JP7008634B2 - アルキルアミンを用いたa/m/x材料の製造方法 - Google Patents

アルキルアミンを用いたa/m/x材料の製造方法 Download PDF

Info

Publication number
JP7008634B2
JP7008634B2 JP2018546829A JP2018546829A JP7008634B2 JP 7008634 B2 JP7008634 B2 JP 7008634B2 JP 2018546829 A JP2018546829 A JP 2018546829A JP 2018546829 A JP2018546829 A JP 2018546829A JP 7008634 B2 JP7008634 B2 JP 7008634B2
Authority
JP
Japan
Prior art keywords
compound
cation
precursor
formula
layer
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
JP2018546829A
Other languages
English (en)
Japanese (ja)
Other versions
JP2019516232A5 (enExample
JP2019516232A (ja
Inventor
ジェームズ スナイス,ヘンリー
ナヤク,パビトラ
ウェンジャー,バーナード
ノエル,ニキータ
ハビスレウティンガー,セベリン
ムーア,デビッド
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Oxford University Innovation Ltd
Original Assignee
Oxford University Innovation Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=55859227&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=JP7008634(B2) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Oxford University Innovation Ltd filed Critical Oxford University Innovation Ltd
Publication of JP2019516232A publication Critical patent/JP2019516232A/ja
Publication of JP2019516232A5 publication Critical patent/JP2019516232A5/ja
Application granted granted Critical
Publication of JP7008634B2 publication Critical patent/JP7008634B2/ja
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • H—ELECTRICITY
    • H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
    • H10K85/00—Organic materials used in the body or electrodes of devices covered by this subclass
    • H10K85/60—Organic compounds having low molecular weight
    • H10K85/649—Aromatic compounds comprising a hetero atom
    • H10K85/656—Aromatic compounds comprising a hetero atom comprising two or more different heteroatoms per ring
    • H10K85/6565—Oxadiazole compounds
    • H—ELECTRICITY
    • H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10P—GENERIC PROCESSES OR APPARATUS FOR THE MANUFACTURE OR TREATMENT OF DEVICES COVERED BY CLASS H10
    • H10P14/00—Formation of materials, e.g. in the shape of layers or pillars
    • H10P14/20—Formation of materials, e.g. in the shape of layers or pillars of semiconductor materials
    • H10P14/34—Deposited materials, e.g. layers
    • H10P14/3402—Deposited materials, e.g. layers characterised by the chemical composition
    • H—ELECTRICITY
    • H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
    • H10K30/00—Organic devices sensitive to infrared radiation, light, electromagnetic radiation of shorter wavelength or corpuscular radiation
    • H—ELECTRICITY
    • H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
    • H10K30/00—Organic devices sensitive to infrared radiation, light, electromagnetic radiation of shorter wavelength or corpuscular radiation
    • H10K30/10—Organic devices sensitive to infrared radiation, light, electromagnetic radiation of shorter wavelength or corpuscular radiation comprising heterojunctions between organic semiconductors and inorganic semiconductors
    • H10K30/15—Sensitised wide-bandgap semiconductor devices, e.g. dye-sensitised TiO2
    • H10K30/151—Sensitised wide-bandgap semiconductor devices, e.g. dye-sensitised TiO2 the wide bandgap semiconductor comprising titanium oxide, e.g. TiO2
    • H—ELECTRICITY
    • H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
    • H10K71/00—Manufacture or treatment specially adapted for the organic devices covered by this subclass
    • H10K71/10—Deposition of organic active material
    • H10K71/12—Deposition of organic active material using liquid deposition, e.g. spin coating
    • H10K71/15—Deposition of organic active material using liquid deposition, e.g. spin coating characterised by the solvent used
    • H—ELECTRICITY
    • H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
    • H10K85/00—Organic materials used in the body or electrodes of devices covered by this subclass
    • H10K85/50—Organic perovskites; Hybrid organic-inorganic perovskites [HOIP], e.g. CH3NH3PbI3
    • H—ELECTRICITY
    • H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10P—GENERIC PROCESSES OR APPARATUS FOR THE MANUFACTURE OR TREATMENT OF DEVICES COVERED BY CLASS H10
    • H10P14/00—Formation of materials, e.g. in the shape of layers or pillars
    • H10P14/20—Formation of materials, e.g. in the shape of layers or pillars of semiconductor materials
    • H10P14/26—Formation of materials, e.g. in the shape of layers or pillars of semiconductor materials using liquid deposition
    • H10P14/265—Formation of materials, e.g. in the shape of layers or pillars of semiconductor materials using liquid deposition using solutions
    • H—ELECTRICITY
    • H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
    • H10K30/00—Organic devices sensitive to infrared radiation, light, electromagnetic radiation of shorter wavelength or corpuscular radiation
    • H10K30/10—Organic devices sensitive to infrared radiation, light, electromagnetic radiation of shorter wavelength or corpuscular radiation comprising heterojunctions between organic semiconductors and inorganic semiconductors
    • H—ELECTRICITY
    • H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
    • H10K30/00—Organic devices sensitive to infrared radiation, light, electromagnetic radiation of shorter wavelength or corpuscular radiation
    • H10K30/50—Photovoltaic [PV] devices
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E10/00—Energy generation through renewable energy sources
    • Y02E10/50—Photovoltaic [PV] energy
    • Y02E10/549—Organic PV cells
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
    • Y02P70/50—Manufacturing or production processes characterised by the final manufactured product

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Electromagnetism (AREA)
  • Inorganic Chemistry (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • Manufacturing & Machinery (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Photovoltaic Devices (AREA)
JP2018546829A 2016-03-09 2017-03-08 アルキルアミンを用いたa/m/x材料の製造方法 Active JP7008634B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
GB1604050.3 2016-03-09
GBGB1604050.3A GB201604050D0 (en) 2016-03-09 2016-03-09 A/M/X material production process with alkylamine
PCT/GB2017/050623 WO2017153752A1 (en) 2016-03-09 2017-03-08 A/m/x material production process with alkylamine

Publications (3)

Publication Number Publication Date
JP2019516232A JP2019516232A (ja) 2019-06-13
JP2019516232A5 JP2019516232A5 (enExample) 2020-04-16
JP7008634B2 true JP7008634B2 (ja) 2022-02-10

Family

ID=55859227

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2018546829A Active JP7008634B2 (ja) 2016-03-09 2017-03-08 アルキルアミンを用いたa/m/x材料の製造方法

Country Status (9)

Country Link
US (1) US10797255B2 (enExample)
EP (1) EP3427290B1 (enExample)
JP (1) JP7008634B2 (enExample)
KR (1) KR102363283B1 (enExample)
CN (1) CN108780759B (enExample)
ES (1) ES2884327T3 (enExample)
GB (1) GB201604050D0 (enExample)
PL (1) PL3427290T3 (enExample)
WO (1) WO2017153752A1 (enExample)

Families Citing this family (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US11174276B2 (en) * 2017-09-06 2021-11-16 Alliance For Sustainable Energy, Llc Organic-inorganic perovskite materials and methods of making the same
JP7304517B2 (ja) * 2018-07-10 2023-07-07 パナソニックIpマネジメント株式会社 太陽電池
GB201811538D0 (en) * 2018-07-13 2018-08-29 Univ Oxford Innovation Ltd Stabilised a/m/x materials
KR102800886B1 (ko) * 2018-08-23 2025-04-29 에이에스엠 아이피 홀딩 비.브이. 기판 처리 장치 및 방법
GB201817166D0 (en) * 2018-10-22 2018-12-05 Univ Oxford Innovation Ltd Multi-junction device production process
GB201817167D0 (en) * 2018-10-22 2018-12-05 Univ Oxford Innovation Ltd Process for producing a layer with mixed solvent system
US11631582B2 (en) 2018-11-21 2023-04-18 Cubicpv Inc. Enhanced perovskite materials for photovoltaic devices
US11339058B2 (en) * 2018-12-14 2022-05-24 Alliance For Sustainable Energy, Llc Manufacturing of perovskite films
GB201820427D0 (en) 2018-12-14 2019-01-30 Univ Oxford Innovation Ltd Device interlayer
CN110048001A (zh) * 2019-04-01 2019-07-23 桂林理工大学 一种通过卤素替换工程来调节铋基有机-无机杂化材料形貌、带隙和稳定性的方法
JP7542224B2 (ja) * 2019-05-29 2024-08-30 パナソニックIpマネジメント株式会社 光電変換膜およびそれを用いた太陽電池、ならびに光電変換膜の製造方法
KR102958206B1 (ko) * 2019-05-30 2026-04-29 에너지 머티리얼즈 코퍼레이션 고속으로 페로브스카이트 층을 제조하는 방법
CN110862232A (zh) * 2019-11-12 2020-03-06 宁波大学 一种硫基微晶玻璃材料及其制备方法
CN113929641B (zh) * 2020-07-14 2025-05-06 西安固能新材料科技有限公司 系列乙二铵三元晶态化合物及其制备方法以及作为含能材料的用途
WO2021207344A1 (en) * 2020-04-08 2021-10-14 The Trustees Of Princeton University Thermal management for perovskite electronic devices
US20210388009A1 (en) * 2020-06-10 2021-12-16 Nanyang Technological University Organic metal-halide perovskite precursor, process for production and use thereof
CN111883664B (zh) * 2020-06-30 2022-09-23 西安理工大学 一种双注入倍增型有机光电探测器及其制备方法
US11846886B2 (en) 2020-11-23 2023-12-19 International Business Machines Corporation Photoacid generator
WO2022217238A1 (en) * 2021-04-06 2022-10-13 Alliance For Sustainable Energy, Llc Methods for purifying perovskite precursors and improved perovskites manufactured therefrom
KR102573246B1 (ko) * 2021-04-20 2023-09-01 한국과학기술원 할라이드 페로브스카이트 박막의 저온 용액 공정 제조를 위한 용매 및 이를 이용한 페로브스카이트 박막 제조 방법
WO2023047116A1 (en) 2021-09-22 2023-03-30 Oxford University Innovation Limited Perovskite production process
KR102761911B1 (ko) * 2022-09-21 2025-02-05 서울대학교산학협력단 탠덤 태양전지의 제조방법
CN117205950A (zh) * 2023-09-19 2023-12-12 浙江师范大学 一种水稳定型卤化物钙钛矿Cs2Pt0.25Sn0.75Br6光催化剂的制备及应用
CN122349789A (zh) * 2023-12-22 2026-07-07 株式会社钟化 钙钛矿前体液、太阳能电池制造方法以及太阳能电池
CN118382342B (zh) * 2024-06-19 2024-10-01 天合光能股份有限公司 钙钛矿吸光层的制备方法、钙钛矿太阳能电池、光伏组件和光伏系统

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2014056903A (ja) 2012-09-12 2014-03-27 Peccell Technologies Inc ペロブスカイト化合物を用いた光電変換素子およびその製造方法
JP2015535390A (ja) 2012-09-18 2015-12-10 イシス イノベイション リミテッド 光電子素子
CN105647530A (zh) 2016-02-01 2016-06-08 南京理工大学 一种金属卤化物无机钙钛矿量子点的制备方法

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5871579A (en) * 1997-09-25 1999-02-16 International Business Machines Corporation Two-step dipping technique for the preparation of organic-inorganic perovskite thin films
WO2013126385A1 (en) 2012-02-21 2013-08-29 Northwestern University Photoluminescent compounds
JP5992389B2 (ja) * 2012-11-16 2016-09-14 富士フイルム株式会社 光電変換素子、色素増感太陽電池、金属錯体色素、色素溶液、色素吸着電極および色素増感太陽電池の製造方法
JP6337561B2 (ja) * 2014-03-27 2018-06-06 株式会社リコー ペロブスカイト型太陽電池
GB201414110D0 (en) * 2014-08-08 2014-09-24 Isis Innovation Thin film production
WO2016105537A1 (en) 2014-12-23 2016-06-30 Los Alamos National Security, Llc Crystalline perovskite thin films and devices that include the films
CN104810480A (zh) * 2015-04-22 2015-07-29 上海纳米技术及应用国家工程研究中心有限公司 一种用于钙钛矿电池的二氧化钛薄层的制备方法
CN104934503B (zh) * 2015-06-12 2017-03-08 辽宁工业大学 一种钙钛矿太阳能电池光吸收层材料甲基胺溴化铅的制备方法
CN105331362B (zh) 2015-12-07 2017-08-04 南京理工大学 一种室温大产率无机卤素钙钛矿荧光量子点的制备方法

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2014056903A (ja) 2012-09-12 2014-03-27 Peccell Technologies Inc ペロブスカイト化合物を用いた光電変換素子およびその製造方法
JP2015535390A (ja) 2012-09-18 2015-12-10 イシス イノベイション リミテッド 光電子素子
CN105647530A (zh) 2016-02-01 2016-06-08 南京理工大学 一种金属卤化物无机钙钛矿量子点的制备方法

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
AKKERMAN, Quinten A. et al.,Solution Synthesis Approach to Colloidal Cesium Lead Halide Perovskite Nanoplatelets with Monolayer-Level Thickness Control,Journal of the American Chemical Society,2016年01月02日,Vol. 138, No. 3,pp. 1010-1016,DOI: 10.1021/jacs.5b12124

Also Published As

Publication number Publication date
KR102363283B1 (ko) 2022-02-15
US10797255B2 (en) 2020-10-06
CN108780759B (zh) 2023-08-08
GB201604050D0 (en) 2016-04-20
JP2019516232A (ja) 2019-06-13
KR20180122393A (ko) 2018-11-12
EP3427290A1 (en) 2019-01-16
PL3427290T3 (pl) 2022-01-10
CN108780759A (zh) 2018-11-09
EP3427290B1 (en) 2021-08-04
ES2884327T3 (es) 2021-12-10
WO2017153752A1 (en) 2017-09-14
US20190115549A1 (en) 2019-04-18

Similar Documents

Publication Publication Date Title
US10797255B2 (en) Material production process with alkylamine
EP3178121B1 (en) Process for producing a layer of organic perovskite material with improved crystallinity
US11264179B2 (en) Methods for producing and using perovskite materials and devices therefrom
Zhu et al. Investigation on the role of Lewis bases in the ripening process of perovskite films for highly efficient perovskite solar cells
EP3298630B1 (en) Method of making organo-metal halide perovskite films
Fairfield et al. Structure and chemical stability in perovskite–polymer hybrid photovoltaic materials
EP4002505A1 (en) Functionalized ionic liquids as stabilizers for perovskite solar cells
KR20210080492A (ko) 다중-접합 장치의 제조방법
US11943993B2 (en) Process for producing a layer with mixed solvent system
CN108350003A (zh) 卤化铅加合物和使用该卤化铅加合物的钙钛矿元件
KR102833574B1 (ko) 페로브스카이트 전구체 용액 및 상기 용액으로 형성된 페로브스카이트 광활성층을 포함하는 태양전지
HK40059008B (en) Process for producing a layer with mixed solvent system
HK40059008A (en) Process for producing a layer with mixed solvent system

Legal Events

Date Code Title Description
RD01 Notification of change of attorney

Free format text: JAPANESE INTERMEDIATE CODE: A7426

Effective date: 20191119

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A821

Effective date: 20191119

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20200305

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20200305

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20210216

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20210406

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20210630

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20210706

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20211216

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20220111

R150 Certificate of patent or registration of utility model

Ref document number: 7008634

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

R157 Certificate of patent or utility model (correction)

Free format text: JAPANESE INTERMEDIATE CODE: R157

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

S111 Request for change of ownership or part of ownership

Free format text: JAPANESE INTERMEDIATE CODE: R313113

S531 Written request for registration of change of domicile

Free format text: JAPANESE INTERMEDIATE CODE: R313531

R360 Written notification for declining of transfer of rights

Free format text: JAPANESE INTERMEDIATE CODE: R360

R360 Written notification for declining of transfer of rights

Free format text: JAPANESE INTERMEDIATE CODE: R360

R371 Transfer withdrawn

Free format text: JAPANESE INTERMEDIATE CODE: R371

S111 Request for change of ownership or part of ownership

Free format text: JAPANESE INTERMEDIATE CODE: R313113

S531 Written request for registration of change of domicile

Free format text: JAPANESE INTERMEDIATE CODE: R313531