JPS5883029A - ポリテトラメチレンアジプアミドの製造方法 - Google Patents
ポリテトラメチレンアジプアミドの製造方法Info
- Publication number
- JPS5883029A JPS5883029A JP57176017A JP17601782A JPS5883029A JP S5883029 A JPS5883029 A JP S5883029A JP 57176017 A JP57176017 A JP 57176017A JP 17601782 A JP17601782 A JP 17601782A JP S5883029 A JPS5883029 A JP S5883029A
- Authority
- JP
- Japan
- Prior art keywords
- polymer
- solvent
- polyamide
- temperature
- pyrrolidone
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000004519 manufacturing process Methods 0.000 title claims description 3
- -1 polytetramethylene Polymers 0.000 title description 4
- GVNWZKBFMFUVNX-UHFFFAOYSA-N Adipamide Chemical compound NC(=O)CCCCC(N)=O GVNWZKBFMFUVNX-UHFFFAOYSA-N 0.000 title 1
- 238000000034 method Methods 0.000 claims description 20
- 229920000642 polymer Polymers 0.000 claims description 20
- KIDHWZJUCRJVML-UHFFFAOYSA-N putrescine Chemical compound NCCCCN KIDHWZJUCRJVML-UHFFFAOYSA-N 0.000 claims description 18
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 claims description 16
- 239000002904 solvent Substances 0.000 claims description 13
- 239000004952 Polyamide Substances 0.000 claims description 9
- 239000005700 Putrescine Substances 0.000 claims description 9
- 229920002647 polyamide Polymers 0.000 claims description 9
- 239000001361 adipic acid Substances 0.000 claims description 8
- 235000011037 adipic acid Nutrition 0.000 claims description 8
- 150000001875 compounds Chemical class 0.000 claims description 8
- 239000013040 bath agent Substances 0.000 claims description 7
- 150000003839 salts Chemical class 0.000 claims description 7
- HNJBEVLQSNELDL-UHFFFAOYSA-N pyrrolidin-2-one Chemical compound O=C1CCCN1 HNJBEVLQSNELDL-UHFFFAOYSA-N 0.000 claims description 6
- 238000009835 boiling Methods 0.000 claims description 4
- 239000007858 starting material Substances 0.000 claims description 3
- SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 description 4
- 238000009833 condensation Methods 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- GHWVXCQZPNWFRO-UHFFFAOYSA-N butane-2,3-diamine Chemical compound CC(N)C(C)N GHWVXCQZPNWFRO-UHFFFAOYSA-N 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 150000001279 adipic acids Chemical class 0.000 description 2
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 2
- 238000005119 centrifugation Methods 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- JBKVHLHDHHXQEQ-UHFFFAOYSA-N epsilon-caprolactam Chemical compound O=C1CCCCCN1 JBKVHLHDHHXQEQ-UHFFFAOYSA-N 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- NAQMVNRVTILPCV-UHFFFAOYSA-N hexane-1,6-diamine Chemical compound NCCCCCCN NAQMVNRVTILPCV-UHFFFAOYSA-N 0.000 description 2
- QQVIHTHCMHWDBS-UHFFFAOYSA-N isophthalic acid Chemical compound OC(=O)C1=CC=CC(C(O)=O)=C1 QQVIHTHCMHWDBS-UHFFFAOYSA-N 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 239000000376 reactant Substances 0.000 description 2
- CXMXRPHRNRROMY-UHFFFAOYSA-N sebacic acid Chemical compound OC(=O)CCCCCCCCC(O)=O CXMXRPHRNRROMY-UHFFFAOYSA-N 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- SLXKOJJOQWFEFD-UHFFFAOYSA-M 6-aminohexanoate Chemical compound NCCCCCC([O-])=O SLXKOJJOQWFEFD-UHFFFAOYSA-M 0.000 description 1
- 239000005711 Benzoic acid Substances 0.000 description 1
- 241000218691 Cupressaceae Species 0.000 description 1
- JHWNWJKBPDFINM-UHFFFAOYSA-N Laurolactam Chemical compound O=C1CCCCCCCCCCCN1 JHWNWJKBPDFINM-UHFFFAOYSA-N 0.000 description 1
- 229920003189 Nylon 4,6 Polymers 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 235000010233 benzoic acid Nutrition 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 150000004985 diamines Chemical class 0.000 description 1
- 150000001991 dicarboxylic acids Chemical class 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 229920006158 high molecular weight polymer Polymers 0.000 description 1
- 229920001519 homopolymer Polymers 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 230000002427 irreversible effect Effects 0.000 description 1
- 150000003951 lactams Chemical class 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- DYFXGORUJGZJCA-UHFFFAOYSA-N phenylmethanediamine Chemical compound NC(N)C1=CC=CC=C1 DYFXGORUJGZJCA-UHFFFAOYSA-N 0.000 description 1
- 239000003495 polar organic solvent Substances 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000007790 solid phase Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
- C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
- C08G69/26—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from polyamines and polycarboxylic acids
- C08G69/28—Preparatory processes
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polyamides (AREA)
- Artificial Filaments (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL8104639 | 1981-10-13 | ||
| NL8104639A NL8104639A (nl) | 1981-10-13 | 1981-10-13 | Werkwijze voor het maken van polytetramethyleenadipamide. |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPS5883029A true JPS5883029A (ja) | 1983-05-18 |
Family
ID=19838209
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP57176017A Pending JPS5883029A (ja) | 1981-10-13 | 1982-10-06 | ポリテトラメチレンアジプアミドの製造方法 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US4463166A (enExample) |
| EP (1) | EP0077106B1 (enExample) |
| JP (1) | JPS5883029A (enExample) |
| CA (1) | CA1188040A (enExample) |
| DE (1) | DE3268581D1 (enExample) |
| ES (1) | ES516413A0 (enExample) |
| IN (1) | IN155281B (enExample) |
| NL (1) | NL8104639A (enExample) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0712359A (ja) * | 1993-06-25 | 1995-01-17 | Tomeji Kawasaki | 集合住宅の調理用排気装置 |
| US20150252188A1 (en) * | 2011-05-13 | 2015-09-10 | Dsm Ip Assets B.V. | Flame retardant semi-aromatic polyamide composition and moulded products made therefrom |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3407492A1 (de) * | 1984-03-01 | 1985-09-05 | Bayer Ag, 5090 Leverkusen | Verfahren zur herstellung von copolyamiden aus adipinsaeure, terephthalsaeure und hexamethylendiamin |
| JPS60220731A (ja) * | 1984-04-17 | 1985-11-05 | Unitika Ltd | ポリアミドフィルムおよびその製造方法 |
| NL8401271A (nl) * | 1984-04-19 | 1985-11-18 | Stamicarbon | Werkwijze voor het bereiden van polytetramethyleenadipamide. |
| EP0207539B1 (en) * | 1985-05-31 | 1989-11-23 | Stamicarbon B.V. | Process for the preparation of nylon 4,6 |
| WO1987002680A2 (en) * | 1985-11-01 | 1987-05-07 | Teijin Limited | Polyamide packaging material |
| NL8601893A (nl) * | 1986-07-22 | 1988-02-16 | Stamicarbon | Bereiding van hoog-moleculair polytetramethyleenadipamide. |
| EP2451863A1 (en) | 2009-07-09 | 2012-05-16 | Invista Technologies S.A R.L. | Preparation of polyamides |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE429727A (enExample) * | 1937-08-20 | |||
| US3932364A (en) * | 1972-10-17 | 1976-01-13 | Sumitomo Chemical Company, Limited | Production of polyamides in the presence of a phosphorus acid ester and an organic base |
-
1981
- 1981-10-13 NL NL8104639A patent/NL8104639A/nl not_active Application Discontinuation
-
1982
- 1982-10-06 JP JP57176017A patent/JPS5883029A/ja active Pending
- 1982-10-11 ES ES516413A patent/ES516413A0/es active Granted
- 1982-10-12 DE DE8282201262T patent/DE3268581D1/de not_active Expired
- 1982-10-12 EP EP82201262A patent/EP0077106B1/en not_active Expired
- 1982-10-12 CA CA000413215A patent/CA1188040A/en not_active Expired
- 1982-10-13 US US06/433,879 patent/US4463166A/en not_active Expired - Fee Related
- 1982-10-13 IN IN1187/CAL/82A patent/IN155281B/en unknown
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0712359A (ja) * | 1993-06-25 | 1995-01-17 | Tomeji Kawasaki | 集合住宅の調理用排気装置 |
| US20150252188A1 (en) * | 2011-05-13 | 2015-09-10 | Dsm Ip Assets B.V. | Flame retardant semi-aromatic polyamide composition and moulded products made therefrom |
Also Published As
| Publication number | Publication date |
|---|---|
| IN155281B (enExample) | 1985-01-12 |
| CA1188040A (en) | 1985-05-28 |
| ES8307267A1 (es) | 1983-06-16 |
| ES516413A0 (es) | 1983-06-16 |
| US4463166A (en) | 1984-07-31 |
| DE3268581D1 (en) | 1986-02-27 |
| NL8104639A (nl) | 1983-05-02 |
| EP0077106A1 (en) | 1983-04-20 |
| EP0077106B1 (en) | 1986-01-15 |
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