CN108780759B - 使用烷基胺制造a/m/x材料的方法 - Google Patents

使用烷基胺制造a/m/x材料的方法 Download PDF

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Publication number
CN108780759B
CN108780759B CN201780016140.XA CN201780016140A CN108780759B CN 108780759 B CN108780759 B CN 108780759B CN 201780016140 A CN201780016140 A CN 201780016140A CN 108780759 B CN108780759 B CN 108780759B
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cation
compound
formula
precursor
layer
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CN108780759A (zh
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亨利·詹姆斯·施耐德
帕比塔·纳亚克
伯纳德·威戈
纳基塔·诺埃尔
塞维林·哈比斯如汀格尔
戴维·莫尔
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Oxford Photovoltaics Ltd
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Oxford University Innovation Ltd
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    • HELECTRICITY
    • H10SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10KORGANIC ELECTRIC SOLID-STATE DEVICES
    • H10K85/00Organic materials used in the body or electrodes of devices covered by this subclass
    • H10K85/60Organic compounds having low molecular weight
    • H10K85/649Aromatic compounds comprising a hetero atom
    • H10K85/656Aromatic compounds comprising a hetero atom comprising two or more different heteroatoms per ring
    • H10K85/6565Oxadiazole compounds
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • H01L21/02Manufacture or treatment of semiconductor devices or of parts thereof
    • H01L21/02104Forming layers
    • H01L21/02365Forming inorganic semiconducting materials on a substrate
    • H01L21/02518Deposited layers
    • H01L21/02521Materials
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • H01L21/02Manufacture or treatment of semiconductor devices or of parts thereof
    • H01L21/02104Forming layers
    • H01L21/02365Forming inorganic semiconducting materials on a substrate
    • H01L21/02612Formation types
    • H01L21/02617Deposition types
    • H01L21/02623Liquid deposition
    • H01L21/02628Liquid deposition using solutions
    • HELECTRICITY
    • H10SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10KORGANIC ELECTRIC SOLID-STATE DEVICES
    • H10K30/00Organic devices sensitive to infrared radiation, light, electromagnetic radiation of shorter wavelength or corpuscular radiation
    • HELECTRICITY
    • H10SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10KORGANIC ELECTRIC SOLID-STATE DEVICES
    • H10K30/00Organic devices sensitive to infrared radiation, light, electromagnetic radiation of shorter wavelength or corpuscular radiation
    • H10K30/10Organic devices sensitive to infrared radiation, light, electromagnetic radiation of shorter wavelength or corpuscular radiation comprising heterojunctions between organic semiconductors and inorganic semiconductors
    • H10K30/15Sensitised wide-bandgap semiconductor devices, e.g. dye-sensitised TiO2
    • H10K30/151Sensitised wide-bandgap semiconductor devices, e.g. dye-sensitised TiO2 the wide bandgap semiconductor comprising titanium oxide, e.g. TiO2
    • HELECTRICITY
    • H10SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10KORGANIC ELECTRIC SOLID-STATE DEVICES
    • H10K71/00Manufacture or treatment specially adapted for the organic devices covered by this subclass
    • H10K71/10Deposition of organic active material
    • H10K71/12Deposition of organic active material using liquid deposition, e.g. spin coating
    • H10K71/15Deposition of organic active material using liquid deposition, e.g. spin coating characterised by the solvent used
    • HELECTRICITY
    • H10SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10KORGANIC ELECTRIC SOLID-STATE DEVICES
    • H10K85/00Organic materials used in the body or electrodes of devices covered by this subclass
    • H10K85/50Organic perovskites; Hybrid organic-inorganic perovskites [HOIP], e.g. CH3NH3PbI3
    • HELECTRICITY
    • H10SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10KORGANIC ELECTRIC SOLID-STATE DEVICES
    • H10K30/00Organic devices sensitive to infrared radiation, light, electromagnetic radiation of shorter wavelength or corpuscular radiation
    • H10K30/10Organic devices sensitive to infrared radiation, light, electromagnetic radiation of shorter wavelength or corpuscular radiation comprising heterojunctions between organic semiconductors and inorganic semiconductors
    • HELECTRICITY
    • H10SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10KORGANIC ELECTRIC SOLID-STATE DEVICES
    • H10K30/00Organic devices sensitive to infrared radiation, light, electromagnetic radiation of shorter wavelength or corpuscular radiation
    • H10K30/50Photovoltaic [PV] devices
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E10/00Energy generation through renewable energy sources
    • Y02E10/50Photovoltaic [PV] energy
    • Y02E10/549Organic PV cells
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P70/00Climate change mitigation technologies in the production process for final industrial or consumer products
    • Y02P70/50Manufacturing or production processes characterised by the final manufactured product

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  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Chemical & Material Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Computer Hardware Design (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Microelectronics & Electronic Packaging (AREA)
  • Power Engineering (AREA)
  • Materials Engineering (AREA)
  • Electromagnetism (AREA)
  • Inorganic Chemistry (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Photovoltaic Devices (AREA)
CN201780016140.XA 2016-03-09 2017-03-08 使用烷基胺制造a/m/x材料的方法 Active CN108780759B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
GBGB1604050.3A GB201604050D0 (en) 2016-03-09 2016-03-09 A/M/X material production process with alkylamine
GB1604050.3 2016-03-09
PCT/GB2017/050623 WO2017153752A1 (en) 2016-03-09 2017-03-08 A/m/x material production process with alkylamine

Publications (2)

Publication Number Publication Date
CN108780759A CN108780759A (zh) 2018-11-09
CN108780759B true CN108780759B (zh) 2023-08-08

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US (1) US10797255B2 (enExample)
EP (1) EP3427290B1 (enExample)
JP (1) JP7008634B2 (enExample)
KR (1) KR102363283B1 (enExample)
CN (1) CN108780759B (enExample)
ES (1) ES2884327T3 (enExample)
GB (1) GB201604050D0 (enExample)
PL (1) PL3427290T3 (enExample)
WO (1) WO2017153752A1 (enExample)

Families Citing this family (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3679607B1 (en) * 2017-09-06 2025-03-12 Alliance for Sustainable Energy, LLC Organic-inorganic perovskite materials and methods of making the same
JP7304517B2 (ja) * 2018-07-10 2023-07-07 パナソニックIpマネジメント株式会社 太陽電池
GB201811538D0 (en) * 2018-07-13 2018-08-29 Univ Oxford Innovation Ltd Stabilised a/m/x materials
TWI827645B (zh) * 2018-08-23 2024-01-01 荷蘭商Asm Ip私人控股有限公司 基板處理設備及方法
GB201817167D0 (en) * 2018-10-22 2018-12-05 Univ Oxford Innovation Ltd Process for producing a layer with mixed solvent system
GB201817166D0 (en) * 2018-10-22 2018-12-05 Univ Oxford Innovation Ltd Multi-junction device production process
US11631582B2 (en) 2018-11-21 2023-04-18 Cubicpv Inc. Enhanced perovskite materials for photovoltaic devices
GB201820427D0 (en) 2018-12-14 2019-01-30 Univ Oxford Innovation Ltd Device interlayer
US11339058B2 (en) * 2018-12-14 2022-05-24 Alliance For Sustainable Energy, Llc Manufacturing of perovskite films
CN110048001A (zh) * 2019-04-01 2019-07-23 桂林理工大学 一种通过卤素替换工程来调节铋基有机-无机杂化材料形貌、带隙和稳定性的方法
CN113812012A (zh) * 2019-05-29 2021-12-17 松下知识产权经营株式会社 光电转换膜和采用该光电转换膜的太阳能电池以及光电转换膜的制造方法
WO2020243287A1 (en) 2019-05-30 2020-12-03 Energy Materials Corporation Method of making a perovskite layer at high speed
CN110862232A (zh) * 2019-11-12 2020-03-06 宁波大学 一种硫基微晶玻璃材料及其制备方法
CN113929641B (zh) * 2020-07-14 2025-05-06 西安固能新材料科技有限公司 系列乙二铵三元晶态化合物及其制备方法以及作为含能材料的用途
WO2021207344A1 (en) * 2020-04-08 2021-10-14 The Trustees Of Princeton University Thermal management for perovskite electronic devices
US20210388009A1 (en) * 2020-06-10 2021-12-16 Nanyang Technological University Organic metal-halide perovskite precursor, process for production and use thereof
CN111883664B (zh) * 2020-06-30 2022-09-23 西安理工大学 一种双注入倍增型有机光电探测器及其制备方法
US11846886B2 (en) 2020-11-23 2023-12-19 International Business Machines Corporation Photoacid generator
KR102573246B1 (ko) * 2021-04-20 2023-09-01 한국과학기술원 할라이드 페로브스카이트 박막의 저온 용액 공정 제조를 위한 용매 및 이를 이용한 페로브스카이트 박막 제조 방법
WO2023047116A1 (en) 2021-09-22 2023-03-30 Oxford University Innovation Limited Perovskite production process
KR102761911B1 (ko) * 2022-09-21 2025-02-05 서울대학교산학협력단 탠덤 태양전지의 제조방법
CN117205950A (zh) * 2023-09-19 2023-12-12 浙江师范大学 一种水稳定型卤化物钙钛矿Cs2Pt0.25Sn0.75Br6光催化剂的制备及应用
WO2025135104A1 (ja) * 2023-12-22 2025-06-26 株式会社カネカ ペロブスカイト前駆体液、太陽電池製造方法および太陽電池
CN118382342B (zh) * 2024-06-19 2024-10-01 天合光能股份有限公司 钙钛矿吸光层的制备方法、钙钛矿太阳能电池、光伏组件和光伏系统

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2014056903A (ja) * 2012-09-12 2014-03-27 Peccell Technologies Inc ペロブスカイト化合物を用いた光電変換素子およびその製造方法
CN104769736A (zh) * 2012-09-18 2015-07-08 埃西斯创新有限公司 光电器件
CN104798156A (zh) * 2012-11-16 2015-07-22 富士胶片株式会社 光电转换元件、色素增感太阳电池、金属络合物色素、色素溶液、色素吸附电极及色素增感太阳电池的制造方法
CN104810480A (zh) * 2015-04-22 2015-07-29 上海纳米技术及应用国家工程研究中心有限公司 一种用于钙钛矿电池的二氧化钛薄层的制备方法
CN104934503A (zh) * 2015-06-12 2015-09-23 辽宁工业大学 一种钙钛矿太阳能电池光吸收层材料甲基胺溴化铅的制备方法
CN104953031A (zh) * 2014-03-27 2015-09-30 株式会社理光 钙钛矿型太阳能电池

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5871579A (en) * 1997-09-25 1999-02-16 International Business Machines Corporation Two-step dipping technique for the preparation of organic-inorganic perovskite thin films
US9181475B2 (en) 2012-02-21 2015-11-10 Northwestern University Photoluminescent compounds
GB201414110D0 (en) * 2014-08-08 2014-09-24 Isis Innovation Thin film production
US20180006254A1 (en) 2014-12-23 2018-01-04 Los Alamos National Security, Llc Crystalline perovskite thin films and devices that include the films
CN105331362B (zh) 2015-12-07 2017-08-04 南京理工大学 一种室温大产率无机卤素钙钛矿荧光量子点的制备方法
CN105647530B (zh) * 2016-02-01 2017-12-12 南京理工大学 一种金属卤化物无机钙钛矿量子点的制备方法

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2014056903A (ja) * 2012-09-12 2014-03-27 Peccell Technologies Inc ペロブスカイト化合物を用いた光電変換素子およびその製造方法
CN104769736A (zh) * 2012-09-18 2015-07-08 埃西斯创新有限公司 光电器件
CN104798156A (zh) * 2012-11-16 2015-07-22 富士胶片株式会社 光电转换元件、色素增感太阳电池、金属络合物色素、色素溶液、色素吸附电极及色素增感太阳电池的制造方法
CN104953031A (zh) * 2014-03-27 2015-09-30 株式会社理光 钙钛矿型太阳能电池
CN104810480A (zh) * 2015-04-22 2015-07-29 上海纳米技术及应用国家工程研究中心有限公司 一种用于钙钛矿电池的二氧化钛薄层的制备方法
CN104934503A (zh) * 2015-06-12 2015-09-23 辽宁工业大学 一种钙钛矿太阳能电池光吸收层材料甲基胺溴化铅的制备方法

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KR102363283B1 (ko) 2022-02-15
US20190115549A1 (en) 2019-04-18
PL3427290T3 (pl) 2022-01-10
US10797255B2 (en) 2020-10-06
CN108780759A (zh) 2018-11-09
EP3427290B1 (en) 2021-08-04
WO2017153752A1 (en) 2017-09-14
GB201604050D0 (en) 2016-04-20
EP3427290A1 (en) 2019-01-16
JP2019516232A (ja) 2019-06-13
KR20180122393A (ko) 2018-11-12
JP7008634B2 (ja) 2022-02-10
ES2884327T3 (es) 2021-12-10

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