JPH0535134B2 - - Google Patents
Info
- Publication number
- JPH0535134B2 JPH0535134B2 JP16144385A JP16144385A JPH0535134B2 JP H0535134 B2 JPH0535134 B2 JP H0535134B2 JP 16144385 A JP16144385 A JP 16144385A JP 16144385 A JP16144385 A JP 16144385A JP H0535134 B2 JPH0535134 B2 JP H0535134B2
- Authority
- JP
- Japan
- Prior art keywords
- ether
- reaction
- organic layer
- mol
- dihydroxyalkane
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 18
- 238000004519 manufacturing process Methods 0.000 claims description 13
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 12
- 239000012044 organic layer Substances 0.000 claims description 10
- 239000007789 gas Substances 0.000 claims description 8
- 229910000041 hydrogen chloride Inorganic materials 0.000 claims description 8
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 claims description 8
- 239000007788 liquid Substances 0.000 claims description 8
- 239000010410 layer Substances 0.000 claims description 4
- 150000002170 ethers Chemical class 0.000 claims description 3
- 238000004508 fractional distillation Methods 0.000 claims description 3
- 239000006227 byproduct Substances 0.000 description 7
- KJDRSWPQXHESDQ-UHFFFAOYSA-N 1,4-dichlorobutane Chemical compound ClCCCCCl KJDRSWPQXHESDQ-UHFFFAOYSA-N 0.000 description 6
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- WERYXYBDKMZEQL-UHFFFAOYSA-N butane-1,4-diol Chemical compound OCCCCO WERYXYBDKMZEQL-UHFFFAOYSA-N 0.000 description 3
- 230000000052 comparative effect Effects 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- PVBMXMKIKMJQRK-UHFFFAOYSA-N 1-chloro-4-(4-chlorobutoxy)butane Chemical compound ClCCCCOCCCCCl PVBMXMKIKMJQRK-UHFFFAOYSA-N 0.000 description 2
- YPFDHNVEDLHUCE-UHFFFAOYSA-N propane-1,3-diol Chemical compound OCCCO YPFDHNVEDLHUCE-UHFFFAOYSA-N 0.000 description 2
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 2
- ALQSHHUCVQOPAS-UHFFFAOYSA-N Pentane-1,5-diol Chemical compound OCCCCCO ALQSHHUCVQOPAS-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000000543 intermediate Substances 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP16144385A JPS6222733A (ja) | 1985-07-22 | 1985-07-22 | ω，ω′−ジクロロアルカンの製造法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP16144385A JPS6222733A (ja) | 1985-07-22 | 1985-07-22 | ω，ω′−ジクロロアルカンの製造法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6222733A JPS6222733A (ja) | 1987-01-30 |
| JPH0535134B2 true JPH0535134B2 (en)van) | 1993-05-25 |
Family
ID=15735209
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP16144385A Granted JPS6222733A (ja) | 1985-07-22 | 1985-07-22 | ω，ω′−ジクロロアルカンの製造法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6222733A (en)van) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4214285B2 (ja) | 1999-12-17 | 2009-01-28 | マニー株式会社 | 歯科用根管治療器具及びその製造方法 |
| JP4168194B2 (ja) | 2003-02-26 | 2008-10-22 | マニー株式会社 | 極細角棒の捩じり方法及び捩じり装置 |
-
1985
- 1985-07-22 JP JP16144385A patent/JPS6222733A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6222733A (ja) | 1987-01-30 |
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