JPH0662502B2 - 脂肪酸メチルエステルの製法 - Google Patents
脂肪酸メチルエステルの製法Info
- Publication number
- JPH0662502B2 JPH0662502B2 JP60277773A JP27777385A JPH0662502B2 JP H0662502 B2 JPH0662502 B2 JP H0662502B2 JP 60277773 A JP60277773 A JP 60277773A JP 27777385 A JP27777385 A JP 27777385A JP H0662502 B2 JPH0662502 B2 JP H0662502B2
- Authority
- JP
- Japan
- Prior art keywords
- methanol
- glycerol
- oil phase
- weight
- mixture
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
- C11C3/003—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
- C11C3/04—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fats or fatty oils
Landscapes
- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Fats And Perfumes (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Hydrogenated Pyridines (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE3444893.4 | 1984-12-08 | ||
DE19843444893 DE3444893A1 (de) | 1984-12-08 | 1984-12-08 | Verfahren zur herstellung von fettsaeuremethylestern |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS61140544A JPS61140544A (ja) | 1986-06-27 |
JPH0662502B2 true JPH0662502B2 (ja) | 1994-08-17 |
Family
ID=6252300
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP60277773A Expired - Lifetime JPH0662502B2 (ja) | 1984-12-08 | 1985-12-09 | 脂肪酸メチルエステルの製法 |
Country Status (13)
Country | Link |
---|---|
US (1) | US4652406A (fr) |
EP (1) | EP0184740B1 (fr) |
JP (1) | JPH0662502B2 (fr) |
AT (1) | ATE61332T1 (fr) |
BR (1) | BR8506119A (fr) |
CA (1) | CA1261870A (fr) |
DE (2) | DE3444893A1 (fr) |
ES (1) | ES8606242A1 (fr) |
GB (1) | GB2168701B (fr) |
MX (1) | MX162267A (fr) |
MY (1) | MY101291A (fr) |
TR (1) | TR25060A (fr) |
ZA (1) | ZA859371B (fr) |
Families Citing this family (55)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1987007632A1 (fr) * | 1986-06-11 | 1987-12-17 | Bio-Energy Technology Ltd. | Production de carburant biologique |
DE3707563A1 (de) * | 1987-03-10 | 1988-09-22 | Klaus Dr Ing Scharmer | Verfahren zur alkoholyse von fettsaeureglyceriden und vorrichtung zum durchfuehren des verfahrens |
SE9001245L (sv) * | 1990-04-05 | 1991-10-06 | Carl Johan Lindquist | Foerestringsprocess |
US6262022B1 (en) | 1992-06-25 | 2001-07-17 | Novartis Ag | Pharmaceutical compositions containing cyclosporin as the active agent |
CA2083346A1 (fr) * | 1991-12-13 | 1993-06-14 | Eric G. Lundquist | Procede d'esterification par catalyse |
DE4209779C1 (fr) * | 1992-03-26 | 1993-07-15 | Oelmuehle Leer Connemann Gmbh & Co., 2950 Leer, De | |
DK0642332T3 (da) | 1992-05-13 | 1997-06-16 | Sandoz Ltd | Ophthalmiske præparater indeholdende cyclosporin |
EP1142568A1 (fr) | 1992-09-25 | 2001-10-10 | Novartis AG | Compositions pharmaceutiques à base de cyclosporines |
AT399336B (de) * | 1993-07-14 | 1995-04-25 | Martin Mag Dr Mittelbach | Verfahren zur herstellung von fettsäurealkylestern |
BR9807528A (pt) | 1997-01-30 | 2000-03-14 | Novartis Ag | Composições farmacêuticas isentas de óleo contendo ciclosporina a |
DE19732578C2 (de) * | 1997-07-29 | 2000-08-24 | Aventis Res & Tech Gmbh & Co | Verwendung von sulfonierten aromatischen Polyetherketon-Kationenaustauschern und sulfonierten Polyphenylensulfid-Kationenaustauschern als Katalysatoren |
DE19810440C1 (de) * | 1998-03-11 | 1999-09-23 | Dhw Deutsche Hydrierwerke Gmbh | Verfahren zur Herstellung von ungesättigten Fettalkoholen aus Lauricölen |
ATA16992000A (de) | 2000-10-05 | 2001-12-15 | Michael Dr Koncar | Verfahren zur herstellung von fettsäurealkylestern |
US6965044B1 (en) | 2001-07-06 | 2005-11-15 | Iowa State University Research Foundation | Method of converting free fatty acids to fatty acid methyl esters with small excess of methanol |
DE10154365A1 (de) * | 2001-11-06 | 2003-05-15 | Cognis Deutschland Gmbh | Verfahren zur Herstellung von Fettsäureestern aus nicht entsäuerten Fetten und Ölen |
AT504727A1 (de) * | 2002-04-12 | 2008-07-15 | Energea Umwelttechnologie Gmbh | Verfahren und anlage zur veresterung von fettsäuren |
US20060042158A1 (en) * | 2004-08-26 | 2006-03-02 | Lee John H | Fuel products from plant or animal lipids |
US7619104B2 (en) * | 2005-04-04 | 2009-11-17 | Renewable Products Development Laboratories, Inc. | Process for producing biodiesel or fatty acid esters from multiple triglyceride feedstocks |
EP1897865B1 (fr) * | 2005-06-27 | 2011-06-08 | Tokyo Institute Of Technology | Procédés servant à produire des esters d'acides gras supérieurs |
US7622600B1 (en) * | 2006-01-06 | 2009-11-24 | Redland Industries, Inc. | System and method for the continuous production of bio-diesel |
US7828978B2 (en) | 2006-01-11 | 2010-11-09 | Doug Geier | Simultaneous synthesis and purification of a fatty acid monoester biodiesel fuel |
US7951967B2 (en) | 2006-04-28 | 2011-05-31 | Sk Chemicals Co., Ltd. | Method and apparatus for preparing fatty acid alkyl ester using fatty acid |
WO2008016330A2 (fr) * | 2006-08-01 | 2008-02-07 | Sie Hendery @ Hendery | Bioformule pour remplacer le carburant diesel |
US20100130763A1 (en) * | 2006-12-06 | 2010-05-27 | Southern Illinois University Carbondale | Processes for the production of fatty acid alkyl esters |
US20080289248A1 (en) * | 2007-05-23 | 2008-11-27 | Southern Illinois University Carbondale | Immobilized esterification catalysts for producing fatty acid alkyl esters |
WO2008071040A1 (fr) | 2006-12-15 | 2008-06-19 | China Petroleum & Chemical Corporation | Procédé de préparation de biodiesel |
US8500828B2 (en) | 2006-12-15 | 2013-08-06 | China Petroleum & Chemical Corporation | Process for preparing a bio-diesel |
JP2008260819A (ja) * | 2007-04-11 | 2008-10-30 | National Institute Of Advanced Industrial & Technology | バイオディーゼル燃料の製造方法 |
US20080282606A1 (en) * | 2007-04-16 | 2008-11-20 | Plaza John P | System and process for producing biodiesel |
US20100242346A1 (en) * | 2007-09-19 | 2010-09-30 | Best Energies, Inc | Processes for the esterification of free fatty acids and the production of biodiesel |
US20090187035A1 (en) * | 2008-01-22 | 2009-07-23 | Cargill, Incorporated | Process for production of fatty acid alkyl esters |
US20090247785A1 (en) * | 2008-03-31 | 2009-10-01 | The University Of Connecticut | Methods and systems for pretreatment of an oil stream |
JP5380523B2 (ja) | 2008-04-01 | 2014-01-08 | エスケー ケミカルズ カンパニー リミテッド | 脂肪酸を用いた脂肪酸アルキルエステルの製造方法 |
FR2929621A1 (fr) * | 2008-04-08 | 2009-10-09 | Arkema France | Utilisation d'acide methane sulfonique pour l'esterification d'acides gras |
WO2009139884A1 (fr) * | 2008-05-14 | 2009-11-19 | Ethox Chemicals, Llc | Beurres naturels reconstitués par transestérification avec de la glycérine et leurs utilisations dans des applications cosmétiques |
US8742150B2 (en) * | 2008-05-14 | 2014-06-03 | Council Of Scientific & Industrial Research | Castor oil fatty acid based estolide esters and their derivatives as potential lubricant base stocks |
KR101554607B1 (ko) | 2008-11-07 | 2015-09-22 | 에스케이케미칼주식회사 | 지방산을 이용한 지방산알킬에스테르의 제조방법 및 장치 |
ES2457097T5 (es) † | 2008-11-17 | 2018-04-16 | Basf Se | Uso de ácido metanosulfónico para la preparación de ésteres de ácidos grasos |
MX2011006179A (es) | 2008-12-08 | 2014-04-25 | Initio Fuels Llc | Transesterificacion de una sola etapa de materia prima de alimentacion usando catalizador gaseoso. |
WO2010148652A1 (fr) | 2009-06-26 | 2010-12-29 | 中国石油化工股份有限公司 | Composition de diesel et procédé pour l'amélioration de la stabilité d'un biodiesel à l'oxydation |
CN102575272B (zh) | 2009-07-17 | 2014-12-10 | 韩国科学技术院 | 使用有产油能力的微生物生产脂肪酸烷基酯的方法 |
MY151440A (en) * | 2009-10-29 | 2014-05-30 | Malaysian Palm Oil Board Mpob | A method of converting free fatty acid (ffa) from oil to methyl ester |
AT510636B1 (de) | 2010-10-28 | 2016-11-15 | Wimmer Theodor | Verfahren zur herstellung von fettsäureestern niederer alkohole |
CN102851122A (zh) * | 2011-06-30 | 2013-01-02 | 中国石油化工股份有限公司 | 一种制备脂肪酸酯的方法 |
CN103013678B (zh) * | 2011-09-20 | 2014-12-31 | 中国石油化工股份有限公司 | 降低生物柴油粗产品酸值的方法以及生物柴油的制备方法 |
KR102327852B1 (ko) | 2013-07-22 | 2021-11-18 | 에스케이에코프라임 주식회사 | 지방을 이용한 지방산알킬에스테르의 제조방법 |
US9328054B1 (en) | 2013-09-27 | 2016-05-03 | Travis Danner | Method of alcoholisis of fatty acids and fatty acid gyicerides |
AU2015227367A1 (en) * | 2014-03-04 | 2016-09-22 | Basf Se | Method for degumming and esterification of an oil |
ES2585706B1 (es) * | 2016-04-21 | 2017-08-14 | Soluciones Industriales Extremeñas Sll | Procedimiento mejorado para el refino y esterificación continua de cualquier material graso de origen vegetal o animal, especialmente diseñado para subproductos animales de categoría 1 y 2 |
ES2660207B8 (es) * | 2016-09-21 | 2019-01-10 | Bio Oils Huelva S L | Procedimiento de alta eficacia para la producción de alquil-ésteres de ácidos grasos mediante catálisis ácida y procedimiento de tratamiento |
FR3059328B1 (fr) * | 2016-11-25 | 2018-11-16 | Arkema France | Composition acide pour le traitement d'acides gras |
MY192473A (en) | 2016-11-25 | 2022-08-23 | Arkema France | Acid composition for processing fatty acids |
CN108977281A (zh) * | 2018-07-05 | 2018-12-11 | 浙江恒翔化工有限公司 | 一种利用高酸价劣质油脂制备甲酯的方法 |
US11591545B2 (en) * | 2018-10-10 | 2023-02-28 | Basf Se | Method of producing biodiesel |
EP4132900A1 (fr) * | 2020-04-07 | 2023-02-15 | Basf Se | Production de biodiesel écoénergétique à partir d'huile usagée naturelle ou industrielle |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US22751A (en) * | 1859-01-25 | Ball furniture-caster | ||
US2360844A (en) * | 1941-11-26 | 1944-10-24 | Du Pont | Preparation of detergents |
US2383599A (en) * | 1942-10-17 | 1945-08-28 | Colgate Palmolive Peet Co | Treating fatty glycerides |
US2383601A (en) * | 1943-04-28 | 1945-08-28 | Colgate Palmolive Peet Co | Treating fats and fatty oils |
US2486444A (en) * | 1947-07-08 | 1949-11-01 | Baker Castor Oil Co | Process of producing esters |
JPS6025478B2 (ja) * | 1977-03-17 | 1985-06-18 | 花王株式会社 | 脂肪酸低級アルコ−ルエステルの製造法 |
DE3319590A1 (de) * | 1983-05-30 | 1984-12-06 | Henkel KGaA, 4000 Düsseldorf | Verfahren zur herstellung von fettsaeureestern kurzkettiger aliphatischer alkohole aus freie fettsaeuren enthaltenden fetten und/oder oelen |
-
1984
- 1984-12-08 DE DE19843444893 patent/DE3444893A1/de not_active Withdrawn
-
1985
- 1985-11-25 GB GB08528953A patent/GB2168701B/en not_active Expired
- 1985-11-30 AT AT85115217T patent/ATE61332T1/de not_active IP Right Cessation
- 1985-11-30 EP EP85115217A patent/EP0184740B1/fr not_active Expired - Lifetime
- 1985-11-30 DE DE8585115217T patent/DE3582022D1/de not_active Expired - Fee Related
- 1985-12-04 TR TR85/48891A patent/TR25060A/xx unknown
- 1985-12-06 ES ES549666A patent/ES8606242A1/es not_active Expired
- 1985-12-06 ZA ZA859371A patent/ZA859371B/xx unknown
- 1985-12-06 CA CA000497012A patent/CA1261870A/fr not_active Expired
- 1985-12-06 US US06/806,074 patent/US4652406A/en not_active Expired - Fee Related
- 1985-12-06 BR BR8506119A patent/BR8506119A/pt not_active IP Right Cessation
- 1985-12-09 JP JP60277773A patent/JPH0662502B2/ja not_active Expired - Lifetime
- 1985-12-09 MX MX866A patent/MX162267A/es unknown
-
1987
- 1987-04-02 MY MYPI87000423A patent/MY101291A/en unknown
Also Published As
Publication number | Publication date |
---|---|
ES549666A0 (es) | 1986-04-16 |
GB8528953D0 (en) | 1986-01-02 |
DE3582022D1 (de) | 1991-04-11 |
TR25060A (tr) | 1992-09-22 |
GB2168701A (en) | 1986-06-25 |
DE3444893A1 (de) | 1986-06-12 |
ATE61332T1 (de) | 1991-03-15 |
CA1261870A (fr) | 1989-09-26 |
JPS61140544A (ja) | 1986-06-27 |
MX162267A (es) | 1991-04-19 |
ZA859371B (en) | 1986-07-30 |
EP0184740A3 (en) | 1987-09-09 |
EP0184740A2 (fr) | 1986-06-18 |
ES8606242A1 (es) | 1986-04-16 |
US4652406A (en) | 1987-03-24 |
EP0184740B1 (fr) | 1991-03-06 |
MY101291A (en) | 1991-09-05 |
GB2168701B (en) | 1988-11-30 |
BR8506119A (pt) | 1986-08-26 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
JPH0662502B2 (ja) | 脂肪酸メチルエステルの製法 | |
US4164506A (en) | Process for producing lower alcohol esters of fatty acids | |
US4695411A (en) | Process for manufacturing a composition of fatty acid esters useful as gas oil substitute motor fuel with hydrated ethyl alcohol and the resultant esters composition | |
JPS61168696A (ja) | 遊離脂肪酸の予備エステル化方法 | |
JP4872047B2 (ja) | グリセリンを用いてアルキルエステルを製造する方法 | |
JPS6035099A (ja) | 短鎖脂肪族アルコールの脂肪酸エステルの製法 | |
EA004051B1 (ru) | Способ получения жирнокислотных эфиров одновалентных алкиловых спиртов и его применение | |
CA2615712C (fr) | Procede de production d'alkylesters d'acide carboxylique | |
WO2009007234A1 (fr) | Nouveau procédé de fabrication d'esters à partir d'huiles végétales et/ou de graisses animales à l'aide de catalyseurs hétérogènes, en particulier en présence d'acidité libre et d'eau | |
JPH03200743A (ja) | 脂肪酸低級アルキルモノエステルの製造方法 | |
MX2008003424A (es) | Metodo mejorado para hacer esteres de etilo a partir de grasas naturales. | |
KR102327852B1 (ko) | 지방을 이용한 지방산알킬에스테르의 제조방법 | |
CA2774343A1 (fr) | Procede de conversion en biodiesel d'huiles peu couteuses a teneur elevee en acides gras libres (agl) | |
EP1512738B1 (fr) | Procede relatif a l'elaboration de composition d'ester d'alkyle d'acide gras | |
JP2006508148A (ja) | アルキルエステルの生産方法 | |
US4976892A (en) | Process for the continuous transesterification of fatty acid lower alkyl esters | |
US2383596A (en) | Method of treating fatty glycerides | |
CN105273851B (zh) | 一种制备脂肪酸酯的方法 | |
US20020082434A1 (en) | Process for the production of sterols | |
JP3934630B2 (ja) | 酸性油脂類および劣化油脂類からのバイオディーゼル燃料製造方法 | |
US5773636A (en) | Process for the production of fatty acid lower alkyl esters | |
JP5454996B2 (ja) | 脂肪酸アルキルエステル組成物の製造方法及び油脂類の処理方法 | |
JP2938586B2 (ja) | α−スルホ脂肪酸エステルの製造法 | |
JP2002241787A (ja) | 脂肪酸低級アルキルエステルの製造法 | |
EP4071226A1 (fr) | Processus pour produire des esters d'alkyle d'acides gras |