl RZWHKKIXMPLQEM-UHFFFAOYSA-N 0.000 description 1
- KFZMGEQAYNKOFK-UHFFFAOYSA-N 2-propanol Substances CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 1
- OSDWBNJEKMUWAV-UHFFFAOYSA-N Allyl chloride Chemical compound ClCC=C OSDWBNJEKMUWAV-UHFFFAOYSA-N 0.000 description 1
- 241000238557 Decapoda Species 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000007805 chemical reaction reactant Substances 0.000 description 1
- XENVCRGQTABGKY-ZHACJKMWSA-N chlorohydrin Chemical compound CC#CC#CC#CC#C\C=C\C(Cl)CO XENVCRGQTABGKY-ZHACJKMWSA-N 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 239000003822 epoxy resin Substances 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 229920000647 polyepoxide Polymers 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 239000005060 rubber Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000012047 saturated solution Substances 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 229920003051 synthetic elastomer Polymers 0.000 description 1
- 239000005061 synthetic rubber Substances 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP110083A JPS59128340A (ja) | 1983-01-10 | 1983-01-10 | ２，３−ジクロル−１−プロパノ−ルの製造法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP110083A JPS59128340A (ja) | 1983-01-10 | 1983-01-10 | ２，３−ジクロル−１−プロパノ−ルの製造法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS59128340A true JPS59128340A (ja) | 1984-07-24 |
| JPS6160054B2 JPS6160054B2 (enrdf_load_stackoverflow) | 1986-12-19 |
Family
ID=11492058
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP110083A Granted JPS59128340A (ja) | 1983-01-10 | 1983-01-10 | ２，３−ジクロル−１−プロパノ−ルの製造法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS59128340A (enrdf_load_stackoverflow) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2565229A1 (fr) * | 1984-06-04 | 1985-12-06 | Showa Denko Kk | Procede de production d'epichlorhydrine |
| JPS63290835A (ja) * | 1987-05-21 | 1988-11-28 | Showa Denko Kk | ２，３−ジクロロ−１−プロパノ−ルの製造法 |
| EP1059278A3 (en) * | 1999-06-08 | 2003-11-12 | Showa Denko Kabushiki Kaisha | Process for producing epichlorohydrin and intermediate thereof |
| US6743955B2 (en) | 2001-04-26 | 2004-06-01 | Showa Denko K.K. | Method for producing 2,3-dichloro-1-propanol and epichlorohyrin |
-
1983
- 1983-01-10 JP JP110083A patent/JPS59128340A/ja active Granted
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2565229A1 (fr) * | 1984-06-04 | 1985-12-06 | Showa Denko Kk | Procede de production d'epichlorhydrine |
| JPS63290835A (ja) * | 1987-05-21 | 1988-11-28 | Showa Denko Kk | ２，３−ジクロロ−１−プロパノ−ルの製造法 |
| EP1059278A3 (en) * | 1999-06-08 | 2003-11-12 | Showa Denko Kabushiki Kaisha | Process for producing epichlorohydrin and intermediate thereof |
| US6743955B2 (en) | 2001-04-26 | 2004-06-01 | Showa Denko K.K. | Method for producing 2,3-dichloro-1-propanol and epichlorohyrin |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6160054B2 (enrdf_load_stackoverflow) | 1986-12-19 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JPS60258171A (ja) | エピクロルヒドリンの製造方法 | |
| JP2003518052A (ja) | フッ素含有アリルエーテルおよび高級同族体 | |
| JPS6256150B2 (enrdf_load_stackoverflow) | ||
| EP0688309B1 (en) | Continuous process for purifying perfluorochemical compositions | |
| US4328376A (en) | Method of removing fluorinated olefin byproduct formed during the synthesis of a fluorinated ether | |
| JPS59128340A (ja) | ２，３−ジクロル−１−プロパノ−ルの製造法 | |
| JPS58105933A (ja) | クロルアセトアルデヒドジメチルアセタ−ルの製法 | |
| JP2562918B2 (ja) | ハロゲン化ポリエーテルの製造方法 | |
| US5155256A (en) | Process for preparing 2-bromoethyl acetate | |
| JP4511359B2 (ja) | 殺虫剤用の合成中間体を調製するための新規方法 | |
| JP3777408B2 (ja) | カルボン酸誘導体の製造法 | |
| JP4467890B2 (ja) | チオフェンのクロロメチル化 | |
| KR101284659B1 (ko) | 1,2,2,2-테트라플루오로에틸 디플루오로메틸 에테르의제조방법 | |
| EP0063352B1 (en) | Process for preparing 5-fluorocytosine salt | |
| JPH09509942A (ja) | ポリフルオロオキセタン類の製造方法 | |
| US3763230A (en) | Sulfonium compounds of alpha-hydroxy-ypsilon-alkylmercaptobutyric acid | |
| JPS59128341A (ja) | ２，３−ジクロル−１−プロパノ−ルの製造方法 | |
| JP3834096B2 (ja) | 含フッ素アルキルエーテルの製造方法 | |
| JP2553261B2 (ja) | クロルヒドリンの製造方法 | |
| JP3110682B2 (ja) | ソルビン酸の製造方法 | |
| JPS6219544A (ja) | ２，３−ジクロル−１−プロパノ−ルの製法 | |
| JP3172173B2 (ja) | フルオロカーボン化合物及びその製造法 | |
| JP2937330B2 (ja) | ビス（２，３，５，６−テトラフルオロー４−アミノフェニル）メタン | |
| JPH0723332B2 (ja) | １，３−ジクロル−２−プロパノ−ルの製造法 | |
| JPS62223141A (ja) | アリルエ−テル類の製法 |