JP6625538B2 - 前剥離させた層状材料 - Google Patents
前剥離させた層状材料 Download PDFInfo
- Publication number
- JP6625538B2 JP6625538B2 JP2016540527A JP2016540527A JP6625538B2 JP 6625538 B2 JP6625538 B2 JP 6625538B2 JP 2016540527 A JP2016540527 A JP 2016540527A JP 2016540527 A JP2016540527 A JP 2016540527A JP 6625538 B2 JP6625538 B2 JP 6625538B2
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- JP
- Japan
- Prior art keywords
- tert
- layered material
- butyl
- bis
- hydroxy
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000000463 material Substances 0.000 title claims description 93
- -1 alkali metal salts Chemical class 0.000 claims description 123
- 239000000203 mixture Substances 0.000 claims description 92
- 239000000654 additive Substances 0.000 claims description 71
- 238000000034 method Methods 0.000 claims description 58
- 239000003063 flame retardant Substances 0.000 claims description 43
- 150000001412 amines Chemical class 0.000 claims description 33
- 238000002844 melting Methods 0.000 claims description 30
- 230000008018 melting Effects 0.000 claims description 26
- 239000004597 plastic additive Substances 0.000 claims description 26
- 239000003963 antioxidant agent Substances 0.000 claims description 23
- 239000004611 light stabiliser Substances 0.000 claims description 18
- 239000006096 absorbing agent Substances 0.000 claims description 16
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 16
- 239000000194 fatty acid Substances 0.000 claims description 16
- 229930195729 fatty acid Natural products 0.000 claims description 16
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 15
- 229910052751 metal Inorganic materials 0.000 claims description 15
- 239000002184 metal Substances 0.000 claims description 15
- 150000004665 fatty acids Chemical class 0.000 claims description 14
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N phenol group Chemical group C1(=CC=CC=C1)O ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims description 12
- 239000003242 anti bacterial agent Substances 0.000 claims description 11
- 230000003078 antioxidant effect Effects 0.000 claims description 11
- 239000003086 colorant Substances 0.000 claims description 11
- 239000003381 stabilizer Substances 0.000 claims description 11
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims description 10
- 239000011229 interlayer Substances 0.000 claims description 9
- 229910052698 phosphorus Inorganic materials 0.000 claims description 8
- 239000011574 phosphorus Substances 0.000 claims description 8
- 239000000377 silicon dioxide Substances 0.000 claims description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 6
- 239000010410 layer Substances 0.000 claims description 6
- GUJOJGAPFQRJSV-UHFFFAOYSA-N dialuminum;dioxosilane;oxygen(2-);hydrate Chemical compound O.[O-2].[O-2].[O-2].[Al+3].[Al+3].O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O GUJOJGAPFQRJSV-UHFFFAOYSA-N 0.000 claims description 5
- 239000000454 talc Substances 0.000 claims description 5
- 229910052623 talc Inorganic materials 0.000 claims description 5
- ZCILGMFPJBRCNO-UHFFFAOYSA-N 4-phenyl-2H-benzotriazol-5-ol Chemical compound OC1=CC=C2NN=NC2=C1C1=CC=CC=C1 ZCILGMFPJBRCNO-UHFFFAOYSA-N 0.000 claims description 4
- 229910052900 illite Inorganic materials 0.000 claims description 4
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims description 4
- 229910044991 metal oxide Inorganic materials 0.000 claims description 4
- 150000004706 metal oxides Chemical class 0.000 claims description 4
- 229910052901 montmorillonite Inorganic materials 0.000 claims description 4
- VGIBGUSAECPPNB-UHFFFAOYSA-L nonaaluminum;magnesium;tripotassium;1,3-dioxido-2,4,5-trioxa-1,3-disilabicyclo[1.1.1]pentane;iron(2+);oxygen(2-);fluoride;hydroxide Chemical compound [OH-].[O-2].[O-2].[O-2].[O-2].[O-2].[F-].[Mg+2].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[K+].[K+].[K+].[Fe+2].O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2 VGIBGUSAECPPNB-UHFFFAOYSA-L 0.000 claims description 4
- 125000002467 phosphate group Chemical group [H]OP(=O)(O[H])O[*] 0.000 claims description 4
- 239000010457 zeolite Substances 0.000 claims description 4
- JYEUMXHLPRZUAT-UHFFFAOYSA-N 1,2,3-triazine Chemical group C1=CN=NN=C1 JYEUMXHLPRZUAT-UHFFFAOYSA-N 0.000 claims description 3
- XMWRBQBLMFGWIX-UHFFFAOYSA-N C60 fullerene Chemical compound C12=C3C(C4=C56)=C7C8=C5C5=C9C%10=C6C6=C4C1=C1C4=C6C6=C%10C%10=C9C9=C%11C5=C8C5=C8C7=C3C3=C7C2=C1C1=C2C4=C6C4=C%10C6=C9C9=C%11C5=C5C8=C3C3=C7C1=C1C2=C4C6=C2C9=C5C3=C12 XMWRBQBLMFGWIX-UHFFFAOYSA-N 0.000 claims description 3
- 239000004113 Sepiolite Substances 0.000 claims description 3
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims description 3
- HPTYUNKZVDYXLP-UHFFFAOYSA-N aluminum;trihydroxy(trihydroxysilyloxy)silane;hydrate Chemical compound O.[Al].[Al].O[Si](O)(O)O[Si](O)(O)O HPTYUNKZVDYXLP-UHFFFAOYSA-N 0.000 claims description 3
- 229960000892 attapulgite Drugs 0.000 claims description 3
- 239000000440 bentonite Substances 0.000 claims description 3
- 229910000278 bentonite Inorganic materials 0.000 claims description 3
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims description 3
- VNSBYDPZHCQWNB-UHFFFAOYSA-N calcium;aluminum;dioxido(oxo)silane;sodium;hydrate Chemical compound O.[Na].[Al].[Ca+2].[O-][Si]([O-])=O VNSBYDPZHCQWNB-UHFFFAOYSA-N 0.000 claims description 3
- 239000002041 carbon nanotube Substances 0.000 claims description 3
- 229910021393 carbon nanotube Inorganic materials 0.000 claims description 3
- GDVKFRBCXAPAQJ-UHFFFAOYSA-A dialuminum;hexamagnesium;carbonate;hexadecahydroxide Chemical compound [OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Al+3].[Al+3].[O-]C([O-])=O GDVKFRBCXAPAQJ-UHFFFAOYSA-A 0.000 claims description 3
- 229910003472 fullerene Inorganic materials 0.000 claims description 3
- 239000010439 graphite Substances 0.000 claims description 3
- 229910002804 graphite Inorganic materials 0.000 claims description 3
- 229910052621 halloysite Inorganic materials 0.000 claims description 3
- 229910000271 hectorite Inorganic materials 0.000 claims description 3
- KWLMIXQRALPRBC-UHFFFAOYSA-L hectorite Chemical compound [Li+].[OH-].[OH-].[Na+].[Mg+2].O1[Si]2([O-])O[Si]1([O-])O[Si]([O-])(O1)O[Si]1([O-])O2 KWLMIXQRALPRBC-UHFFFAOYSA-L 0.000 claims description 3
- 229910001701 hydrotalcite Inorganic materials 0.000 claims description 3
- 229960001545 hydrotalcite Drugs 0.000 claims description 3
- 229910052622 kaolinite Inorganic materials 0.000 claims description 3
- 239000010445 mica Substances 0.000 claims description 3
- 229910052618 mica group Inorganic materials 0.000 claims description 3
- 229910000273 nontronite Inorganic materials 0.000 claims description 3
- 229910052625 palygorskite Inorganic materials 0.000 claims description 3
- 125000003386 piperidinyl group Chemical group 0.000 claims description 3
- 229910000275 saponite Inorganic materials 0.000 claims description 3
- 229910000276 sauconite Inorganic materials 0.000 claims description 3
- 229910052624 sepiolite Inorganic materials 0.000 claims description 3
- 235000019355 sepiolite Nutrition 0.000 claims description 3
- 239000010455 vermiculite Substances 0.000 claims description 3
- 229910052902 vermiculite Inorganic materials 0.000 claims description 3
- 235000019354 vermiculite Nutrition 0.000 claims description 3
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 claims description 2
- 229910052783 alkali metal Inorganic materials 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims description 2
- 239000007800 oxidant agent Substances 0.000 claims 1
- OJMIONKXNSYLSR-UHFFFAOYSA-N phosphorous acid Chemical group OP(O)O OJMIONKXNSYLSR-UHFFFAOYSA-N 0.000 claims 1
- 125000001425 triazolyl group Chemical group 0.000 claims 1
- 229920000642 polymer Polymers 0.000 description 52
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 48
- 239000000049 pigment Substances 0.000 description 44
- 230000000996 additive effect Effects 0.000 description 43
- 238000001125 extrusion Methods 0.000 description 29
- 229920001577 copolymer Polymers 0.000 description 26
- 239000002114 nanocomposite Substances 0.000 description 26
- 235000006708 antioxidants Nutrition 0.000 description 21
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 20
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 17
- 229920000877 Melamine resin Polymers 0.000 description 16
- 239000004952 Polyamide Substances 0.000 description 16
- 238000002156 mixing Methods 0.000 description 16
- 229920002647 polyamide Polymers 0.000 description 16
- ABLZXFCXXLZCGV-UHFFFAOYSA-N Phosphorous acid Chemical compound OP(O)=O ABLZXFCXXLZCGV-UHFFFAOYSA-N 0.000 description 15
- JDSHMPZPIAZGSV-UHFFFAOYSA-N melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 description 15
- RSOILICUEWXSLA-UHFFFAOYSA-N bis(1,2,2,6,6-pentamethylpiperidin-4-yl) decanedioate Chemical compound C1C(C)(C)N(C)C(C)(C)CC1OC(=O)CCCCCCCCC(=O)OC1CC(C)(C)N(C)C(C)(C)C1 RSOILICUEWXSLA-UHFFFAOYSA-N 0.000 description 14
- 150000001875 compounds Chemical class 0.000 description 14
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 13
- JKIJEFPNVSHHEI-UHFFFAOYSA-N Phenol, 2,4-bis(1,1-dimethylethyl)-, phosphite (3:1) Chemical compound CC(C)(C)C1=CC(C(C)(C)C)=CC=C1OP(OC=1C(=CC(=CC=1)C(C)(C)C)C(C)(C)C)OC1=CC=C(C(C)(C)C)C=C1C(C)(C)C JKIJEFPNVSHHEI-UHFFFAOYSA-N 0.000 description 13
- 230000007423 decrease Effects 0.000 description 13
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 12
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 12
- 238000002360 preparation method Methods 0.000 description 12
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 description 11
- 229920005989 resin Polymers 0.000 description 11
- 239000011347 resin Substances 0.000 description 11
- DLHNOZQXRABONJ-UHFFFAOYSA-N bis(1-cyclohexyloxy-2,2,6,6-tetramethylpiperidin-4-yl) decanedioate Chemical compound CC1(C)CC(OC(=O)CCCCCCCCC(=O)OC2CC(C)(C)N(OC3CCCCC3)C(C)(C)C2)CC(C)(C)N1OC1CCCCC1 DLHNOZQXRABONJ-UHFFFAOYSA-N 0.000 description 10
- 238000002474 experimental method Methods 0.000 description 10
- 150000007974 melamines Chemical class 0.000 description 10
- 239000000178 monomer Substances 0.000 description 10
- 239000004417 polycarbonate Substances 0.000 description 10
- 229920000388 Polyphosphate Polymers 0.000 description 9
- XITRBUPOXXBIJN-UHFFFAOYSA-N bis(2,2,6,6-tetramethylpiperidin-4-yl) decanedioate Chemical compound C1C(C)(C)NC(C)(C)CC1OC(=O)CCCCCCCCC(=O)OC1CC(C)(C)NC(C)(C)C1 XITRBUPOXXBIJN-UHFFFAOYSA-N 0.000 description 9
- 229920001519 homopolymer Polymers 0.000 description 9
- 239000007788 liquid Substances 0.000 description 9
- 229920000728 polyester Polymers 0.000 description 9
- 229920006324 polyoxymethylene Polymers 0.000 description 9
- 239000001205 polyphosphate Substances 0.000 description 9
- 239000006097 ultraviolet radiation absorber Substances 0.000 description 9
- 229920002554 vinyl polymer Polymers 0.000 description 9
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 description 8
- 229910019142 PO4 Inorganic materials 0.000 description 8
- BGYHLZZASRKEJE-UHFFFAOYSA-N [3-[3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoyloxy]-2,2-bis[3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoyloxymethyl]propyl] 3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoate Chemical compound CC(C)(C)C1=C(O)C(C(C)(C)C)=CC(CCC(=O)OCC(COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)(COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)=C1 BGYHLZZASRKEJE-UHFFFAOYSA-N 0.000 description 8
- XECAHXYUAAWDEL-UHFFFAOYSA-N acrylonitrile butadiene styrene Chemical compound C=CC=C.C=CC#N.C=CC1=CC=CC=C1 XECAHXYUAAWDEL-UHFFFAOYSA-N 0.000 description 8
- 229920000122 acrylonitrile butadiene styrene Polymers 0.000 description 8
- 239000004676 acrylonitrile butadiene styrene Substances 0.000 description 8
- KBPLFHHGFOOTCA-UHFFFAOYSA-N caprylic alcohol Natural products CCCCCCCCO KBPLFHHGFOOTCA-UHFFFAOYSA-N 0.000 description 8
- 150000002148 esters Chemical class 0.000 description 8
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 description 8
- 235000021317 phosphate Nutrition 0.000 description 8
- 229920002857 polybutadiene Polymers 0.000 description 8
- 229920002961 polybutylene succinate Polymers 0.000 description 8
- 239000004631 polybutylene succinate Substances 0.000 description 8
- 229920001707 polybutylene terephthalate Polymers 0.000 description 8
- VEORPZCZECFIRK-UHFFFAOYSA-N 3,3',5,5'-tetrabromobisphenol A Chemical compound C=1C(Br)=C(O)C(Br)=CC=1C(C)(C)C1=CC(Br)=C(O)C(Br)=C1 VEORPZCZECFIRK-UHFFFAOYSA-N 0.000 description 7
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 7
- 239000005977 Ethylene Substances 0.000 description 7
- 239000005062 Polybutadiene Substances 0.000 description 7
- 239000004698 Polyethylene Substances 0.000 description 7
- 239000007983 Tris buffer Substances 0.000 description 7
- 125000003118 aryl group Chemical group 0.000 description 7
- 239000004927 clay Substances 0.000 description 7
- 229910052570 clay Inorganic materials 0.000 description 7
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 description 7
- 239000010452 phosphate Substances 0.000 description 7
- 229920000573 polyethylene Polymers 0.000 description 7
- 239000004800 polyvinyl chloride Substances 0.000 description 7
- 229920000915 polyvinyl chloride Polymers 0.000 description 7
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 6
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 6
- 239000004721 Polyphenylene oxide Substances 0.000 description 6
- 239000004743 Polypropylene Substances 0.000 description 6
- 239000004793 Polystyrene Substances 0.000 description 6
- ADCOVFLJGNWWNZ-UHFFFAOYSA-N antimony trioxide Chemical compound O=[Sb]O[Sb]=O ADCOVFLJGNWWNZ-UHFFFAOYSA-N 0.000 description 6
- WHHGLZMJPXIBIX-UHFFFAOYSA-N decabromodiphenyl ether Chemical compound BrC1=C(Br)C(Br)=C(Br)C(Br)=C1OC1=C(Br)C(Br)=C(Br)C(Br)=C1Br WHHGLZMJPXIBIX-UHFFFAOYSA-N 0.000 description 6
- 150000001993 dienes Chemical class 0.000 description 6
- 229910052757 nitrogen Inorganic materials 0.000 description 6
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 6
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 6
- 235000011176 polyphosphates Nutrition 0.000 description 6
- 229920002223 polystyrene Polymers 0.000 description 6
- 239000000843 powder Substances 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- ZMWRRFHBXARRRT-UHFFFAOYSA-N 2-(benzotriazol-2-yl)-4,6-bis(2-methylbutan-2-yl)phenol Chemical compound CCC(C)(C)C1=CC(C(C)(C)CC)=CC(N2N=C3C=CC=CC3=N2)=C1O ZMWRRFHBXARRRT-UHFFFAOYSA-N 0.000 description 5
- 150000001252 acrylic acid derivatives Chemical class 0.000 description 5
- 125000000217 alkyl group Chemical group 0.000 description 5
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 5
- PVIFXIBJQWPGNU-UHFFFAOYSA-N bis(1-acetyloxy-2,2,6,6-tetramethylpiperidin-4-yl) decanedioate Chemical compound C1C(C)(C)N(OC(=O)C)C(C)(C)CC1OC(=O)CCCCCCCCC(=O)OC1CC(C)(C)N(OC(C)=O)C(C)(C)C1 PVIFXIBJQWPGNU-UHFFFAOYSA-N 0.000 description 5
- 239000003054 catalyst Substances 0.000 description 5
- XCJYREBRNVKWGJ-UHFFFAOYSA-N copper(II) phthalocyanine Chemical compound [Cu+2].C12=CC=CC=C2C(N=C2[N-]C(C3=CC=CC=C32)=N2)=NC1=NC([C]1C=CC=CC1=1)=NC=1N=C1[C]3C=CC=CC3=C2[N-]1 XCJYREBRNVKWGJ-UHFFFAOYSA-N 0.000 description 5
- 239000011159 matrix material Substances 0.000 description 5
- 239000002530 phenolic antioxidant Substances 0.000 description 5
- XFZRQAZGUOTJCS-UHFFFAOYSA-N phosphoric acid;1,3,5-triazine-2,4,6-triamine Chemical compound OP(O)(O)=O.NC1=NC(N)=NC(N)=N1 XFZRQAZGUOTJCS-UHFFFAOYSA-N 0.000 description 5
- 229920000098 polyolefin Polymers 0.000 description 5
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- 150000005846 sugar alcohols Polymers 0.000 description 5
- KKEYFWRCBNTPAC-UHFFFAOYSA-L terephthalate(2-) Chemical compound [O-]C(=O)C1=CC=C(C([O-])=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-L 0.000 description 5
- BHYQWBKCXBXPKM-UHFFFAOYSA-N tris[3-bromo-2,2-bis(bromomethyl)propyl] phosphate Chemical compound BrCC(CBr)(CBr)COP(=O)(OCC(CBr)(CBr)CBr)OCC(CBr)(CBr)CBr BHYQWBKCXBXPKM-UHFFFAOYSA-N 0.000 description 5
- KAKZBPTYRLMSJV-UHFFFAOYSA-N vinyl-ethylene Natural products C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 5
- 239000001993 wax Substances 0.000 description 5
- HJIAMFHSAAEUKR-UHFFFAOYSA-N (2-hydroxyphenyl)-phenylmethanone Chemical compound OC1=CC=CC=C1C(=O)C1=CC=CC=C1 HJIAMFHSAAEUKR-UHFFFAOYSA-N 0.000 description 4
- DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 description 4
- BPXVHIRIPLPOPT-UHFFFAOYSA-N 1,3,5-tris(2-hydroxyethyl)-1,3,5-triazinane-2,4,6-trione Chemical compound OCCN1C(=O)N(CCO)C(=O)N(CCO)C1=O BPXVHIRIPLPOPT-UHFFFAOYSA-N 0.000 description 4
- ALVZNPYWJMLXKV-UHFFFAOYSA-N 1,9-Nonanediol Chemical compound OCCCCCCCCCO ALVZNPYWJMLXKV-UHFFFAOYSA-N 0.000 description 4
- ZPIRWAHWDCHWLM-UHFFFAOYSA-N 2-dodecylsulfanylethanol Chemical compound CCCCCCCCCCCCSCCO ZPIRWAHWDCHWLM-UHFFFAOYSA-N 0.000 description 4
- VVISQEKWYPFFLK-UHFFFAOYSA-N 2-n,2-n,4-n,4-n-tetrabutyl-6-chloro-1,3,5-triazine-2,4-diamine Chemical compound CCCCN(CCCC)C1=NC(Cl)=NC(N(CCCC)CCCC)=N1 VVISQEKWYPFFLK-UHFFFAOYSA-N 0.000 description 4
- YEJRWHAVMIAJKC-UHFFFAOYSA-N 4-Butyrolactone Chemical compound O=C1CCCO1 YEJRWHAVMIAJKC-UHFFFAOYSA-N 0.000 description 4
- CKPKHTKLLYPGFM-UHFFFAOYSA-N 6,6-dimethylheptane-1,1-diol Chemical compound CC(CCCCC(O)O)(C)C CKPKHTKLLYPGFM-UHFFFAOYSA-N 0.000 description 4
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 4
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 4
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 4
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- FAUOSXUSCVJWAY-UHFFFAOYSA-N tetrakis(hydroxymethyl)phosphanium Chemical class OC[P+](CO)(CO)CO FAUOSXUSCVJWAY-UHFFFAOYSA-N 0.000 description 1
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- HKFXIAYXXUVGPX-UHFFFAOYSA-N triazanium urea phosphate Chemical compound [NH4+].[NH4+].[NH4+].NC(N)=O.[O-]P([O-])([O-])=O HKFXIAYXXUVGPX-UHFFFAOYSA-N 0.000 description 1
- ZZMPGNVAROSUSZ-UHFFFAOYSA-N triazanium;1,3,5-triazine-2,4,6-triamine;phosphate Chemical compound [NH4+].[NH4+].[NH4+].[O-]P([O-])([O-])=O.NC1=NC(N)=NC(N)=N1 ZZMPGNVAROSUSZ-UHFFFAOYSA-N 0.000 description 1
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- VLCLHFYFMCKBRP-UHFFFAOYSA-N tricalcium;diborate Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]B([O-])[O-].[O-]B([O-])[O-] VLCLHFYFMCKBRP-UHFFFAOYSA-N 0.000 description 1
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- 125000005591 trimellitate group Chemical group 0.000 description 1
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- KVMPUXDNESXNOH-UHFFFAOYSA-N tris(1-chloropropan-2-yl) phosphate Chemical compound ClCC(C)OP(=O)(OC(C)CCl)OC(C)CCl KVMPUXDNESXNOH-UHFFFAOYSA-N 0.000 description 1
- JZZBTMVTLBHJHL-UHFFFAOYSA-N tris(2,3-dichloropropyl) phosphate Chemical compound ClCC(Cl)COP(=O)(OCC(Cl)CCl)OCC(Cl)CCl JZZBTMVTLBHJHL-UHFFFAOYSA-N 0.000 description 1
- WTLBZVNBAKMVDP-UHFFFAOYSA-N tris(2-butoxyethyl) phosphate Chemical compound CCCCOCCOP(=O)(OCCOCCCC)OCCOCCCC WTLBZVNBAKMVDP-UHFFFAOYSA-N 0.000 description 1
- LUVCTYHBTXSAMX-UHFFFAOYSA-N tris(2-chloroethyl) phosphite Chemical compound ClCCOP(OCCCl)OCCCl LUVCTYHBTXSAMX-UHFFFAOYSA-N 0.000 description 1
- WGKLOLBTFWFKOD-UHFFFAOYSA-N tris(2-nonylphenyl) phosphite Chemical compound CCCCCCCCCC1=CC=CC=C1OP(OC=1C(=CC=CC=1)CCCCCCCCC)OC1=CC=CC=C1CCCCCCCCC WGKLOLBTFWFKOD-UHFFFAOYSA-N 0.000 description 1
- SEOBQCUWPSPHTB-UHFFFAOYSA-N tris(3-bromo-3,3-dichloropropyl) phosphite Chemical compound ClC(Cl)(Br)CCOP(OCCC(Cl)(Cl)Br)OCCC(Cl)(Cl)Br SEOBQCUWPSPHTB-UHFFFAOYSA-N 0.000 description 1
- BSVBQGMMJUBVOD-UHFFFAOYSA-N trisodium borate Chemical compound [Na+].[Na+].[Na+].[O-]B([O-])[O-] BSVBQGMMJUBVOD-UHFFFAOYSA-N 0.000 description 1
- KJIOQYGWTQBHNH-UHFFFAOYSA-N undecanol Chemical compound CCCCCCCCCCCO KJIOQYGWTQBHNH-UHFFFAOYSA-N 0.000 description 1
- LSGOVYNHVSXFFJ-UHFFFAOYSA-N vanadate(3-) Chemical compound [O-][V]([O-])([O-])=O LSGOVYNHVSXFFJ-UHFFFAOYSA-N 0.000 description 1
- 235000019871 vegetable fat Nutrition 0.000 description 1
- 235000019154 vitamin C Nutrition 0.000 description 1
- 239000011718 vitamin C Substances 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 239000010456 wollastonite Substances 0.000 description 1
- 229910052882 wollastonite Inorganic materials 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
- 239000001052 yellow pigment Substances 0.000 description 1
- 239000011592 zinc chloride Substances 0.000 description 1
- 235000005074 zinc chloride Nutrition 0.000 description 1
- XOOUIPVCVHRTMJ-UHFFFAOYSA-L zinc stearate Chemical compound [Zn+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O XOOUIPVCVHRTMJ-UHFFFAOYSA-L 0.000 description 1
- PICXIOQBANWBIZ-UHFFFAOYSA-N zinc;1-oxidopyridine-2-thione Chemical compound [Zn+2].[O-]N1C=CC=CC1=S.[O-]N1C=CC=CC1=S PICXIOQBANWBIZ-UHFFFAOYSA-N 0.000 description 1
- NDKWCCLKSWNDBG-UHFFFAOYSA-N zinc;dioxido(dioxo)chromium Chemical compound [Zn+2].[O-][Cr]([O-])(=O)=O NDKWCCLKSWNDBG-UHFFFAOYSA-N 0.000 description 1
- 239000004711 α-olefin Substances 0.000 description 1
- 239000002076 α-tocopherol Substances 0.000 description 1
- 235000004835 α-tocopherol Nutrition 0.000 description 1
- 239000011590 β-tocopherol Substances 0.000 description 1
- 235000007680 β-tocopherol Nutrition 0.000 description 1
- 239000002478 γ-tocopherol Substances 0.000 description 1
- QUEDXNHFTDJVIY-UHFFFAOYSA-N γ-tocopherol Chemical class OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1 QUEDXNHFTDJVIY-UHFFFAOYSA-N 0.000 description 1
- QUEDXNHFTDJVIY-DQCZWYHMSA-N γ-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1 QUEDXNHFTDJVIY-DQCZWYHMSA-N 0.000 description 1
- 239000002446 δ-tocopherol Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/10—Esters; Ether-esters
- C08K5/12—Esters; Ether-esters of cyclic polycarboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/20—Compounding polymers with additives, e.g. colouring
- C08J3/22—Compounding polymers with additives, e.g. colouring using masterbatch techniques
- C08J3/223—Packed additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/0008—Organic ingredients according to more than one of the "one dot" groups of C08K5/01 - C08K5/59
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K9/00—Use of pretreated ingredients
- C08K9/04—Ingredients treated with organic substances
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/40—Compounds of aluminium
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/40—Compounds of aluminium
- C09C1/42—Clays
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K15/00—Anti-oxidant compositions; Compositions inhibiting chemical change
- C09K15/04—Anti-oxidant compositions; Compositions inhibiting chemical change containing organic compounds
- C09K15/06—Anti-oxidant compositions; Compositions inhibiting chemical change containing organic compounds containing oxygen
- C09K15/08—Anti-oxidant compositions; Compositions inhibiting chemical change containing organic compounds containing oxygen containing a phenol or quinone moiety
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
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Description
本出願は、発明の名称「Pre−Exfoliated Layered Material」で201312月17日にファイルされた米国仮特許出願第61/916,950号に対する優先権およびその利益を主張し、その内容全体を本明細書に援用する。
天然または合成で変性または未変性の層状材料と、紫外線吸収剤、ヒンダードアミン系光安定剤、抗酸化物質、着色料、難燃剤、抗菌剤、脂肪酸添加剤からなる群から選択される1種または2種以上のプラスチック添加剤と、を混合し、
この混合物を押出すことを含む方法が開示される。
(2)ビス(2,2,6,6−テトラメチルピペリジン−4−イル)セバケート、
(3)ビス(1−アセトキシ−2,2,6,6−テトラメチルピペリジン−4−イル)セバケート、
(4)ビス(1,2,2,6,6−ペンタメチルピペリジン−4−イル)セバケート、
(5)ビス(1−シクロヘキシルオキシ−2,2,6,6−テトラメチルピペリジン−4−イル)セバケート、
(6)ビス(1−オクチルオキシ−2,2,6,6−テトラメチルピペリジン−4−イル)セバケート、
(7)ビス(1−アシル−2,2,6,6−テトラメチルピペリジン−4−イル)セバケート、
(8)ビス(1,2,2,6,6−ペンタメチル−4−ピペリジル)n−ブチル−3,5−ジ−tert−ブチル−4−ヒドロキシベンジルマロネート、
(9)2,4−ビス[(1−シクロヘキシルオキシ−2,2,6,6−テトラメチルピペリジン−4−イル)ブチルアミノ]−6−(2−ヒドロキシ−エチルアミノ−s−トリアジン、
(10)ビス(1−シクロヘキシルオキシ−2,2,6,6−テトラメチルピペリジン−4−イル)アジペート、
(11)2,4−ビス[(1−シクロヘキシルオキシ−2,2,6,6−ピペリジン−4−イル)ブチルアミノ]−6−クロロ−s−トリアジン、
(12)1−(2−ヒドロキシ−2−メチルプロポキシ)−4−ヒドロキシ−2,2,6,6−テトラメチルピペリジン、
(13)1−(2−ヒドロキシ−2−メチルプロポキシ)−4−オキソ−2,2,6,6−テトラメチルピペリジン、
(14)1−(2−ヒドロキシ−2−メチルプロポキシ)−4−オクタデカノイルオキシ−2,2,6,6−テトラメチルピペリジン、
(15)ビス(1−(2−ヒドロキシ−2−メチルプロポキシ)−2,2,6,6−テトラメチルピペリジン−4−イル)セバケート
(16)ビス(1−(2−ヒドロキシ−2−メチルプロポキシ)−2,2,6,6−テトラメチルピペリジン−4−イル)アジペート、
(17)2,4−ビス{N−[1−(2−ヒドロキシ−2−メチルプロポキシ)−2,2,6,6−テトラメチルピペリジン−4−イル]−N−ブチル−アミノ}−6−(2−ヒドロキシエチルアミノ)−s−トリアジン、
(18)4−ベンゾイル−2,2,6,6−テトラメチルピペリジン、
(19)ジ−(1,2,2,6,6−ペンタメチルピペリジン−4−イル)p−メトキシベンジリデンマロネート、
(20)2,2,6,6−テトラメチルピペリジン−4−イルオクタデカノエート、
(21)ビス(1−オクチルオキシ−2,2,6,6−テトラメチルピペリジル)スクシネート、
(22)1,2,2,6,6−ペンタメチル−4−アミノピペリジン、
(23)2−ウンデシル−7,7,9,9−テトラメチル−1−オキサ−3,8−ジアザ−4−オキソ−スピロ[4,5]デカン、
(24)トリス(2,2,6,6−テトラメチル−4−ピペリジル)ニトリロトリアセテート、
(25)トリス(2−ヒドロキシ−3−(アミノ−(2,2,6,6−テトラメチルピペリジン−4−イル)プロピル)ニトリロトリアセテート
(26)テトラキス(2,2,6,6−テトラメチル−4−ピペリジル)−1,2,3,4−ブタン−テトラカルボキシレート、
(27)テトラキス(1,2,2,6,6−ペンタメチル−4−ピペリジル)−1,2,3,4−ブタン−テトラカルボキシレート、
(28)1,1’−(1,2−エタンジイル)−ビス(3,3,5,5−テトラメチルピペラジノン)、
(29)3−n−オクチル−7,7,9,9−テトラメチル−1,3,8−トリアザスピロ[4.5]デカン−2,4−ジオン、
(30)8−アセチル−3−ドデシル−7,7,9,9−テトラメチル−1,3,8−トリアザスピロ[4.5]デカン−2,4−ジオン、
(31)3−ドデシル−1−(2,2,6,6−テトラメチル−4−ピペリジル)ピロリジン−2,5−ジオン、
(32)3−ドデシル−1−(1,2,2,6,6−ペンタメチル−4−ピペリジル)ピロリジン−2,5−ジオン、
(33)N,N’−ビス−ホルミル−N,N’−ビス(2,2,6,6−テトラメチル−4−ピペリジル)ヘキサメチレンジアミン、
(34)2,4−ビス[(1−シクロヘキシルオキシ−2,2,6,6−ピペリジン−4−イル)ブチルアミノ]−6−クロロ−s−トリアジンとN,N’−ビス(3−アミノプロピル)エチレンジアミン)との反応生成物、
(35)1−(2−ヒドロキシエチル)−2,2,6,6−テトラメチル−4−ヒドロキシピペリジンとコハク酸との縮合物、
(36)N,N’−ビス(2,2,6,6−テトラメチル−4−ピペリジル)−ヘキサメチレンジアミンと4−tert−オクチルアミノ−2,6−ジクロロ−1,3,5−トリアジンとの縮合物、
(37)N,N’−ビス(2,2,6,6−テトラメチル−4−ピペリジル)−ヘキサメチレンジアミンと4−シクロヘキシルアミノ−2,6−ジクロロ−1,3,5−トリアジンとの縮合物
(38)N,N’−ビス−(2,2,6,6−テトラメチル−4−ピペリジル)ヘキサメチレンジアミンと4−モルホリノ−2,6−ジクロロ−1,3,5−トリアジンとの縮合物、
(39)N,N’−ビス−(1,2,2,6,6−ペンタメチル−4−ピペリジル)ヘキサメチレンジアミンと4−モルホリノ−2,6−ジクロロ−1,3,5−トリアジンとの縮合物、
(40)2−クロロ−4,6−ビス(4−n−ブチルアミノ−2,2,6,6−テトラメチルピペリジル)−1,3,5−トリアジンと1,2−ビス(3−アミノプロピルアミノ)エタンとの縮合物、
(41)2−クロロ−4,6−ジ−(4−n−ブチルアミノ−1,2,2,6,6−ペンタメチルピペリジル)−1,3,5−トリアジンと1,2−ビス−(3−アミノプロピルアミノ)エタンとの縮合物、
(42)7,7,9,9−テトラメチル−2−シクロウンデシル−1−オキサ−3,8−ジアザ−4−オキソスピロ[4,5]デカンおよびエピクロロヒドリンとの反応生成物、
(43)ポリ[メチル,(3−オキシ−(2,2,6,6−テトラメチルピペリジン−4−イル)プロピル)]シロキサン、
CAS番号182635−99−0、
(44)無水マレイン酸−C18−C22−α−オレフィン−コポリマーと2,2,6,6−テトラメチル−4−アミノピペリジンとの反応生成物、
(45)2−クロロ−4,6−ビス(ジブチルアミノ)−s−トリアジンで末端キャップされた、4,4’−ヘキサメチレンビス(アミノ−2,2,6,6−テトラメチル−ピペリジン)と2,4−ジクロロ−6−[(2,2,6,6−テトラメチルピペリジン−4−イル)ブチルアミノ]−s−トリアジンとのオリゴマー縮合物、
(46)2−クロロ−4,6−ビス(ジブチルアミノ)−s−トリアジンで末端キャップされた、4,4’−ヘキサメチレンビス(アミノ−1,2,2,6,6−ペンタメチル−ピペリジン)と2,4−ジクロロ−6−[(1,2,2,6,6−ペンタメチルピペリジン−4−イル)ブチルアミノ]−s−トリアジンとのオリゴマー縮合物、
(47)2−クロロ−4,6−ビス(ジブチルアミノ)−s−トリアジンで末端キャップされた、4,4’−ヘキサメチレンビス(アミノ−1−プロポキシ−2,2,6,6−テトラ−メチルピペリジン)と2,4−ジクロロ−6−[(1−プロポキシ−2,2,6,6−テトラメチルピペリジン−4−イル)ブチルアミノ]−s−トリアジンとのオリゴマー縮合物、
(48)2−クロロ−4,6−ビス(ジブチルアミノ)−s−トリアジンで末端キャップされた、4,4’−ヘキサメチレンビス(アミノ−1−アシルオキシ−2,2,6,6−テトラ−メチルピペリジン)と2,4−ジクロロ−6−[(1−アシルオキシ−2,2,6,6−テトラメチルピペリジン−4−イル)ブチルアミノ]−s−トリアジンとのオリゴマー縮合物、
(49)1,2−ビス(3−アミノ−プロピルアミノ)エタンと塩化シアヌルとを反応させることによって得られる生成物と、(2,2,6,6−テトラメチルピペリジン−4−イル)ブチルアミンとを反応させることによって得られる生成物。
また、上述した化合物のいずれかの、立体障害のある、N−H、N−メチル、N−メトキシ、N−プロポキシ、N−オクチルオキシ、N−シクロヘキシルオキシ、N−アシルオキシ、N−(2−ヒドロキシ−2−メチルプロポキシ)アナログも含まれる。たとえば、N−HヒンダードアミンをN−メチルヒンダードアミンで置換するには、N−Hの代わりにN−メチルアナログを用いることになろう。
a)ラジカル重合(通常は高圧高温下)。
b)通常は、周期律表のIVb、Vb、VlbまたはVIII族の1種または2種以上の金属を含有する触媒を用いる触媒重合。これらの金属は通常、π配位またはσ配位した1種または2種以上の配位子、一般には酸化物、ハロゲン化物、アルコラート、エステル、エーテル、アミン、アルキル、アルケニルおよび/またはアリールを有する。これらの金属錯体は、遊離した形態であってもよいし、一般に活性化塩化マグネシウム、塩化チタン(III)、酸化アルミナまたは酸化ケイ素である基質上に固定されていてもよい。これらの触媒は、重合媒体に可溶であっても不溶であってもよい。触媒は、それ自体を重合時に用いることも可能であるし、一般に金属アルキル、金属水素化物、金属アルキルハライド、金属アルキルオキシドまたは金属アルキルオキサンである別の活性化剤を用いてもよい。前記金属は、周期律表のIa、IIaおよび/またはIIIa族の元素である。活性化剤は、別のエステル、エーテル、アミンまたはシリルエーテル基で、適宜修飾されていてもよい。これらの触媒系は通常、フィリップス、スタンダードオイルインディアナ、チグラー(−ナッタ)、TNZ(DuPont)、メタロセンまたはシングルサイト触媒(SSC)と称される。
1)エチレンおよびプロピレンなどのオレフィンモノマーのホモポリマーおよびコポリマーであるが、1−ブテン、1−ペンテン、1−ヘキセンまたは1−オクテンなど、より高次の1−オレフィンもある。たとえば、ポリエチレン、LDPE、LLDPE、HDPE、ポリプロピレン、エチレンおよびプロピレンのコポリマーなど。
2)ブタジエン、イソプレン、ノルボルネンなどの環状オレフィンなど、オレフィンモノマーとジオレフィンモノマーのホモポリマーおよびコポリマー。
3)1種または2種以上の1−オレフィンおよび/またはジオレフィンと、一酸化炭素および/または酢酸ビニル、ビニルケトン、スチレン、無水マレイン酸、塩化ビニルを含むがこれらに限定されるものではない他のビニルモノマーとのコポリマー。
4)ポリビニルアルコール。
5)ポリスチレン、スチレン−アクリロニトリルコポリマー、アクリロニトリル−ブタジエン−スチレンコポリマー、塩化ポリビニル、塩化ポリビニリデン、酢酸ポリビニル、ポリビニルブチラール、エチレン−ビニルアルコールコポリマー、ポリエチレンテレフタレート(PET)、ポリブチレンテレフタレート(PBT)、液晶ポリエステル(LCP)、ポリアセタール(たとえば、POM)、ポリアミド(PA)、ポリカーボネート、ポリウレタン、ポリフェニレンスルフィド(PPS)などの他の熱可塑性樹脂;これらの樹脂のうち2種類以上で形成されるポリマーブレンドまたはポリマー合金;ガラス繊維、炭素繊維、半炭化繊維、セルロース繊維およびガラスビーズ、難燃剤、発泡剤、抗菌剤、架橋剤、ポリオレフィン樹脂微粉末、ポリオレフィンワックス、エチレンビスアミドワックス、金属石鹸などのフィラーを、単独またはこれらの樹脂と併用して添加して得られる化合物。熱硬化性樹脂の例は、一方では、エポキシ樹脂、メラミン樹脂、不飽和ポリエステル樹脂などの熱硬化性樹脂を含むことが可能であり、ガラス繊維、炭素繊維、半炭化繊維、セルロース繊維、ガラスビーズ、難燃剤などのフィラーを、単独またはこれらの樹脂と併用して取り込んだ化合物も含むことが可能である。
ポリエチレンスクシネート、ポリブチレンスクシネート、ポリブチレンスクシネート/アジペート、ポリブチレンスクシネート/カーボネート、ポリブチレンスクシネート/テレフタレート、ポリカプロラクトン、ポリ(ヒドロキシアルカノエート)、ポリ3−ヒドロキシブチレート、ポリ乳酸、ポリエステルアミドあるいは、これらの材料と、天然スターチまたは化工スターチ、多糖類、リグニン、木粉、セルロースまたはキチンとのブレンドを含むが、これらに限定されるものではない、天然または合成由来の生分解性ポリマー。
前剥離させた、天然または合成で変性または未変性の層状材料と、
紫外線吸収剤、ヒンダードアミン系光安定剤、抗酸化物質、着色料、難燃剤、抗菌剤、脂肪酸添加剤と、
20重量%未満、15重量%未満、10重量%未満、5重量%未満、3重量%未満または2重量%未満の他の成分からなる群から選択される1種または2種以上のプラスチック添加剤と、からなる組成物も開示されている。
前剥離させた、天然または合成で変性または未変性の層状材料と、
紫外線吸収剤、ヒンダードアミン系光安定剤、抗酸化物質、着色料、難燃剤、抗菌剤、脂肪酸添加剤からなる群から選択される1種または2種以上のプラスチック添加剤と、からなる組成物も開示されている。
実施例1 前剥離させた変性モンモリロナイト
実施例2
Claims (10)
- 前剥離させた層状材料を調製するための方法であって、
天然または合成で、変性または未変性の層状材料と、紫外線吸収剤、ヒンダードアミン系光安定剤、抗酸化物質、着色料、難燃剤、抗菌剤、脂肪酸のアルカリ金属塩およびアルカリ土類金属塩の添加剤からなる群から選択される1種または2種以上のプラスチック添加剤と、を混合し、
前記混合物を、二軸スクリュー押出機を用いて押出して、前記前剥離させた層状材料を調製することを含み、
ここで、前記層状材料とプラスチック添加剤の総重量に対して、他の成分が20重量%未満存在し、そして前記前剥離させた層状材料は、前記変性または未変性の層状材料に比べて≧0.5nmの層間の拡大が生じている、
上記方法。 - 前記変性または未変性の層状材料は、層状シリケート、グラファイト、ヴァーティソール、層状複水酸化物、フラーレン、カーボンナノチューブ、シリカ、多面体オリゴマーシルセスキオキサン、ナノメタル、金属酸化物、金属有機構造体、ゼオライト、これらの混合物からなる群から選択される、請求項1に記載の方法。
- 前記変性または未変性の層状材料は、モンモリロナイト、ベントナイト、バイデライト、雲母、ヘクトライト、サポナイト、ノントロナイト、ソーコナイト、バーミキュライト、レディカイト、マガタイト、ケニヤアイト、ステベンサイト、ボルコンスコアイト、ハイドロタルサイト、イライト、カオリナイト、ウラストナイト、アタパルジャイト、セピオライト、ハロイサイト、タルク、シリカおよびこれらの混合物からなる群から選択される、請求項1に記載の方法。
- 前記混合物の前記押出しは、少なくとも1種の前記添加剤の融点より高い温度で実施される、請求項1に記載の方法。
- 前記1種または2種以上のプラスチック添加剤は、フェノール部分、ピペリジン部分、トリアゾール部分、トリアジン部分、ホスファイト部分またはホスフェート部分を含有する、請求項1に記載の方法。
- 前記1種または2種以上のプラスチック添加剤は、ヒドロキシフェニルベンゾトリアゾール系紫外線吸収剤、トリス−アリール−s−トリアジン系紫外線吸収剤、ヒンダードアミン系光安定剤、有機リン安定剤、ヒンダードフェノール系抗酸化物質からなる群から選択される、請求項1に記載の方法。
- 前記変性または未変性の層状材料の前記プラスチック添加剤に対する重量:重量比が、10:90から90:10、20:80から80:20、30:70から70:30、40:60から60:40または50:50から10:90である、請求項1に記載の方法。
- 前記前剥離させた層状材料には、≧1nm、≧1.5nmまたは≧2nmの層間の拡大が生じている、請求項1に記載の方法。
- 前記前剥離させた層状材料の前記層間は、≧3nmまたは≧3.5nmまで拡大される、請求項8に記載の方法。
- 前記層状材料とプラスチック添加剤の総重量に対して、15重量%未満、10重量%未満、5重量%未満、3重量%未満、2重量%未満または0重量%の他の成分が存在する、請求項1に記載の方法。
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WO2015094888A1 (en) | 2015-06-25 |
EP3083243A1 (en) | 2016-10-26 |
TW201609907A (zh) | 2016-03-16 |
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EP3083243A4 (en) | 2017-07-05 |
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