JP2019516232A5 - - Google Patents
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- JP2019516232A5 JP2019516232A5 JP2018546829A JP2018546829A JP2019516232A5 JP 2019516232 A5 JP2019516232 A5 JP 2019516232A5 JP 2018546829 A JP2018546829 A JP 2018546829A JP 2018546829 A JP2018546829 A JP 2018546829A JP 2019516232 A5 JP2019516232 A5 JP 2019516232A5
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- JP
- Japan
- Prior art keywords
- compound
- cation
- formula
- precursor
- substrate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 150000001875 compounds Chemical class 0.000 claims description 50
- 238000000034 method Methods 0.000 claims description 46
- 239000002243 precursor Substances 0.000 claims description 44
- 150000001768 cations Chemical class 0.000 claims description 37
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 claims description 30
- 239000000203 mixture Substances 0.000 claims description 29
- 239000000758 substrate Substances 0.000 claims description 22
- 150000003973 alkyl amines Chemical class 0.000 claims description 19
- 239000002904 solvent Substances 0.000 claims description 17
- BAVYZALUXZFZLV-UHFFFAOYSA-N Methylamine Chemical compound NC BAVYZALUXZFZLV-UHFFFAOYSA-N 0.000 claims description 15
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 claims description 12
- 239000000463 material Substances 0.000 claims description 11
- 239000004065 semiconductor Substances 0.000 claims description 11
- -1 metalloid cation Chemical class 0.000 claims description 10
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 8
- 229910021589 Copper(I) bromide Inorganic materials 0.000 claims description 6
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 claims description 6
- HQABUPZFAYXKJW-UHFFFAOYSA-N butan-1-amine Chemical compound CCCCN HQABUPZFAYXKJW-UHFFFAOYSA-N 0.000 claims description 6
- 125000000250 methylamino group Chemical group [H]N(*)C([H])([H])[H] 0.000 claims description 5
- 125000004169 (C1-C6) alkyl group Chemical group 0.000 claims description 4
- 125000004209 (C1-C8) alkyl group Chemical group 0.000 claims description 4
- 229910021591 Copper(I) chloride Inorganic materials 0.000 claims description 4
- QUSNBJAOOMFDIB-UHFFFAOYSA-N Ethylamine Chemical compound CCN QUSNBJAOOMFDIB-UHFFFAOYSA-N 0.000 claims description 4
- 150000001450 anions Chemical class 0.000 claims description 4
- OXBLHERUFWYNTN-UHFFFAOYSA-M copper(I) chloride Chemical compound [Cu]Cl OXBLHERUFWYNTN-UHFFFAOYSA-M 0.000 claims description 4
- 239000007772 electrode material Substances 0.000 claims description 4
- 239000011810 insulating material Substances 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 239000002184 metal Substances 0.000 claims description 4
- 229910052752 metalloid Inorganic materials 0.000 claims description 4
- DPBLXKKOBLCELK-UHFFFAOYSA-N pentan-1-amine Chemical compound CCCCCN DPBLXKKOBLCELK-UHFFFAOYSA-N 0.000 claims description 4
- FVSKHRXBFJPNKK-UHFFFAOYSA-N propionitrile Chemical compound CCC#N FVSKHRXBFJPNKK-UHFFFAOYSA-N 0.000 claims description 4
- WGYKZJWCGVVSQN-UHFFFAOYSA-N propylamine Chemical compound CCCN WGYKZJWCGVVSQN-UHFFFAOYSA-N 0.000 claims description 4
- 125000003837 (C1-C20) alkyl group Chemical group 0.000 claims description 2
- BAVYZALUXZFZLV-UHFFFAOYSA-O Methylammonium ion Chemical compound [NH3+]C BAVYZALUXZFZLV-UHFFFAOYSA-O 0.000 claims description 2
- 125000000217 alkyl group Chemical group 0.000 claims description 2
- 125000003118 aryl group Chemical group 0.000 claims description 2
- 238000010438 heat treatment Methods 0.000 claims description 2
- 229940100684 pentylamine Drugs 0.000 claims description 2
- 238000004528 spin coating Methods 0.000 claims description 2
- 101100533757 Caenorhabditis elegans snf-3 gene Proteins 0.000 claims 1
- 125000002091 cationic group Chemical group 0.000 claims 1
- 239000002195 soluble material Substances 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GBGB1604050.3A GB201604050D0 (en) | 2016-03-09 | 2016-03-09 | A/M/X material production process with alkylamine |
| GB1604050.3 | 2016-03-09 | ||
| PCT/GB2017/050623 WO2017153752A1 (en) | 2016-03-09 | 2017-03-08 | A/m/x material production process with alkylamine |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2019516232A JP2019516232A (ja) | 2019-06-13 |
| JP2019516232A5 true JP2019516232A5 (enExample) | 2020-04-16 |
| JP7008634B2 JP7008634B2 (ja) | 2022-02-10 |
Family
ID=55859227
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2018546829A Active JP7008634B2 (ja) | 2016-03-09 | 2017-03-08 | アルキルアミンを用いたa/m/x材料の製造方法 |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US10797255B2 (enExample) |
| EP (1) | EP3427290B1 (enExample) |
| JP (1) | JP7008634B2 (enExample) |
| KR (1) | KR102363283B1 (enExample) |
| CN (1) | CN108780759B (enExample) |
| ES (1) | ES2884327T3 (enExample) |
| GB (1) | GB201604050D0 (enExample) |
| PL (1) | PL3427290T3 (enExample) |
| WO (1) | WO2017153752A1 (enExample) |
Families Citing this family (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2019050906A1 (en) * | 2017-09-06 | 2019-03-14 | Alliance For Sustainable Energy, Llc | ORGANIC-INORGANIC PEROVSKITE MATERIALS AND METHODS OF MAKING SAME |
| JP7304517B2 (ja) * | 2018-07-10 | 2023-07-07 | パナソニックIpマネジメント株式会社 | 太陽電池 |
| GB201811538D0 (en) * | 2018-07-13 | 2018-08-29 | Univ Oxford Innovation Ltd | Stabilised a/m/x materials |
| TWI827645B (zh) * | 2018-08-23 | 2024-01-01 | 荷蘭商Asm Ip私人控股有限公司 | 基板處理設備及方法 |
| GB201817166D0 (en) * | 2018-10-22 | 2018-12-05 | Univ Oxford Innovation Ltd | Multi-junction device production process |
| GB201817167D0 (en) * | 2018-10-22 | 2018-12-05 | Univ Oxford Innovation Ltd | Process for producing a layer with mixed solvent system |
| US11631582B2 (en) * | 2018-11-21 | 2023-04-18 | Cubicpv Inc. | Enhanced perovskite materials for photovoltaic devices |
| US11339058B2 (en) * | 2018-12-14 | 2022-05-24 | Alliance For Sustainable Energy, Llc | Manufacturing of perovskite films |
| GB201820427D0 (en) | 2018-12-14 | 2019-01-30 | Univ Oxford Innovation Ltd | Device interlayer |
| CN110048001A (zh) * | 2019-04-01 | 2019-07-23 | 桂林理工大学 | 一种通过卤素替换工程来调节铋基有机-无机杂化材料形貌、带隙和稳定性的方法 |
| EP3979350A4 (en) * | 2019-05-29 | 2022-08-03 | Panasonic Intellectual Property Management Co., Ltd. | PHOTOELECTRIC CONVERSION FILM, SOLAR CELL USING THE SAME AND METHOD FOR PRODUCING PHOTOELECTRIC CONVERSION FILM |
| JP7519701B2 (ja) * | 2019-05-30 | 2024-07-22 | エナジー マテリアルズ コーポレイション | ペロブスカイト層の高速製造方法 |
| CN110862232A (zh) * | 2019-11-12 | 2020-03-06 | 宁波大学 | 一种硫基微晶玻璃材料及其制备方法 |
| CN113929641B (zh) * | 2020-07-14 | 2025-05-06 | 西安固能新材料科技有限公司 | 系列乙二铵三元晶态化合物及其制备方法以及作为含能材料的用途 |
| WO2021207344A1 (en) * | 2020-04-08 | 2021-10-14 | The Trustees Of Princeton University | Thermal management for perovskite electronic devices |
| US20210388009A1 (en) * | 2020-06-10 | 2021-12-16 | Nanyang Technological University | Organic metal-halide perovskite precursor, process for production and use thereof |
| CN111883664B (zh) * | 2020-06-30 | 2022-09-23 | 西安理工大学 | 一种双注入倍增型有机光电探测器及其制备方法 |
| US11846886B2 (en) | 2020-11-23 | 2023-12-19 | International Business Machines Corporation | Photoacid generator |
| KR102573246B1 (ko) * | 2021-04-20 | 2023-09-01 | 한국과학기술원 | 할라이드 페로브스카이트 박막의 저온 용액 공정 제조를 위한 용매 및 이를 이용한 페로브스카이트 박막 제조 방법 |
| WO2023047116A1 (en) | 2021-09-22 | 2023-03-30 | Oxford University Innovation Limited | Perovskite production process |
| KR102761911B1 (ko) * | 2022-09-21 | 2025-02-05 | 서울대학교산학협력단 | 탠덤 태양전지의 제조방법 |
| CN117205950A (zh) * | 2023-09-19 | 2023-12-12 | 浙江师范大学 | 一种水稳定型卤化物钙钛矿Cs2Pt0.25Sn0.75Br6光催化剂的制备及应用 |
| WO2025135104A1 (ja) * | 2023-12-22 | 2025-06-26 | 株式会社カネカ | ペロブスカイト前駆体液、太陽電池製造方法および太陽電池 |
| CN118382342B (zh) * | 2024-06-19 | 2024-10-01 | 天合光能股份有限公司 | 钙钛矿吸光层的制备方法、钙钛矿太阳能电池、光伏组件和光伏系统 |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5871579A (en) * | 1997-09-25 | 1999-02-16 | International Business Machines Corporation | Two-step dipping technique for the preparation of organic-inorganic perovskite thin films |
| US9181475B2 (en) | 2012-02-21 | 2015-11-10 | Northwestern University | Photoluminescent compounds |
| JP6069987B2 (ja) * | 2012-09-12 | 2017-02-01 | 日本ゼオン株式会社 | ペロブスカイト化合物を用いた光電変換素子の製造方法 |
| KR102698732B1 (ko) * | 2012-09-18 | 2024-08-27 | 옥스포드 유니버시티 이노베이션 리미티드 | 광전자 디바이스 |
| JP5992389B2 (ja) * | 2012-11-16 | 2016-09-14 | 富士フイルム株式会社 | 光電変換素子、色素増感太陽電池、金属錯体色素、色素溶液、色素吸着電極および色素増感太陽電池の製造方法 |
| JP6337561B2 (ja) * | 2014-03-27 | 2018-06-06 | 株式会社リコー | ペロブスカイト型太陽電池 |
| GB201414110D0 (en) | 2014-08-08 | 2014-09-24 | Isis Innovation | Thin film production |
| US20180006254A1 (en) | 2014-12-23 | 2018-01-04 | Los Alamos National Security, Llc | Crystalline perovskite thin films and devices that include the films |
| CN104810480A (zh) * | 2015-04-22 | 2015-07-29 | 上海纳米技术及应用国家工程研究中心有限公司 | 一种用于钙钛矿电池的二氧化钛薄层的制备方法 |
| CN104934503B (zh) * | 2015-06-12 | 2017-03-08 | 辽宁工业大学 | 一种钙钛矿太阳能电池光吸收层材料甲基胺溴化铅的制备方法 |
| CN105331362B (zh) | 2015-12-07 | 2017-08-04 | 南京理工大学 | 一种室温大产率无机卤素钙钛矿荧光量子点的制备方法 |
| CN105647530B (zh) * | 2016-02-01 | 2017-12-12 | 南京理工大学 | 一种金属卤化物无机钙钛矿量子点的制备方法 |
-
2016
- 2016-03-09 GB GBGB1604050.3A patent/GB201604050D0/en not_active Ceased
-
2017
- 2017-03-08 KR KR1020187028785A patent/KR102363283B1/ko active Active
- 2017-03-08 US US16/082,415 patent/US10797255B2/en active Active
- 2017-03-08 JP JP2018546829A patent/JP7008634B2/ja active Active
- 2017-03-08 WO PCT/GB2017/050623 patent/WO2017153752A1/en not_active Ceased
- 2017-03-08 ES ES17711270T patent/ES2884327T3/es active Active
- 2017-03-08 PL PL17711270T patent/PL3427290T3/pl unknown
- 2017-03-08 CN CN201780016140.XA patent/CN108780759B/zh active Active
- 2017-03-08 EP EP17711270.3A patent/EP3427290B1/en active Active
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