JP7352719B2 - 殺菌剤組成物 - Google Patents
殺菌剤組成物 Download PDFInfo
- Publication number
- JP7352719B2 JP7352719B2 JP2022503667A JP2022503667A JP7352719B2 JP 7352719 B2 JP7352719 B2 JP 7352719B2 JP 2022503667 A JP2022503667 A JP 2022503667A JP 2022503667 A JP2022503667 A JP 2022503667A JP 7352719 B2 JP7352719 B2 JP 7352719B2
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- Prior art keywords
- dicarboxylic acid
- acid
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- DQJCHOQLCLEDLL-UHFFFAOYSA-N tricyclazole Chemical compound CC1=CC=CC2=C1N1C=NN=C1S2 DQJCHOQLCLEDLL-UHFFFAOYSA-N 0.000 description 1
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- HSMVPDGQOIQYSR-KGENOOAVSA-N triflumizole Chemical compound C1=CN=CN1C(/COCCC)=N/C1=CC=C(Cl)C=C1C(F)(F)F HSMVPDGQOIQYSR-KGENOOAVSA-N 0.000 description 1
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- JARYYMUOCXVXNK-IMTORBKUSA-N validamycin Chemical compound N([C@H]1C[C@@H]([C@H]([C@H](O)[C@H]1O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)CO)[C@H]1C=C(CO)[C@H](O)[C@H](O)[C@H]1O JARYYMUOCXVXNK-IMTORBKUSA-N 0.000 description 1
- DBXFMOWZRXXBRN-LWKPJOBUSA-N valifenalate Chemical compound CC(C)OC(=O)N[C@@H](C(C)C)C(=O)NC(CC(=O)OC)C1=CC=C(Cl)C=C1 DBXFMOWZRXXBRN-LWKPJOBUSA-N 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 239000010455 vermiculite Substances 0.000 description 1
- 229910052902 vermiculite Inorganic materials 0.000 description 1
- 235000019354 vermiculite Nutrition 0.000 description 1
- BCEHBSKCWLPMDN-MGPLVRAMSA-N voriconazole Chemical compound C1([C@H](C)[C@](O)(CN2N=CN=C2)C=2C(=CC(F)=CC=2)F)=NC=NC=C1F BCEHBSKCWLPMDN-MGPLVRAMSA-N 0.000 description 1
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- 239000004552 water soluble powder Substances 0.000 description 1
- 238000001238 wet grinding Methods 0.000 description 1
- 239000004563 wettable powder Substances 0.000 description 1
- 239000000230 xanthan gum Substances 0.000 description 1
- 229920001285 xanthan gum Polymers 0.000 description 1
- 235000010493 xanthan gum Nutrition 0.000 description 1
- 229940082509 xanthan gum Drugs 0.000 description 1
- 239000010457 zeolite Substances 0.000 description 1
- 239000011787 zinc oxide Substances 0.000 description 1
- AMHNZOICSMBGDH-UHFFFAOYSA-L zineb Chemical compound [Zn+2].[S-]C(=S)NCCNC([S-])=S AMHNZOICSMBGDH-UHFFFAOYSA-L 0.000 description 1
- 229910000166 zirconium phosphate Inorganic materials 0.000 description 1
- LEHFSLREWWMLPU-UHFFFAOYSA-B zirconium(4+);tetraphosphate Chemical compound [Zr+4].[Zr+4].[Zr+4].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O LEHFSLREWWMLPU-UHFFFAOYSA-B 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01G—HORTICULTURE; CULTIVATION OF VEGETABLES, FLOWERS, RICE, FRUIT, VINES, HOPS OR SEAWEED; FORESTRY; WATERING
- A01G13/00—Protecting plants
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01G—HORTICULTURE; CULTIVATION OF VEGETABLES, FLOWERS, RICE, FRUIT, VINES, HOPS OR SEAWEED; FORESTRY; WATERING
- A01G20/00—Cultivation of turf, lawn or the like; Apparatus or methods therefor
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/06—Unsaturated carboxylic acids or thio analogues thereof; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01P—BIOCIDAL, PEST REPELLANT, PEST ATTRACTANT OR PLANT GROWTH REGULATORY ACTIVITY OF CHEMICAL COMPOUNDS OR PREPARATIONS
- A01P3/00—Fungicides
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Environmental Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Zoology (AREA)
- Pest Control & Pesticides (AREA)
- Agronomy & Crop Science (AREA)
- Dentistry (AREA)
- Toxicology (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
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Description
例えば、特許文献1は、チモールおよびカルバクロールから選ばれた1種以上と、フマル酸およびフィチン酸から選ばれた1種以上と、を水に溶解させて成り、前記チモールおよびカルバクロールを合わせた配合量が0.01質量%以上0.04質量%以下であることを特徴とする水性殺菌組成物を開示している。
[2]前記ジカルボン酸以外の殺菌作用を有する物質がベンジルアミノプリンである、[1]に記載の殺菌剤組成物。
[3]前記ジカルボン酸がフマル酸である、[1]または[2]に記載の殺菌剤組成物。
[4][1]~[3]のいずれかひとつに記載の殺菌剤組成物をイネ科植物に施用することを含む、殺菌方法。
[5]ジカルボン酸、およびジカルボン酸以外の殺菌作用を有する物質を、同時にまたは正順もしくは逆順に、イネ科植物に施用することを含む、殺菌方法。
[6]前記イネ科植物がシバである、[4]または[5]に記載の殺菌方法。
[7]さらに添加剤を含有し、前記ジカルボン酸以外の殺菌作用を有する物質がベンジルアミノプリンであり、前記ジカルボン酸がフマル酸であることを特徴とする[1]に記載の殺菌剤組成物。
[8]殺菌剤組成物の総質量100%に対して、前記ジカルボン酸が20質量%~90質量%、前記ジカルボン酸以外の殺菌作用を有する物質が0.01質量%~10質量%、および前記添加剤が0.1質量%~70質量%であことを特徴とする[7]に記載の殺菌剤組成物。
本発明に用いられるジカルボン酸は、カルボキシル基(COOH基)を2つ有する有機化合物であれば特に制限されない。本発明に用いられるジカルボン酸は、カルボキシル基以外の部分を構成する炭素原子の数が6以下であってもよい。
ジカルボン酸の質量は、ジカルボン酸以外の殺菌作用を有する物質の質量に対して、1以上4000以下、好ましくは10以上3000以下、より好ましくは50以上2000以下、さらに好ましくは100以上1000以下である。
フマル酸(Fumaric Acid)は、式(I)で表させる化合物(IUPAC名:(E)-2-butenedioic acid、CAS番号110-17-8)である。
フマル酸は無色結晶であり、ベントグラスに対して、かさ枯病や藻類に高い効果があることが知られている。
フマル酸を含有する農薬組成物の製品としては、アルテリア(登録商標)水和剤(日本曹達株式会社製)などを挙げることができる。
本発明に用いられるジカルボン酸以外の殺菌作用を有する物質は、ジカルボン酸以外の化合物であって、殺菌作用を有するものであれば、特に限定されない。
本発明に用いられるジカルボン酸以外の殺菌作用を有する物質は、農薬の有効成分として用いられるものであってもよい。
(a)RNAポリメラーゼI阻害剤: ベナラキシル(benalaxyl)、ベナラキシル-M(benalaxyl-M)、フララキシル(furalaxyl)、メタラキシル(metalaxyl)、メタラキシル-M(metalaxyl-M)、オキサジキシル(oxadixyl)、クロジラコン(clozylacon)、オフレース(ofurace);
(b)アデノシンデアミナーゼ阻害剤: ブピリメート(bupirimate)、ジメチリモール(dimethirimol)、エチリモール(ethirimol);
(c)DNA/RNA合成阻害剤: ヒメキサゾール(hymexazol)、オクチリノン(octhilinone);
(d)DNAトポイソメラーゼII阻害剤: オキソリン酸(oxolinic acid)。
(a)β-チューブリン重合阻害剤: ベノミル(benomyl)、カルベンダジム(carbendazim)、クロルフェナゾール(chlorfenazole)、フベリダゾール(fuberidazole)、チアベンダゾール(thiabendazole)、チオファネート(thiophanate)、チオファネートメチル(thiophanate-methyl)、ジエトフェンカルブ(diethofencarb)、ゾキサミド(zoxamide)、エタボキサム(ethaboxam);
(b)細胞分裂阻害剤: ペンシクロン(pencycuron);
(c)スペクトリン様タンパク質の非局在化阻害剤: フルオピコリド(fluopicolide)。
(a)複合体I NADH酸化還元酵素阻害剤: ジフルメトリム(diflumetorim)、トルフェンピラド(tolfenpyrad);
(b)複合体IIコハク酸脱水素酵素阻害剤: ベノダニル(benodanil)、フルトラニル(flutolanil)、メプロニル(mepronil)、イソフェタミド(isofetamid)、フルオピラム(fluopyram)、フェンフラム(fenfuram)、フルメシクロックス(furmecyclox)、カルボキシン(carboxin)、オキシカルボキシン(oxycarboxin)、チフルザミド(thifluzamide)、ベンゾビンジフルピル(benzovindiflupyr)、ビキサフェン(bixafen)、フルキサピロキサド(fluxapyroxad)、フラメトピル(furametpyr)、イソピラザム(isopyrazam)、ペンフルフェン(penflufen)、ペンチオピラド(penthiopyrad)、セダキサン(sedaxane)、ボスカリド(boscalid)、ピラジフルミド(pyraziflumid)、ピジフルメトフェン(pydiflumetofen)、イソフルシプラム(isoflucypram)、インピルフルキサム(inpyrfluxam);
(c)複合体IIIユビキノールオキシダーゼQo阻害剤: アゾキシストロビン(azoxystrobin)、クモキシストロビン(coumoxystrobin)、クメトキシストロビン(coumethoxystrobin)、エノキサストロビン(enoxastrobin)、フルフェノキシストロビン(flufenoxystrobin)、ピコキシストロビン(picoxystrobin)、ピラオキシストロビン(pyraoxystrobin)、ピラクロストロビン(pyraclostrobin)、ピラメトストロビン(pyrametostrobin)、トリクロピリカルブ(triclopyricarb)、クレソキシム-メチル(kresoxim-methyl)、トリフロキシストロビン(trifloxystrobin)、ジモキシストロビン(dimoxystrobin)、フェナミンストロビン(fenaminstrobin)、メトミノストロビン(metominostrobin)、オリサストロビン(orysastrobin)、ファモキサドン(famoxadone)、フルオキサストロビン(fluoxastrobin)、フェンアミドン(fenamidone)、ピリベンカルブ(pyribencarb)、マンデストロビン(mandestrobin)、メチルテトラプロール(metyltetraprole);
(d)複合体IIIユビキノール還元酵素Qi阻害剤: シアゾファミド(cyazofamid)、アミスルブロム(amisulbrom)、フェンピコキサミド(fenpicoxamid);
(e)酸化的リン酸化の脱共役剤: ビナパクリル(binapacryl)、メプチルジノカップ(meptyldinocap)、ジノカップ(dinocap)、フルアジナム(fluazinam)、フェリムゾン(ferimzone);
(f)酸化的リン酸化阻害剤(ATP 合成酵素の阻害剤): フェンチンアセテート(fentin acetate)、塩化フェンチン(fentin chloride)、水酸化フェンチン(fentin hydroxide);
(g)ATP生産阻害剤: シルチオファム(silthiofam);
(h)複合体III:シトクローム bc1(ユビキノン還元酵素)のQx(未知)阻害剤: アメトクトラジン(ametoctradin)。
(a)メチオニン生合成阻害剤: アンドプリム(andoprim)、シプロジニル(cyprodinil)、メパニピリム(mepanipyrim)、ピリメタニル(pyrimethanil);
(b)タンパク質合成阻害剤: ブラストサイジン-S(blasticidin-S)、カスガマイシン(kasugamycin)、カスガマイシン塩酸塩(kasugamycin hydrochloride)、ストレプトマイシン(streptomycin)、オキシテトラサイクリン(oxytetracycline)。
(a)シグナル伝達阻害剤: キノキシフェン(quinoxyfen)、プロキナジド(proquinazid);
(b)浸透圧シグナル伝達におけるMAP・ヒスチジンキナーゼ阻害剤: フェンピクロニル(fenpiclonil)、フルジオキソニル(fludioxonil)、クロゾリネート(chlozolinate)、イプロジオン(iprodione)、プロシミドン(procymidone)、ビンクロゾリン(vinclozolin)。
(a)りん脂質生合成、メチルトランスフェラーゼ阻害剤: エジフェンホス(edifenphos)、イプロベンホス(iprobenfos)、ピラゾホス(pyrazophos)、イソプロチオラン(isoprothiolane);
(b)脂質の過酸化剤: ビフェニル(biphenyl)、クロロネブ(chloroneb)、ジクロラン(dichloran)、キントゼン(quintozene)、テクナゼン(tecnazene)、トルクロホスメチル(tolclofos-methyl)、エトリジアゾール(etridiazole);
(c)細胞膜に作用する剤: ヨードカルブ(iodocarb)、プロパモカルブ(propamocarb)、プロパモカルブ塩酸塩(propamocarb-hydrochloride)、プロパモカルブホセチレート(propamocarb-fosetylate)、プロチオカルブ(prothiocarb);
(d)病原菌細胞膜を撹乱する微生物: バチルス ズブチリス菌(bacillus subtilis)、バチルス ズブチリスQST713株(bacillus subtilis strain QST713)、バチルス ズブチリスFZB24株(bacillus subtilis strain FZB24)、バチルス ズブチリスMBI600株(bacillus subtilis strain MBI600)、バチルス ズブチリスD747株(bacillus subtilis strain D747)、バチルス アミロリクエファシエンス(bacillus amyloliquefaciens);
(e)細胞膜を撹乱する剤: ゴセイカユプテ(ティーツリー)の抽出物(melaleuca alternifolia (tea tree) extract)。
(a)ステロール生合成におけるC14位の脱メチル化阻害剤: トリホリン(triforine)、ピリフェノックス(pyrifenox)、ピリソキサゾール(pyrisoxazole)、フェナリモル(fenarimol)、フルルプリミドール(flurprimidol)、ヌアリモル(nuarimol)、イマザリル(imazalil)、イマザリル硫酸塩(imazalil-sulphate)、オキスポコナゾールフマル酸塩(oxpoconazole fumarate)、ペフラゾエート(pefurazoate)、プロクロラズ(prochloraz)、トリフルミゾール(triflumizole)、ビニコナゾール(viniconazole)、アザコナゾール(azaconazole)、ビテルタノール(bitertanol)、ブロムコナゾール(bromuconazole)、シプロコナゾール(cyproconazole)、ジクロブトラゾール(diclobutrazol)、ジフェノコナゾール(difenoconazole)、ジニコナゾール(diniconazole)、ジニコナゾール-M(diniconazole-M)、エポキシコナゾール(epoxiconazole)、エタコナゾール(etaconazole)、フェンブコナゾール(fenbuconazole)、フルキンコナゾール(fluquinconazole)、フルシラゾール(flusilazole)、フルトリアホール(flutriafol)、フルコナゾール(furconazole)、フルコナゾール-シス(furconazole-cis)、ヘキサコナゾール(hexaconazole)、イミベンコナゾール(imibenconazole)、イプコナゾール(ipconazole)、メトコナゾール(metconazole)、ミクロブタニル(myclobutanil)、ペンコナゾール(penconazole)、プロピコナゾール(propiconazole)、フルキンコナゾール(fluquinconazole)、シメコナゾール(simeconazole)、テブコナゾール(tebuconazole)、テトラコナゾール(tetraconazole)、トリアジメホン(triadimefon)、トリアジメノール(triadimenol)、トリチコナゾール(triticonazole)、プロチオコナゾール(prothioconazole)、ボリコナゾール(voriconazole)、メフェントリフルコナゾール(mefentrifluconazole);
(b)ステロール生合成におけるΔ14還元酵素およびΔ8→Δ7-イソメラーゼの阻害剤:
アルジモルフ(aldimorph)、ドデモルフ(dodemorph)、ドデモルフ酢酸塩(dodemorph acetate)、フェンプロピモルフ(fenpropimorph)、トリデモルフ(tridemorph)、フェンプロピジン(fenpropidin)、ピペラリン(piperalin)、スピロキサミン(spiroxamine);
(c)ステロール生合成系のC4位脱メチル化における3-ケト還元酵素阻害剤: フェンヘキサミド(fenhexamid)、フェンピラザミン(fenpyrazamine);
(d)ステロール生合成系のスクワレンエポキシダーゼ阻害剤: ピリブチカルブ(pyributicarb)、ナフチフィン(naftifine)、テルビナフィン(terbinafine)。
(a)トレハラーゼ阻害剤: バリダマイシン(validamycin);
(b)キチン合成酵素阻害剤: ポリオキシン(polyoxins)、ポリオクソリム(polyoxorim);
(c)セルロース合成酵素阻害剤: ジメトモルフ(dimethomorph)、フルモルフ(flumorph)、ピリモルフ(pyrimorph)、ベンチアバリカルブイソプロピル(benthiavalicarb-isopropyl)、イプロバリカルブ(iprovalicarb)、バリフェナレート(valifenalate)、マンジプロパミド(mandipropamid)。
(a)メラニン生合成の還元酵素阻害剤: フサライド(fthalide)、ピロキロン(pyroquilon)、トリシクラゾール(tricyclazole);
(b)メラニン生合成の脱水酵素阻害剤: カルプロパミド(carpropamid)、ジクロシメット(diclocymet)、フェノキサニル(fenoxanil);
(c)メラニン生合成のポリケタイド合成阻害剤:トルプロカルブ(tolprocarb)。
(a)サリチル酸合成経路に作用する剤: アシベンゾラル-S-メチル(acibenzolar-S-methyl);
(b)その他: プロベナゾール(probenazole)、チアジニル(tiadinil)、イソチアニル(isotianil)、ジクロベンチアゾクス(dichlobentiazox)、ラミナリン(laminarin)、オオイタドリ抽出液(reynoutria sachalinensis extract)。
ベンジルアミノプリンは、式(II)で表させる化合物(6-ベンジルアミノプリン、ベンジルアデニン、またはBAP(CAS番号1214-39-7))である。
ベンジルアミノプリンの原体は、白色粉末として、通常、提供される。
ベンジルアミノプリンを含有する製品としては、ビーエー(登録商標)液剤(クミアイ化学工業株式会社製)、ドラード(登録商標)液剤(株式会社理研グリーン社製)、プレリュード(登録商標)液剤(アグロ カネショウ株式会社製)などを挙げることができる。
本発明の殺菌剤組成物の総質量100%に対して、ジカルボン酸、ジカルボン酸以外の殺菌作用を有する物質、および添付剤の質量は、
ジカルボン酸 20質量%~90質量%
ジカルボン酸以外の殺菌作用を有する物質 0.03質量%~10質量%
添加剤 0.1質量%~70質量%
であり、さらに好ましくは、
ジカルボン酸 50質量%~85質量%
ジカルボン酸以外の殺菌作用を有する物質 0.05質量%~ 5質量%
添加剤 10質量%~45質量%
である。さらに好ましくは、
ジカルボン酸 60質量%~80質量%
ジカルボン酸以外の殺菌作用を有する物質 0.1質量%~ 1質量%
添加剤 19質量%~39質量%
である。
本発明の殺菌剤組成物を水で希釈して使用することができる。その場合の質量は上記質量に水で希釈した倍率で除した値になる。
非イオン性界面活性剤としては、ソルビタン脂肪酸エステル(C12~18)、POEソルビタン脂肪酸エステル(C12~18)、ショ糖脂肪酸エステルなどの糖エステル型界面活性剤;POE脂肪酸エステル(C12~18)、POE樹脂酸エステル、POE脂肪酸ジエステル(C12~18)などの脂肪酸エステル型界面活性剤;POEアルキルエーテル(C12~18)等のアルコール型界面活性剤;POEアルキル(C8~12)フェニルエーテル、POEジアルキル(C8~12)フェニルエーテル、POEアルキル(C8~12)フェニルエーテルホルマリン縮合物などのアルキルフェノール型界面活性剤;ポリオキシエチレン・ポリオキシプロピレンブロックポリマー;アルキル(C12~18)ポリオキシエチレン・ポリオキシプロピレンブロックポリマーエーテルなどのポリオキシエチレン・ポリオキシプロピレンブロックポリマー型界面活性剤;POEアルキルアミン(C12~18)、POE脂肪酸アミド(C12~18)などのアルキルアミン型界面活性剤;POE脂肪酸ビスフェニルエーテルなどのビスフェノール型界面活性剤;POAベンジルフェニル(又はフェニルフェニル)エーテル、POAスチリルフェニル(又はフェニルフェニル)エーテルなどの多芳香環型界面活性剤;POEエーテル及びエステル型シリコン及びフッ素系界面活性剤などのシリコン系、フッ素系界面活性剤;POEヒマシ油、POE硬化ヒマシ油などの植物油型界面活性剤;等を挙げることができる。
本発明の殺菌剤組成物は、上記の成分以外に、他の成分をさらに含有していてもよい。他の成分としては、殺虫剤、殺ダニ剤、殺線虫剤、殺土壌害虫剤、駆虫剤、除草剤、植物成長調整剤、肥料などの非殺菌性成分を挙げることができる。混用の比率は、特に限定するものではなく、他の成分が適切な濃度になるように混合すれば良い。例えば、本発明の殺菌剤組成物と、殺虫剤、殺ダニ剤または成長調整剤との質量比は、好ましくは1/100~100/1、より好ましくは、1/10~10/1である。
液体製剤においては、ケロシン、キシレンおよびソルベントナフサなどの石油留分、シクロヘキサン、シクロヘキサノン、ジメチルホルムアミド、ジメチルスルホキシド、アルコール、アセトン、トリクロルエチレン、メチルイソブチルケトン、鉱物油、植物油、水などの溶剤を用いることができる。
本発明の殺菌剤組成物 40部
珪藻土 53部
高級アルコール硫酸エステル 4部、および
アルキルナフタレンスルホン酸塩 3部
を均一に混合して微細に粉砕して、有効成分40%の水和剤を得る。
本発明の殺菌剤組成物 30部
キシレン 33部
ジメチルホルムアミド 30部、および
ポリオキシエチレンアルキルアリルエーテル 7部
を混合溶解して、有効成分30%の乳剤を得る。
本発明の殺菌剤組成物 5部
タルク 40部
クレー 38部
ベントナイト 10部、および
アルキル硫酸ソーダ 7部
を均一に混合して微細に粉砕後、直径0.5~1.0mmの粒状に造粒して有効成分5%の粒剤を得る。
本発明の殺菌剤組成物 5部
クレー 73部
ベントナイト 20部
ジオクチルスルホサクシネートナトリウム塩 1部、および
リン酸カリウム 1部
をよく粉砕混合し、水を加えてよく練り合せた後、造粒乾燥して有効成分5%の粒剤を得る。
本発明の殺菌剤組成物 10部
ポリオキシエチレンアルキルアリルエーテル 4部
ポリカルボン酸ナトリウム塩 2部
グリセリン 10部
キサンタンガム 0.2部、および
水 73.8部
を混合し、粒度が3ミクロン以下になるまで湿式粉砕し、有効成分10%の懸濁剤を得る。
逐次施用においては、ジカルボン酸を含有する製剤とジカルボン酸以外の殺菌作用を有する物質を含有する製剤と、必要に応じて他の成分を含有する製剤とを所定割合で、順不同で、植物、土壌または水耕地に、散布、噴霧、灌注などする。逐次施用におけるジカルボン酸を含有する製剤とジカルボン酸以外の殺菌作用を有する物質を含有する製剤との施用間隔は、特に制限されないが、前段の成分が植物、土壌または水耕地に残っている間に後段の成分を施用することが好ましい。
本発明の殺菌剤組成物が対象としうる作物としては、特に限定されないが、好ましくはイネ科植物などが挙げられる。
イネ科(Gramineae)の植物として、例えば、エンバク(Avena sativa)、ハトムギ(Coix lacryma-jobi var. ma-yuen)、オーチャードグラス(Dactylis glomerata)、オオムギ(Hordeum vulgare)、イネ(Oryza sativa)、チモシー(Phleum pratense)、サトウキビ(Saccharum officinarum)、ライムギ(Secale cereale)、アワ(Setaria italica)、パンコムギ(Triticum aestivum)、トウモロコシ(Zea mays)、シバ(Zoysia spp.)を例示することができる。
さらにシバとして、ノシバ、コウライシバ、ヒメコウライシバ、バミューダグラス類、ティフトン類、ウィーピングラブグラス、ベントグラス類、ブルーグラス類、フェスク類、ライグラス類等が知られている。
本発明の殺菌剤組成物はこれら植物類の各部位、例えば、葉、茎、柄、花、蕾、果実、種子、スプラウト、根、塊茎、塊根、苗条、挿し木などに施用することができる。また、これら植物類の改良品種・変種、栽培品種、さらには突然変異体、ハイブリッド体、遺伝子組み換え体(GMO)を対象として処理することもできる。
以下、実施例を挙げて本発明をさらに詳細に説明する。但し、本発明はこれらに限定されるものではない。
ジカルボン酸組成物:アルテリア水和剤(フマル酸 80%含有、日本曹達株式会社製)
ジカルボン酸以外の殺菌剤組成物:ビーエー液剤(ベンジルアミノプリン 3%含有、クミアイ化学工業株式会社製)
比較例1
プラスチックポット(縦横長さ7cm、高さ3cm)で栽培した実生のベントグラス(品種:ペンクロス)にかさ枯病菌(Pseudomonas syringe pv.atropurpurea)の懸濁液を刈込接種しビニール袋をかけた。それを温室内(平均気温20度)で2日間、静置した。次に、水道水200mlをベントグラスの上部から散布した。散布後7日目にベントグラスの葉の先端から2mm以上の病斑が認められるものの数を計測した。この実験を2回繰り返し、その平均値(以下、発病個体数という。)を算出した。発病個体数は35であった。
プラスチックポット(縦横長さ7cm、高さ3cm)で栽培した実生のベントグラス(品種:ペンクロス)にかさ枯病菌(Pseudomonas syringe pv.atropurpurea)の懸濁液を刈込接種しビニール袋をかけた。それを温室内(平均気温20度)で2日間、静置した。次に、水道水200mlにジカルボン酸組成物2g、ジカルボン酸以外の殺菌剤組成物0.2ml(0.22g)を混合して、その混合液をベントグラスの上部から散布した。散布後7日目にベントグラスの葉の先端から2mm以上の病斑が認められるものの数を計測した。この実験を2回繰り返し、その平均値(以下、病斑個体数という。)を算出した。病斑個体数は10、防除価は71.4%であった。
防除価(%)=100×(1-病斑個体数/発病個体数)
ジカルボン酸組成物の量を0gにした以外は実施例1と同じ方法で病斑個体数を算出した。病斑個体数は20、防除価は42.9%であった。
ジカルボン酸以外の殺菌剤組成物の量を0mlにした以外は実施例1と同じ方法で病斑個体数を算出した。病斑個体数は20、防除価は42.9%であった。
ただし、Eは、第一成分と第二成分との併用における防除価の期待値、Mは、第一成分単独使用における防除価の実測値、Nは、第二成分単独使用における防除価の実測値である。
[比較例4]
かさ枯病菌を褐条病菌(Acidovorax avenae subsp. avenae)に変えた以外は、比較例1と同じ方法で発病個体数を算出した。発病個体数は28であった。
比較例2、比較例3および実施例1において、かさ枯病菌を褐条病菌(Acidovorax avenae subsp. avenae)に変えた以外は、比較例2、比較例3および実施例1と同じ方法で病斑個体数をそれぞれ算出した。比較例5、比較例6および実施例2における病斑個体数は、それぞれ、14、18および5であった。
比較例5、比較例6および実施例2における防除価の実測値は、それぞれ、50.0%、35.7%および82.1%であった。
比較例5および比較例6における防除価の実測値からコルビーの式にて算出される実施例2における防除価の期待値は、67.9%である。防除価の実測値が防除価の期待値より高いので、ジカルボン酸組成物とジカルボン酸以外の殺菌剤組成物との併用によって褐条病菌に対する殺菌性に相乗効果があったことがわかる。
Claims (6)
- ジカルボン酸と、ジカルボン酸以外の殺菌作用を有する物質とを含有し、且つ
ジカルボン酸の質量が、ジカルボン酸以外の殺菌作用を有する物質の質量に対して、1以上4000以下であり、
前記ジカルボン酸以外の殺菌作用を有する物質がベンジルアミノプリンであり、
前記ジカルボン酸がフマル酸である、殺菌剤組成物。 - 請求項1に記載の殺菌剤組成物をイネ科植物に施用することを含む、殺菌方法。
- ジカルボン酸、およびジカルボン酸以外の殺菌作用を有する物質を、同時にまたは正順もしくは逆順に、イネ科植物に施用することを含み、
前記ジカルボン酸以外の殺菌作用を有する物質がベンジルアミノプリンであり、
前記ジカルボン酸がフマル酸である、殺菌方法。 - 前記イネ科植物がシバである、請求項2または3に記載の殺菌方法。
- さらに添加剤を含有することを特徴とする請求項1に記載の殺菌剤組成物。
- 殺菌剤組成物の総質量100%に対して、前記ジカルボン酸が20質量%~90質量%、前記ジカルボン酸以外の殺菌作用を有する物質が0.01質量%~10質量%、および前記添加剤が0.1質量%~70質量%であことを特徴とする請求項5に記載の殺菌剤組成物。
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