JP6692315B2 - 圧力変動吸着式水素製造装置 - Google Patents

圧力変動吸着式水素製造装置 Download PDF

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JP6692315B2
JP6692315B2 JP2017051668A JP2017051668A JP6692315B2 JP 6692315 B2 JP6692315 B2 JP 6692315B2 JP 2017051668 A JP2017051668 A JP 2017051668A JP 2017051668 A JP2017051668 A JP 2017051668A JP 6692315 B2 JP6692315 B2 JP 6692315B2
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pressure
adsorption
gas
tower
adsorption tower
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JP2018154518A (ja
JP2018154518A5 (enrdf_load_stackoverflow
Inventor
飛昂 阿曽沼
飛昂 阿曽沼
翼 清水
翼 清水
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Osaka Gas Co Ltd
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Osaka Gas Co Ltd
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Priority to JP2017051668A priority Critical patent/JP6692315B2/ja
Application filed by Osaka Gas Co Ltd filed Critical Osaka Gas Co Ltd
Priority to US16/493,048 priority patent/US11369915B2/en
Priority to KR1020197026142A priority patent/KR20190127713A/ko
Priority to CN201880018530.5A priority patent/CN110382408B/zh
Priority to PCT/JP2018/010134 priority patent/WO2018168985A1/ja
Priority to EP18768092.1A priority patent/EP3597592B1/en
Priority to AU2018236554A priority patent/AU2018236554B2/en
Publication of JP2018154518A publication Critical patent/JP2018154518A/ja
Publication of JP2018154518A5 publication Critical patent/JP2018154518A5/ja
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/047—Pressure swing adsorption
    • B01D53/0476—Vacuum pressure swing adsorption
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/047—Pressure swing adsorption
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/047—Pressure swing adsorption
    • B01D53/053—Pressure swing adsorption with storage or buffer vessel
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/50—Separation of hydrogen or hydrogen containing gases from gaseous mixtures, e.g. purification
    • C01B3/56—Separation of hydrogen or hydrogen containing gases from gaseous mixtures, e.g. purification by contacting with solids; Regeneration of used solids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2256/00—Main component in the product gas stream after treatment
    • B01D2256/16—Hydrogen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40007—Controlling pressure or temperature swing adsorption
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40013—Pressurization
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40013—Pressurization
    • B01D2259/40018—Pressurization with more than three sub-steps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40028—Depressurization
    • B01D2259/4003—Depressurization with two sub-steps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40035—Equalization
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40035—Equalization
    • B01D2259/40037—Equalization with two sub-steps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40035—Equalization
    • B01D2259/40041—Equalization with more than three sub-steps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40058—Number of sequence steps, including sub-steps, per cycle
    • B01D2259/40071—Nine
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40058—Number of sequence steps, including sub-steps, per cycle
    • B01D2259/40075—More than ten
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/404—Further details for adsorption processes and devices using four beds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/406—Further details for adsorption processes and devices using more than four beds
    • B01D2259/4061—Further details for adsorption processes and devices using more than four beds using five beds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/042—Purification by adsorption on solids
    • C01B2203/0425—In-situ adsorption process during hydrogen production
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/042—Purification by adsorption on solids
    • C01B2203/043—Regenerative adsorption process in two or more beds, one for adsorption, the other for regeneration

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Combustion & Propulsion (AREA)
  • Inorganic Chemistry (AREA)
  • Separation Of Gases By Adsorption (AREA)
  • Hydrogen, Water And Hydrids (AREA)
JP2017051668A 2017-03-16 2017-03-16 圧力変動吸着式水素製造装置 Active JP6692315B2 (ja)

Priority Applications (7)

Application Number Priority Date Filing Date Title
JP2017051668A JP6692315B2 (ja) 2017-03-16 2017-03-16 圧力変動吸着式水素製造装置
KR1020197026142A KR20190127713A (ko) 2017-03-16 2018-03-15 압력 변동 흡착식 수소 제조 장치
CN201880018530.5A CN110382408B (zh) 2017-03-16 2018-03-15 压力变动吸附式氢制造装置
PCT/JP2018/010134 WO2018168985A1 (ja) 2017-03-16 2018-03-15 圧力変動吸着式水素製造装置
US16/493,048 US11369915B2 (en) 2017-03-16 2018-03-15 Pressure swing adsorption type hydrogen manufacturing apparatus
EP18768092.1A EP3597592B1 (en) 2017-03-16 2018-03-15 Pressure swing adsorption hydrogen manufacturing apparatus
AU2018236554A AU2018236554B2 (en) 2017-03-16 2018-03-15 Pressure swing adsorption hydrogen manufacturing apparatus

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2017051668A JP6692315B2 (ja) 2017-03-16 2017-03-16 圧力変動吸着式水素製造装置

Publications (3)

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JP2018154518A JP2018154518A (ja) 2018-10-04
JP2018154518A5 JP2018154518A5 (enrdf_load_stackoverflow) 2020-02-20
JP6692315B2 true JP6692315B2 (ja) 2020-05-13

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JP2017051668A Active JP6692315B2 (ja) 2017-03-16 2017-03-16 圧力変動吸着式水素製造装置

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US (1) US11369915B2 (enrdf_load_stackoverflow)
EP (1) EP3597592B1 (enrdf_load_stackoverflow)
JP (1) JP6692315B2 (enrdf_load_stackoverflow)
KR (1) KR20190127713A (enrdf_load_stackoverflow)
CN (1) CN110382408B (enrdf_load_stackoverflow)
AU (1) AU2018236554B2 (enrdf_load_stackoverflow)
WO (1) WO2018168985A1 (enrdf_load_stackoverflow)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP7129329B2 (ja) * 2018-12-21 2022-09-01 東京瓦斯株式会社 水素製造装置、及び水素製造装置の洗浄方法、水素製造装置制御プログラム、及び水素製造システム
KR20220043468A (ko) * 2020-09-29 2022-04-05 현대자동차주식회사 압력흡착시스템 및 방법
KR20220075958A (ko) 2020-11-30 2022-06-08 현대자동차주식회사 원료가스 개질 시스템 및 제어방법
KR102513166B1 (ko) * 2021-08-05 2023-03-23 주식회사 에프알디 압력순환흡착 방식을 이용한 고순도 수소 가스 정제 장치
CN114148990B (zh) * 2021-12-02 2023-06-23 西南化工研究设计院有限公司 一种具有复合缓冲罐的变压吸附制氢系统
CN115259087B (zh) * 2022-07-29 2023-09-05 广西柳州钢铁集团有限公司 一种创建预判机制提高氢气纯度的制氢操作方法及系统

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US4077780A (en) * 1976-10-20 1978-03-07 Union Carbide Corporation Recovery of hydrogen and nitrogen from ammonia plant purge gas
US5354346A (en) * 1992-10-01 1994-10-11 Air Products And Chemicals, Inc. Purge effluent repressurized adsorption process
JP3377256B2 (ja) * 1993-06-30 2003-02-17 日本パイオニクス株式会社 ガス発生装置
US5704964A (en) * 1994-12-27 1998-01-06 Nippon Sanso Corporation Pressure swing adsorption process
US5656065A (en) * 1995-10-04 1997-08-12 Air Products And Chemicals, Inc. Multibed pressure swing adsorption apparatus and method for the operation thereof
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US7491260B2 (en) * 2005-06-23 2009-02-17 Air Products And Chemicals, Inc. Valve operation diagnostic method for pressure swing adsorption systems
JP2007209868A (ja) * 2006-02-08 2007-08-23 Mitsubishi Kakoki Kaisha Ltd 圧力スイング吸着装置の安定運転方法
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KR100896455B1 (ko) * 2007-07-09 2009-05-14 한국에너지기술연구원 압력변동흡착장치 및 이를 이용한 수소 정제 방법
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Also Published As

Publication number Publication date
JP2018154518A (ja) 2018-10-04
CN110382408A (zh) 2019-10-25
KR20190127713A (ko) 2019-11-13
US11369915B2 (en) 2022-06-28
EP3597592A1 (en) 2020-01-22
WO2018168985A1 (ja) 2018-09-20
CN110382408B (zh) 2023-04-18
US20200122080A1 (en) 2020-04-23
EP3597592A4 (en) 2021-01-27
EP3597592B1 (en) 2023-01-25
AU2018236554A1 (en) 2019-10-31
AU2018236554B2 (en) 2022-11-24

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