MX2015004948A - Postratamiento de zeolita beta desboronada mww. - Google Patents

Postratamiento de zeolita beta desboronada mww.

Info

Publication number
MX2015004948A
MX2015004948A MX2015004948A MX2015004948A MX2015004948A MX 2015004948 A MX2015004948 A MX 2015004948A MX 2015004948 A MX2015004948 A MX 2015004948A MX 2015004948 A MX2015004948 A MX 2015004948A MX 2015004948 A MX2015004948 A MX 2015004948A
Authority
MX
Mexico
Prior art keywords
zeolitic material
post
treatment
framework structure
mww zeolite
Prior art date
Application number
MX2015004948A
Other languages
English (en)
Other versions
MX355246B (es
Inventor
Manuela Gaab
Stefan Maurer
Ulrich Müller
Jeff Yang
Karsten Seidel
Andrei-Nicolae Parvulescu
Olga Gerlach
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of MX2015004948A publication Critical patent/MX2015004948A/es
Publication of MX355246B publication Critical patent/MX355246B/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • C01B39/48—Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7038—MWW-type, e.g. MCM-22, ERB-1, ITQ-1, PSH-3 or SSZ-25
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/30—Catalysts, in general, characterised by their form or physical properties characterised by their physical properties
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
    • C01B37/007—Borosilicates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/026—After-treatment
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/06—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis
    • C01B39/12—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis the replacing atoms being at least boron atoms
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/10—After treatment, characterised by the effect to be obtained
    • B01J2229/16—After treatment, characterised by the effect to be obtained to increase the Si/Al ratio; Dealumination
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/37—Acid treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/40—Special temperature treatment, i.e. other than just for template removal

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Catalysts (AREA)

Abstract

Un proceso para el postratamiento de un material zeolítico que tiene una estructura marco MWW, que comprende (i) brindar un material zeolítico que tiene una estructura marco MVVW, en donde la estructura marco del material zeolítico comprende X2O3 e YO2, en donde Y es un elemento tetravalente y X es un elemento trivalente y en donde la relación molar X2O3: YO2 es mayor que 0,02 1; (ii) tratar el material zeolítico proporcionado en (i) con un sistema solvente líquido obteniendo así un material zeolítico que tiene una relación molar X2O3: YO2 de a lo sumo 0,02: 1 y al menos separar parcialmente el material zeolítico del sistema solvente líquido; (iii) tratar el material zeolítico obtenido de (ii) con un sistema acuoso líquido que tiene un pH en el rango de 5,5 a 8 y una temperatura de al menos 75 °C.
MX2015004948A 2012-10-18 2013-10-09 Postratamiento de zeolita desboronada mww. MX355246B (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP12189042 2012-10-18
PCT/EP2013/071042 WO2014060261A1 (en) 2012-10-18 2013-10-09 Post-treatment of deboronated mww zeolite

Publications (2)

Publication Number Publication Date
MX2015004948A true MX2015004948A (es) 2016-01-20
MX355246B MX355246B (es) 2018-04-11

Family

ID=47046432

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2015004948A MX355246B (es) 2012-10-18 2013-10-09 Postratamiento de zeolita desboronada mww.

Country Status (13)

Country Link
US (1) US10099933B2 (es)
EP (1) EP2909141B1 (es)
JP (1) JP6267211B2 (es)
KR (1) KR102184609B1 (es)
CN (1) CN104854028B (es)
BR (1) BR112015008390B1 (es)
ES (1) ES2620030T3 (es)
MX (1) MX355246B (es)
MY (1) MY169039A (es)
RU (1) RU2638851C2 (es)
SG (1) SG11201503019SA (es)
WO (1) WO2014060261A1 (es)
ZA (1) ZA201503155B (es)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2637021C2 (ru) 2012-10-18 2017-11-29 Басф Се Последующая обработка цеолитного материала
WO2015185633A1 (en) * 2014-06-06 2015-12-10 Basf Se Synthesis of a boron-containing zeolite with an mww framework structure
EP3191404B1 (en) * 2014-09-09 2019-02-20 Basf Se A process for the preparation of an mww zeolitic material comprising boron and titanium
KR20170070052A (ko) 2014-10-15 2017-06-21 바스프 에스이 제올라이트 물질의 고체열 합성 및 이로부터 수득한 제올라이트
EP3509991B1 (en) * 2016-09-06 2021-12-01 Basf Se Solidothermal synthesis of a boron-containing zeolite with an mww framework structure
BR112019010916B1 (pt) 2016-12-20 2023-03-28 Basf Se Processo para preparar uma composição, composição extrudável, usos de uma composição extrudável e de uma moldagem, e, moldagem.
BR112019011059B1 (pt) 2016-12-20 2022-08-09 Basf Se Usos de um material zeolítico contendo titânio tratado com ácido e de um óxido de polietileno
WO2018158244A1 (en) 2017-02-28 2018-09-07 Basf Se Process for preparing an unsaturated alcohol
WO2018210809A1 (en) * 2017-05-15 2018-11-22 Basf Se A process for preparing a zeolitic material having framework type aei

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2445747A1 (fr) * 1979-01-05 1980-08-01 Armines Procede de fabrication de pieces en silicium nitrure
US4622166A (en) * 1982-03-17 1986-11-11 Mizusawa Kagaku Kogyo Kabushiki Kaisha Process for preparation of zeolite slurry excellent in static stability and dynamic stability
DE4207745A1 (de) * 1992-03-11 1993-09-16 Basf Ag Azofarbstoffe enthaltende molekularsiebe
AU2002248274A1 (en) 2000-12-22 2002-07-30 California Institute Of Technology Synthesis of molecular sieves by hydrothermal treatment with acid
JP4241068B2 (ja) * 2002-03-07 2009-03-18 昭和電工株式会社 Ｍｗｗ型ゼオライト物質の製造方法
US20090325790A1 (en) * 2004-06-17 2009-12-31 Yale University Size-controllable transition metal clusters in mcm-41 for improving chemical catalysis
CN100363259C (zh) * 2004-12-23 2008-01-23 中国科学院大连化学物理研究所 一种高硅mcm-22分子筛的制备方法
KR101044495B1 (ko) * 2006-07-28 2011-06-27 엑손모빌 케미칼 패턴츠 인코포레이티드 분자체 조성물(ｅｍｍ-10), 이의 제조 방법, 및 탄화수소 전환에 있어서의 용도
EP2025402A1 (en) * 2007-07-31 2009-02-18 Total Petrochemicals Research Feluy Phosphorus modified molecular sieves, their use in conversion of organics to olefins
US7737313B2 (en) * 2006-12-21 2010-06-15 Exxonmobil Chemical Patents Inc. Catalyst composition, the method of manufacturing, and the process of using thereof in hydrocarbon conversions
EP2406241A2 (en) * 2009-03-13 2012-01-18 Sumitomo Chemical Company, Limited Method for producing olefin oxide
WO2012074033A1 (ja) * 2010-11-30 2012-06-07 住友化学株式会社 チタン含有珪素酸化物成形体の製造方法及びオキシラン化合物の製造方法
US9522390B2 (en) * 2010-12-10 2016-12-20 The Regents Of The University Of California Oxide materials and synthesis by fluoride/chloride anion promoted exfoliation

Also Published As

Publication number Publication date
MX355246B (es) 2018-04-11
CN104854028B (zh) 2017-07-18
ES2620030T3 (es) 2017-06-27
JP2015532259A (ja) 2015-11-09
RU2015118225A (ru) 2016-12-10
ZA201503155B (en) 2017-11-29
EP2909141A1 (en) 2015-08-26
JP6267211B2 (ja) 2018-01-24
MY169039A (en) 2019-02-07
US20150329368A1 (en) 2015-11-19
BR112015008390A2 (pt) 2017-08-08
EP2909141B1 (en) 2016-12-14
SG11201503019SA (en) 2015-05-28
WO2014060261A1 (en) 2014-04-24
KR102184609B1 (ko) 2020-12-01
RU2638851C2 (ru) 2017-12-18
US10099933B2 (en) 2018-10-16
BR112015008390B1 (pt) 2021-11-03
KR20150074076A (ko) 2015-07-01
CN104854028A (zh) 2015-08-19

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