JP6267211B2 - 脱ホウ素化ｍｗｗゼオライトの後処理 - Google Patents

脱ホウ素化ｍｗｗゼオライトの後処理 Download PDF

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Publication number
JP6267211B2
JP6267211B2 JP2015537193A JP2015537193A JP6267211B2 JP 6267211 B2 JP6267211 B2 JP 6267211B2 JP 2015537193 A JP2015537193 A JP 2015537193A JP 2015537193 A JP2015537193 A JP 2015537193A JP 6267211 B2 JP6267211 B2 JP 6267211B2
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Prior art keywords
zeolitic material
iii
range
ppm
treatment
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Japanese (ja)
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JP2015532259A5 (OSRAM
JP2015532259A (ja
Inventor
パルフレスク，アンドライ−ニコラエ
ヤン，ジェフ
マウラー，シュテファン
ガープ，マヌエラ
ザイデル，カルシュテン
ガーラッハ，オルガ
ミュラー，ウルリヒ
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BASF SE
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BASF SE
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • C01B39/48—Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B01J2235/05—Nuclear magnetic resonance [NMR]
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B01J2235/10—Infrared [IR]
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B01J2235/15—X-ray diffraction
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7038—MWW-type, e.g. MCM-22, ERB-1, ITQ-1, PSH-3 or SSZ-25
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/70—Catalysts, in general, characterised by their form or physical properties characterised by their crystalline properties, e.g. semi-crystalline
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
    • C01B37/007—Borosilicates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/026—After-treatment
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/06—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis
    • C01B39/12—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis the replacing atoms being at least boron atoms
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/10—After treatment, characterised by the effect to be obtained
    • B01J2229/16—After treatment, characterised by the effect to be obtained to increase the Si/Al ratio; Dealumination
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/37—Acid treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/40—Special temperature treatment, i.e. other than just for template removal

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Catalysts (AREA)
JP2015537193A 2012-10-18 2013-10-09 脱ホウ素化ｍｗｗゼオライトの後処理 Active JP6267211B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP12189042.0 2012-10-18
EP12189042 2012-10-18
PCT/EP2013/071042 WO2014060261A1 (en) 2012-10-18 2013-10-09 Post-treatment of deboronated mww zeolite

Publications (3)

Publication Number Publication Date
JP2015532259A JP2015532259A (ja) 2015-11-09
JP2015532259A5 JP2015532259A5 (OSRAM) 2016-12-01
JP6267211B2 true JP6267211B2 (ja) 2018-01-24

Family

ID=47046432

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2015537193A Active JP6267211B2 (ja) 2012-10-18 2013-10-09 脱ホウ素化ｍｗｗゼオライトの後処理

Country Status (13)

Country Link
US (1) US10099933B2 (OSRAM)
EP (1) EP2909141B1 (OSRAM)
JP (1) JP6267211B2 (OSRAM)
KR (1) KR102184609B1 (OSRAM)
CN (1) CN104854028B (OSRAM)
BR (1) BR112015008390B1 (OSRAM)
ES (1) ES2620030T3 (OSRAM)
MX (1) MX355246B (OSRAM)
MY (1) MY169039A (OSRAM)
RU (1) RU2638851C2 (OSRAM)
SG (1) SG11201503019SA (OSRAM)
WO (1) WO2014060261A1 (OSRAM)
ZA (1) ZA201503155B (OSRAM)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102179936B1 (ko) 2012-10-18 2020-11-17 바스프 에스이 제올라이트 물질의 후처리
WO2015185633A1 (en) * 2014-06-06 2015-12-10 Basf Se Synthesis of a boron-containing zeolite with an mww framework structure
WO2016038030A1 (en) * 2014-09-09 2016-03-17 Basf Se A process for the preparation of an mww zeolitic material comprising boron and titanium
WO2016058541A1 (en) 2014-10-15 2016-04-21 Basf Se Solidothermal synthesis of zeolitic materials and zeolites obtained therefrom
KR102470492B1 (ko) * 2016-09-06 2022-11-23 바스프 에스이 Mww 골격 구조를 갖는 붕소 함유 제올라이트의 고체열 합성
RU2761301C2 (ru) * 2016-12-20 2021-12-07 Басф Се Применение кислотной обработки для снижения пластичности композиции, содержащей титансодержащий цеолитный материал, имеющий структурный тип mww
MY199941A (en) 2016-12-20 2023-11-30 Basf Se Process for preparing an extrudable composition comprising a titanium-containing zeolitic material, having framework type mww
CN110325497B (zh) 2017-02-28 2023-03-31 巴斯夫欧洲公司 制备不饱和醇的方法
US11224867B2 (en) * 2017-05-15 2022-01-18 Basf Corporation Process for preparing a zeolitic material having framework type AEI

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2445747A1 (fr) * 1979-01-05 1980-08-01 Armines Procede de fabrication de pieces en silicium nitrure
US4622166A (en) * 1982-03-17 1986-11-11 Mizusawa Kagaku Kogyo Kabushiki Kaisha Process for preparation of zeolite slurry excellent in static stability and dynamic stability
DE4207745A1 (de) * 1992-03-11 1993-09-16 Basf Ag Azofarbstoffe enthaltende molekularsiebe
AU2002248274A1 (en) 2000-12-22 2002-07-30 California Institute Of Technology Synthesis of molecular sieves by hydrothermal treatment with acid
JP4241068B2 (ja) * 2002-03-07 2009-03-18 昭和電工株式会社 Ｍｗｗ型ゼオライト物質の製造方法
US20090325790A1 (en) * 2004-06-17 2009-12-31 Yale University Size-controllable transition metal clusters in mcm-41 for improving chemical catalysis
CN100363259C (zh) * 2004-12-23 2008-01-23 中国科学院大连化学物理研究所 一种高硅mcm-22分子筛的制备方法
WO2008016456A2 (en) * 2006-07-28 2008-02-07 Exxonmobil Chemical Patents Inc. Molecular sieve composition (emm-10), its method of making, and use for hydrocarbon conversions
EP2025402A1 (en) * 2007-07-31 2009-02-18 Total Petrochemicals Research Feluy Phosphorus modified molecular sieves, their use in conversion of organics to olefins
US7737313B2 (en) * 2006-12-21 2010-06-15 Exxonmobil Chemical Patents Inc. Catalyst composition, the method of manufacturing, and the process of using thereof in hydrocarbon conversions
KR20110126598A (ko) * 2009-03-13 2011-11-23 스미또모 가가꾸 가부시끼가이샤 올레핀 옥사이드의 제조 방법
WO2012074033A1 (ja) * 2010-11-30 2012-06-07 住友化学株式会社 チタン含有珪素酸化物成形体の製造方法及びオキシラン化合物の製造方法
US9522390B2 (en) * 2010-12-10 2016-12-20 The Regents Of The University Of California Oxide materials and synthesis by fluoride/chloride anion promoted exfoliation

Also Published As

Publication number Publication date
ES2620030T3 (es) 2017-06-27
CN104854028B (zh) 2017-07-18
BR112015008390A2 (pt) 2017-08-08
US10099933B2 (en) 2018-10-16
RU2638851C2 (ru) 2017-12-18
MX2015004948A (es) 2016-01-20
WO2014060261A1 (en) 2014-04-24
BR112015008390B1 (pt) 2021-11-03
JP2015532259A (ja) 2015-11-09
CN104854028A (zh) 2015-08-19
MY169039A (en) 2019-02-07
EP2909141B1 (en) 2016-12-14
SG11201503019SA (en) 2015-05-28
US20150329368A1 (en) 2015-11-19
KR20150074076A (ko) 2015-07-01
KR102184609B1 (ko) 2020-12-01
RU2015118225A (ru) 2016-12-10
ZA201503155B (en) 2017-11-29
MX355246B (es) 2018-04-11
EP2909141A1 (en) 2015-08-26

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