JP6280243B2 - 架橋組成物及びこれを含む化粧料組成物 - Google Patents
架橋組成物及びこれを含む化粧料組成物 Download PDFInfo
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- JP6280243B2 JP6280243B2 JP2016564963A JP2016564963A JP6280243B2 JP 6280243 B2 JP6280243 B2 JP 6280243B2 JP 2016564963 A JP2016564963 A JP 2016564963A JP 2016564963 A JP2016564963 A JP 2016564963A JP 6280243 B2 JP6280243 B2 JP 6280243B2
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- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/56—Organo-metallic compounds, i.e. organic compounds containing a metal-to-carbon bond
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L83/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon only; Compositions of derivatives of such polymers
- C08L83/04—Polysiloxanes
- C08L83/06—Polysiloxanes containing silicon bound to oxygen-containing groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L83/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon only; Compositions of derivatives of such polymers
- C08L83/14—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon only; Compositions of derivatives of such polymers in which at least two but not all the silicon atoms are connected by linkages other than oxygen atoms
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/10—General cosmetic use
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/594—Mixtures of polymers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/12—Polysiloxanes containing silicon bound to hydrogen
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/14—Polysiloxanes containing silicon bound to oxygen-containing groups
Description
(R4 3SiO1/2)(R4 2SiO2/2)a(R1R4SiO2/2)b(R4HSiO2/2)c(R2R4SiO2/2)d(R3R4SiO2/2)e(R4 3Si−O1/2)
式(I)中、R1及びR2のそれぞれは、独立に、水素原子又は置換若しくは非置換ヒドロカルビル基から選択される。R3は、水素原子又は少なくとも1個のカルボキシル基を有する基又はそれらの前駆体である。R4は、独立に選択された置換若しくは非置換ヒドロカルビル基である。更に、a≧0、b≧0、c≧1、d≧0、かつe≧1である。架橋剤は、少なくとも2個の脂肪族不飽和炭化水素基を有する。
架橋組成物
(R4 3SiO1/2)(R4 2SiO2/2)a(R1R4SiO2/2)b(R4HSiO2/2)c(R2R4SiO2/2)d(R3R4SiO2/2)e(R4 3Si−O1/2)
式(I)中、シロキシ単位は、下付き文字a、b、c、d、及びeにより表され、すなわち、括弧内の基は、上記及び本開示中に示すものとは異なる順序を含む任意の順序でシロキサン内に存在し得る。更に、これらの基はランダム化された状態又はブロック状態で存在し得る。
(R2R5SiO1/2)(SiO4/2)w(R2R5SiO1/2)、(R2R5SiO1/2)(SiO4/2)w(R2SiO2/2)x(R2R5SiO1/2)、
(R2R5SiO1/2)(R2SiO2/2)x(R2R5SiO1/2)、R3SiO1/2)(R2SiO2/2)x(R5RSiO2/2)y(R3SiO1/2)、(R3SiO1/2)(R2SiO2/2)x(R5RSiO2/2)y(RSiO3/2)z(R3SiO1/2)、及び(R3SiO1/2)(R2SiO2/2)x(R5RSiO2/2)y(SiO4/2)w(R3SiO1/2)が挙げられ、式中、w≧0、x≧0、y≧2、z≧0であり、R及びR5は上記のとおりのものである。
H2C=CHCH2O[C3H6O]gCH2CH=CH2、H2C=CHO[C3H6O]gCH=CH2、H2C=C(CH3)CH2O[C3H6O]gCH2C(CH3)=CH2、HC≡CCH2O[C3H6O]gCH2C≡CH、HC≡CC(CH3)2O[C3H6O]gC(CH3)2C≡CH、H2C=CHCH2O[C4H8O]hCH2CH=CH2、H2C=CHO[C4H8O]hCH=CH2、H2C=C(CH3)CH2O[C4H8O]hCH2C(CH3)=CH2、及びHC≡CCH2O[C4H8O]hCH2C≡CH、及びHC≡CC(CH3)2O[C4H8O]hC(CH3)2C≡CHが挙げられ、式中、g及びhのそれぞれは上記のとおりのものである。架橋剤は、様々なポリエーテルの混合物、すなわち、(B3)構成成分の混合物であってもよい。
架橋組成物の形成方法
化粧料組成物
化粧料組成物を形成する方法
実施例1:アリルコハク酸無水物(ASA)オルガノハイドロジェンシロキサン
実施例2:1−ヘキセンを用いるASAオルガノハイドロジェンシロキサン
実施例3:1−ヘキサデセンを用いるASAオルガノハイドロジェンシロキサン
実施例5:開環したASAエラストマーブレンド
実施例6:トリメチルシリルウンデシレナートエラストマーブレンド
実施例7:脱ブロック化したトリメチルシリルウンデシレナートエラストマーブレンド
Si−H中間体の調製
Me3SiO(Me2SiO)93(MeR1SiO)7(MeHSiO)3.9(MeR2SiO)4.1SiMe3
エラストマーゲルの調製
COOH−エラストマーの調製
フィルム形成ポリマー(トリメチルシロキシシリケート及びポリプロピルシルセスキオキサン)は、上記のものなどの任意のその他のフィルム形成剤により置き換えることができる。揮発性シリコーンオイル(カプリリルメチコン)は、処方6に記載のとおりの任意の「揮発性油」で置き換えることができる。顔料(酸化鉄)は、処方7に記載のとおりの任意のその他の顔料により置き換えることができる。
Claims (14)
- 架橋組成物であって、ヒドロシリル化触媒の存在下での、
A)以下の平均式(I)のシロキシ単位を含むオルガノハイドロジェンシロキサン
(R4 3SiO1/2)(R4 2SiO2/2)a(R1R4SiO2/2)b(R4HSiO2/2)c(R2R4SiO2/2)d(R3R4SiO2/2)e(R4 3Si−O1/2)
[式中、R1及びR2のそれぞれは、独立に選択された水素原子又は置換若しくは非置換ヒドロカルビル基であり、R3は、水素原子であるか、又は少なくとも1個のカルボキシル基を有する基又はそれらの前駆体であり、それぞれのR4は、独立に選択された置換若しくは非置換ヒドロカルビル基であり、a≧0、b≧0、c≧1、d≧0、かつe≧1である]、及び
B)少なくとも2個の脂肪族不飽和炭化水素基を有する架橋剤、
の反応生成物を含み、
但し、
R3が水素原子であるとき、前記架橋組成物が、C1)アリルコハク酸無水物(ASA)、トリメチルシリルウンデシレナート、又はこれらの組み合わせの更なる反応生成物を含み、
R3が少なくとも1種のカルボキシル基又はそれらの前駆体を有する基であるとき、前記架橋組成物が、C2)水、アルコール、又はこれらの組み合わせの更なる反応生成物を含む、架橋組成物。 - 化粧料組成物であって、
(I)架橋組成物であって、ヒドロシリル化触媒の存在下での、
A)以下の平均式(I)のシロキシ単位を含むオルガノハイドロジェンシロキサン
(R4 3SiO1/2)(R4 2SiO2/2)a(R1R4SiO2/2)b(R4HSiO2/2)c(R2R4SiO2/2)d(R3R4SiO2/2)e(R4 3SiO1/2)
[式中、R1及びR2のそれぞれは、独立に選択された水素原子又は置換若しくは非置換ヒドロカルビル基であり、R3は、水素原子であるか、又は少なくとも1個のカルボキシル基を有する基又はそれらの前駆体であり、それぞれのR4は、独立に選択された置換若しくは非置換ヒドロカルビル基であり、a≧0、b≧0、c≧1、d≧0、かつe≧1である]、及び
B)少なくとも2個の脂肪族不飽和炭化水素基を有する架橋剤、
の反応生成物を含む、架橋組成物と、
(II)少なくとも1種の化粧料構成成分とを、
場合により、化粧料的に許容され得る媒体中に含み、
但し、
R3が水素原子であるとき、前記架橋組成物が、C1)アリルコハク酸無水物(ASA)、トリメチルシリルウンデシレナート、又はこれらの組み合わせの更なる反応生成物を含み、
R3が少なくとも1種のカルボキシル基又はそれらの前駆体を有する基であるとき、前記架橋組成物が、C2)水、アルコール、又はこれらの組み合わせの更なる反応生成物を含む、化粧料組成物。 - R3が水素原子であり、前記架橋組成物が、
C1)アリルコハク酸無水物(ASA)、トリメチルシリルウンデシレナート、又はこれらの組み合わせの更なる反応生成物を含む、請求項1又は2に記載の組成物。 - i)構成成分C1)が、アリルコハク酸無水物(ASA)を含み、かつ前記架橋組成物が、D)水、アルコール、若しくはこれらの組み合わせの更なる反応生成物を含み、又は
ii)構成成分C1)が、トリメチルシリルウンデシレナートを含み、かつ前記架橋組成物が、D)アルコールの更なる反応生成物を含み、又は
iii)i)及びii)の両方である、請求項1に記載の組成物。 - R3が、少なくとも1種のカルボキシル基又はその前駆体であり、あるいはアリルコハク酸無水物(ASA)又はトリメチルシリルウンデシレナートの誘導体であり、前記架橋組成物が、C2)水、アルコール、又はこれらの組み合わせの更なる反応生成物を含む、請求項1又は2に記載の組成物。
- 構成成分B)が式(III):R5−Y−R5のものであり、R5が、2〜12個の炭素原子を有する一価の不飽和脂肪族炭化水素基であり、かつYが、二価有機基、二価シロキサン基、又は二価オルガノシロキサン基である、請求項1〜5のいずれか一項に記載の組成物。
- i)R3が、末端カルボキシル基を有し、又は
ii)R3が、無水物基若しくはキャップ化カルボキシル基から選択された末端カルボキシル基前駆体を有し、又は
iii)R3が、アリルコハク酸無水物(ASA)若しくはトリメチルシリルウンデシレナートの誘導体である、請求項1又は7に記載の組成物。 - i)a+b+c+d+eの合計が、4〜2,000から選択される整数であり、かつ/又は
ii)10≦a≦500、0≦b≦100、1≦c≦100、0≦d≦100、及び1≦e≦100であり、かつ/又は
iii)R1が、メチル基であり、R2が、1〜12個の炭素原子を有する脂肪族若しくは芳香族基であり、かつR4がR1である、請求項1〜8のいずれか一項に記載の組成物。 - パーソナルケア用、あるいはケラチン基質のケア用の、請求項1〜9のいずれか一項に記載の組成物の使用。
- 架橋組成物の形成方法であって、
A)以下の平均式(I)のシロキシ単位を含むオルガノハイドロジェンシロキサンを提供する工程と、
(R4 3SiO1/2)(R4 2SiO2/2)a(R1R4SiO2/2)b(R4HSiO2/2)c(R2R4SiO2/2)d(R3R4SiO2/2)e(R4 3Si−O1/2)
[式中、R1及びR2のそれぞれは、独立に選択された水素原子又は置換若しくは非置換ヒドロカルビル基であり、R3は、水素原子であるか、又は少なくとも1個のカルボキシル基を有する基又はそれらの前駆体であり、それぞれのR4は、独立に選択された置換若しくは非置換ヒドロカルビル基であり、a≧0、b≧0、c≧1、d≧0、かつe≧1である]
B)少なくとも2個の脂肪族不飽和炭化水素基を有する架橋剤を提供する工程と、
ヒドロシリル化触媒の存在下で構成成分A)及びB)を組み合わせて、前記架橋組成物を形成する工程と、を含み、
前記架橋組成物が、請求項1〜9のいずれか一項に記載のものである、架橋組成物の形成方法。 - R3が水素素原子であり、
C1)脂肪族不飽和炭化水素基及び少なくとも1種のカルボキシル基又はカルボキシル基前駆体を有する化合物、あるいはC1)アリルコハク酸無水物(ASA)、トリメチルシリルウンデシレナート、又はそれらの組み合わせを提供する工程と、
R3と、構成成分C1)とを反応させて、前記架橋組成物を更に形成させる工程と、を更に含む、請求項11に記載の方法。 - D)水、アルコール、又はこれらの組み合わせを提供する工程と、
前記架橋組成物と構成成分D)とを反応させて、前記架橋組成物を更に形成させる工程と、を更に含む、請求項12に記載の方法。 - R3が、少なくとも1種のカルボキシル基又はその前駆体であり、あるいはアリルコハク酸無水物(ASA)又はトリメチルシリルウンデシレナートの誘導体であり、
C2)水、アルコール、又はこれらの組み合わせを提供する工程と、
R3と、構成成分C2)とを反応させて、前記架橋組成物を更に形成させる工程と、を更に含む、請求項11に記載の方法。
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- 2015-04-24 CN CN201580021079.9A patent/CN106232100B/zh active Active
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CN106232100A (zh) | 2016-12-14 |
WO2015167963A1 (en) | 2015-11-05 |
US20170065514A1 (en) | 2017-03-09 |
US10357445B2 (en) | 2019-07-23 |
EP3113757A1 (en) | 2017-01-11 |
KR20160141863A (ko) | 2016-12-09 |
EP3113757B1 (en) | 2020-12-16 |
JP2017514944A (ja) | 2017-06-08 |
KR101902167B1 (ko) | 2018-10-01 |
BR112016025241B8 (pt) | 2022-03-29 |
CN106232100B (zh) | 2020-08-28 |
BR112016025241B1 (pt) | 2021-02-02 |
BR112016025241A2 (pt) | 2017-08-15 |
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