JP7090158B2 - Ａｅｉ構造モレキュラーシーブの製造方法 - Google Patents

Ａｅｉ構造モレキュラーシーブの製造方法 Download PDF

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JP7090158B2
JP7090158B2 JP2020529787A JP2020529787A JP7090158B2 JP 7090158 B2 JP7090158 B2 JP 7090158B2 JP 2020529787 A JP2020529787 A JP 2020529787A JP 2020529787 A JP2020529787 A JP 2020529787A JP 7090158 B2 JP7090158 B2 JP 7090158B2
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molecular sieve
aei
crystallization
zeolite
electrodialysis
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JP2020529964A (ja
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進 李
志光 王
炳春 王
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中触媒新材料股▲ふん▼有限公司
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/34—Irradiation by, or application of, electric, magnetic or wave energy, e.g. ultrasonic waves ; Ionic sputtering; Flame or plasma spraying; Particle radiation
    • B01J37/341—Irradiation by, or application of, electric, magnetic or wave energy, e.g. ultrasonic waves ; Ionic sputtering; Flame or plasma spraying; Particle radiation making use of electric or magnetic fields, wave energy or particle radiation
    • B01J37/342—Irradiation by, or application of, electric, magnetic or wave energy, e.g. ultrasonic waves ; Ionic sputtering; Flame or plasma spraying; Particle radiation making use of electric or magnetic fields, wave energy or particle radiation of electric, magnetic or electromagnetic fields, e.g. for magnetic separation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/46—Removing components of defined structure
    • B01D53/54—Nitrogen compounds
    • B01D53/56—Nitrogen oxides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/92—Chemical or biological purification of waste gases of engine exhaust gases
    • B01D53/94—Chemical or biological purification of waste gases of engine exhaust gases by catalytic processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/92—Chemical or biological purification of waste gases of engine exhaust gases
    • B01D53/94—Chemical or biological purification of waste gases of engine exhaust gases by catalytic processes
    • B01D53/9404—Removing only nitrogen compounds
    • B01D53/9409—Nitrogen oxides
    • B01D53/9413—Processes characterised by a specific catalyst
    • B01D53/9418—Processes characterised by a specific catalyst for removing nitrogen oxides by selective catalytic reduction [SCR] using a reducing agent in a lean exhaust gas
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/20—Sulfiding
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/34—Irradiation by, or application of, electric, magnetic or wave energy, e.g. ultrasonic waves ; Ionic sputtering; Flame or plasma spraying; Particle radiation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/34—Irradiation by, or application of, electric, magnetic or wave energy, e.g. ultrasonic waves ; Ionic sputtering; Flame or plasma spraying; Particle radiation
    • B01J37/348—Electrochemical processes, e.g. electrochemical deposition or anodisation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/04—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof using at least one organic template directing agent, e.g. an ionic quaternary ammonium compound or an aminated compound
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/03—Particle morphology depicted by an image obtained by SEM

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Biomedical Technology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Environmental & Geological Engineering (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Toxicology (AREA)
  • Combustion & Propulsion (AREA)
  • Inorganic Chemistry (AREA)
  • Plasma & Fusion (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Electromagnetism (AREA)
  • Optics & Photonics (AREA)
  • Electrochemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Catalysts (AREA)
  • Exhaust Gas Treatment By Means Of Catalyst (AREA)
JP2020529787A 2017-08-10 2017-10-13 Ａｅｉ構造モレキュラーシーブの製造方法 Active JP7090158B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
CN201710681346.6A CN109384246B (zh) 2017-08-10 2017-08-10 一种aei结构分子筛及其制备方法和应用
CN201710681346.6 2017-08-10
PCT/CN2017/106026 WO2019028999A1 (zh) 2017-08-10 2017-10-13 一种aei结构分子筛及其制备方法和应用

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JP7090158B2 true JP7090158B2 (ja) 2022-06-23

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KR (1) KR102370849B1 (zh)
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Families Citing this family (11)

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Publication number Priority date Publication date Assignee Title
CN112239214B (zh) * 2019-07-17 2022-07-08 中国石油化工股份有限公司 硅锗酸盐及其制备方法
CN110592610B (zh) * 2019-09-29 2021-02-05 肯特催化材料股份有限公司 一种季铵盐模板剂的制备方法和应用
CN111250152B (zh) * 2020-03-31 2021-05-28 中国科学院过程工程研究所 一种Ni@ZSM-5双功能催化剂的封装方法
CN112010322B (zh) * 2020-08-20 2022-02-15 华中科技大学 一种分子筛的制备方法及其应用和废水的利用方法
CN112221463B (zh) * 2020-09-30 2022-04-26 中触媒新材料股份有限公司 一种高效连续分子筛吸附剂后处理装置及使用方法
CN114477209B (zh) * 2020-10-23 2023-10-13 中国石油化工股份有限公司 一种硅铝分子筛及其制备方法和应用
CN112517050B (zh) * 2021-01-06 2021-11-30 南京大学 一种包覆活性双金属氧化物的中空囊泡型介孔分子筛催化剂及其制备方法和应用
KR102484715B1 (ko) 2021-04-06 2023-01-03 손원일 휴대용 온수 보일러
CN116443889A (zh) * 2021-12-30 2023-07-18 中国石油化工股份有限公司 分子筛合成废液中模板剂的回收方法和分子筛的制备方法
CN114573003B (zh) * 2022-04-25 2023-03-31 淮安六元环新材料有限公司 一种晶种法合成ssz-39分子筛的方法
CN115710717A (zh) * 2022-11-25 2023-02-24 华北电力大学 一种微等离子体合成Na-A沸石分子筛的方法

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20070100188A1 (en) 2005-11-02 2007-05-03 Mertens Machteld M Metalloaluminophosphate molecular sieves, their synthesis and use
CN101076401A (zh) 2004-04-05 2007-11-21 埃克森美孚化学专利公司 结晶共生材料及其合成和在含氧化合物－烯烃转化中的用途
CN104030499A (zh) 2014-05-22 2014-09-10 浙江工业大学 一种特种分子筛合成母液的综合处理方法
JP2016538217A (ja) 2013-10-31 2016-12-08 ジョンソン、マッセイ、パブリック、リミテッド、カンパニーＪｏｈｎｓｏｎ Ｍａｔｔｈｅｙ Ｐｕｂｌｉｃ Ｌｉｍｉｔｅｄ Ｃｏｍｐａｎｙ Ａｅｉゼオライトの合成

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100525208B1 (ko) * 2003-08-18 2005-11-04 한국화학연구원 나노 세공을 갖는 ｖｓｂ-5 분자체의 제조방법
CN103771434B (zh) * 2012-10-25 2015-10-28 中国石油化工股份有限公司 一种分子筛离子交换方法
CN103771436B (zh) * 2012-10-25 2015-07-29 中国石油化工股份有限公司 一种分子筛离子交换方法及其应用
KR101560091B1 (ko) * 2014-05-16 2015-10-13 이원근 전기투석시스템을 이용한 h-타입 제올라이트의 제조방법
JP6572751B2 (ja) 2014-11-21 2019-09-11 三菱ケミカル株式会社 Ａｅｉ型ゼオライト及びその製造方法と用途
ES2586775B1 (es) 2015-04-16 2017-08-14 Consejo Superior De Investigaciones Científicas (Csic) Método de preparación de la estructura zeolítica aei en su forma silicoaluminato con grandes rendimientos, y su aplicación en catálisis
CN105540743A (zh) * 2015-10-30 2016-05-04 中国石油化工股份有限公司 一种废水的处理方法和一种分子筛的制备方法以及一种分子筛制备系统
KR20180083368A (ko) 2015-11-11 2018-07-20 존슨 맛쎄이 퍼블릭 리미티드 컴파니 알루미노실리케이트 aei 제올라이트 제법
CN106745057B (zh) * 2017-03-10 2018-11-13 中触媒新材料股份有限公司 一种无粘结剂的aei/mfi共晶硅铝分子筛及合成方法和应用

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101076401A (zh) 2004-04-05 2007-11-21 埃克森美孚化学专利公司 结晶共生材料及其合成和在含氧化合物－烯烃转化中的用途
US20070100188A1 (en) 2005-11-02 2007-05-03 Mertens Machteld M Metalloaluminophosphate molecular sieves, their synthesis and use
JP2016538217A (ja) 2013-10-31 2016-12-08 ジョンソン、マッセイ、パブリック、リミテッド、カンパニーＪｏｈｎｓｏｎ Ｍａｔｔｈｅｙ Ｐｕｂｌｉｃ Ｌｉｍｉｔｅｄ Ｃｏｍｐａｎｙ Ａｅｉゼオライトの合成
CN104030499A (zh) 2014-05-22 2014-09-10 浙江工业大学 一种特种分子筛合成母液的综合处理方法

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WO2019028999A1 (zh) 2019-02-14
KR102370849B1 (ko) 2022-03-04
JP2020529964A (ja) 2020-10-15
KR20200039727A (ko) 2020-04-16
CN109384246A (zh) 2019-02-26

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