JP6114648B2 - 粘着性組成物、粘着剤および粘着シート - Google Patents
粘着性組成物、粘着剤および粘着シート Download PDFInfo
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- JP6114648B2 JP6114648B2 JP2013137538A JP2013137538A JP6114648B2 JP 6114648 B2 JP6114648 B2 JP 6114648B2 JP 2013137538 A JP2013137538 A JP 2013137538A JP 2013137538 A JP2013137538 A JP 2013137538A JP 6114648 B2 JP6114648 B2 JP 6114648B2
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- Prior art keywords
- pressure
- sensitive adhesive
- meth
- monomer
- acrylate
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- 239000000853 adhesive Substances 0.000 title claims description 84
- 230000001070 adhesive effect Effects 0.000 title claims description 84
- 239000000203 mixture Substances 0.000 title claims description 70
- 239000004820 Pressure-sensitive adhesive Substances 0.000 claims description 139
- 239000000178 monomer Substances 0.000 claims description 101
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims description 94
- 229920000642 polymer Polymers 0.000 claims description 84
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 claims description 80
- 239000010410 layer Substances 0.000 claims description 37
- 239000003431 cross linking reagent Substances 0.000 claims description 32
- 239000012948 isocyanate Substances 0.000 claims description 32
- 150000002513 isocyanates Chemical class 0.000 claims description 32
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 29
- 239000006087 Silane Coupling Agent Substances 0.000 claims description 27
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 claims description 26
- 239000012790 adhesive layer Substances 0.000 claims description 23
- 125000003118 aryl group Chemical group 0.000 claims description 22
- 239000000463 material Substances 0.000 claims description 22
- 238000012360 testing method Methods 0.000 claims description 18
- 125000003396 thiol group Chemical group [H]S* 0.000 claims description 16
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- 238000003860 storage Methods 0.000 claims description 9
- 125000004122 cyclic group Chemical group 0.000 claims description 4
- DVKJHBMWWAPEIU-UHFFFAOYSA-N toluene 2,4-diisocyanate Chemical class CC1=CC=C(N=C=O)C=C1N=C=O DVKJHBMWWAPEIU-UHFFFAOYSA-N 0.000 claims description 4
- 125000000094 2-phenylethyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])C([H])([H])* 0.000 claims description 3
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- -1 trimethylol propane modified tolylene diisocyanate Chemical class 0.000 description 55
- 238000000576 coating method Methods 0.000 description 27
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- 238000005259 measurement Methods 0.000 description 23
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- 238000000034 method Methods 0.000 description 10
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- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 8
- 125000000217 alkyl group Chemical group 0.000 description 8
- 125000004432 carbon atom Chemical group C* 0.000 description 8
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- 125000000524 functional group Chemical group 0.000 description 7
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- ZFSLODLOARCGLH-UHFFFAOYSA-N isocyanuric acid Chemical compound OC1=NC(O)=NC(O)=N1 ZFSLODLOARCGLH-UHFFFAOYSA-N 0.000 description 7
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- 229920000139 polyethylene terephthalate Polymers 0.000 description 7
- 239000005020 polyethylene terephthalate Substances 0.000 description 7
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- 238000011282 treatment Methods 0.000 description 7
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 6
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- IQPQWNKOIGAROB-UHFFFAOYSA-N isocyanate group Chemical group [N-]=C=O IQPQWNKOIGAROB-UHFFFAOYSA-N 0.000 description 6
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- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 5
- 125000005370 alkoxysilyl group Chemical group 0.000 description 5
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- PJXISJQVUVHSOJ-UHFFFAOYSA-N indium(iii) oxide Chemical compound [O-2].[O-2].[O-2].[In+3].[In+3] PJXISJQVUVHSOJ-UHFFFAOYSA-N 0.000 description 5
- 239000000123 paper Substances 0.000 description 5
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- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 4
- TXBCBTDQIULDIA-UHFFFAOYSA-N 2-[[3-hydroxy-2,2-bis(hydroxymethyl)propoxy]methyl]-2-(hydroxymethyl)propane-1,3-diol Chemical compound OCC(CO)(CO)COCC(CO)(CO)CO TXBCBTDQIULDIA-UHFFFAOYSA-N 0.000 description 4
- UUEWCQRISZBELL-UHFFFAOYSA-N 3-trimethoxysilylpropane-1-thiol Chemical compound CO[Si](OC)(OC)CCCS UUEWCQRISZBELL-UHFFFAOYSA-N 0.000 description 4
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 4
- BAPJBEWLBFYGME-UHFFFAOYSA-N Methyl acrylate Chemical compound COC(=O)C=C BAPJBEWLBFYGME-UHFFFAOYSA-N 0.000 description 4
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- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 4
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- KCTAWXVAICEBSD-UHFFFAOYSA-N prop-2-enoyloxy prop-2-eneperoxoate Chemical compound C=CC(=O)OOOC(=O)C=C KCTAWXVAICEBSD-UHFFFAOYSA-N 0.000 description 4
- 229920005989 resin Polymers 0.000 description 4
- 239000011347 resin Substances 0.000 description 4
- OMIGHNLMNHATMP-UHFFFAOYSA-N 2-hydroxyethyl prop-2-enoate Chemical compound OCCOC(=O)C=C OMIGHNLMNHATMP-UHFFFAOYSA-N 0.000 description 3
- SXIFAEWFOJETOA-UHFFFAOYSA-N 4-hydroxy-butyl Chemical group [CH2]CCCO SXIFAEWFOJETOA-UHFFFAOYSA-N 0.000 description 3
- 229920002799 BoPET Polymers 0.000 description 3
- 229920002284 Cellulose triacetate Polymers 0.000 description 3
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 239000004698 Polyethylene Substances 0.000 description 3
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- 239000004372 Polyvinyl alcohol Substances 0.000 description 3
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
- NNLVGZFZQQXQNW-ADJNRHBOSA-N [(2r,3r,4s,5r,6s)-4,5-diacetyloxy-3-[(2s,3r,4s,5r,6r)-3,4,5-triacetyloxy-6-(acetyloxymethyl)oxan-2-yl]oxy-6-[(2r,3r,4s,5r,6s)-4,5,6-triacetyloxy-2-(acetyloxymethyl)oxan-3-yl]oxyoxan-2-yl]methyl acetate Chemical compound O([C@@H]1O[C@@H]([C@H]([C@H](OC(C)=O)[C@H]1OC(C)=O)O[C@H]1[C@@H]([C@@H](OC(C)=O)[C@H](OC(C)=O)[C@@H](COC(C)=O)O1)OC(C)=O)COC(=O)C)[C@@H]1[C@@H](COC(C)=O)O[C@@H](OC(C)=O)[C@H](OC(C)=O)[C@H]1OC(C)=O NNLVGZFZQQXQNW-ADJNRHBOSA-N 0.000 description 3
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- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 3
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- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 3
- 229920000570 polyether Polymers 0.000 description 3
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- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 description 3
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- CPUDPFPXCZDNGI-UHFFFAOYSA-N triethoxy(methyl)silane Chemical compound CCO[Si](C)(OCC)OCC CPUDPFPXCZDNGI-UHFFFAOYSA-N 0.000 description 3
- 239000012956 1-hydroxycyclohexylphenyl-ketone Substances 0.000 description 2
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- OZAIFHULBGXAKX-UHFFFAOYSA-N 2-(2-cyanopropan-2-yldiazenyl)-2-methylpropanenitrile Chemical compound N#CC(C)(C)N=NC(C)(C)C#N OZAIFHULBGXAKX-UHFFFAOYSA-N 0.000 description 2
- 125000000954 2-hydroxyethyl group Chemical group [H]C([*])([H])C([H])([H])O[H] 0.000 description 2
- NJWGQARXZDRHCD-UHFFFAOYSA-N 2-methylanthraquinone Chemical compound C1=CC=C2C(=O)C3=CC(C)=CC=C3C(=O)C2=C1 NJWGQARXZDRHCD-UHFFFAOYSA-N 0.000 description 2
- HPSGLFKWHYAKSF-UHFFFAOYSA-N 2-phenylethyl prop-2-enoate Chemical compound C=CC(=O)OCCC1=CC=CC=C1 HPSGLFKWHYAKSF-UHFFFAOYSA-N 0.000 description 2
- LOOUJXUUGIUEBC-UHFFFAOYSA-N 3-(dimethoxymethylsilyl)propane-1-thiol Chemical compound COC(OC)[SiH2]CCCS LOOUJXUUGIUEBC-UHFFFAOYSA-N 0.000 description 2
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- MQDJYUACMFCOFT-UHFFFAOYSA-N bis[2-(1-hydroxycyclohexyl)phenyl]methanone Chemical compound C=1C=CC=C(C(=O)C=2C(=CC=CC=2)C2(O)CCCCC2)C=1C1(O)CCCCC1 MQDJYUACMFCOFT-UHFFFAOYSA-N 0.000 description 2
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J133/00—Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Adhesives based on derivatives of such polymers
- C09J133/04—Homopolymers or copolymers of esters
- C09J133/06—Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, the oxygen atom being present only as part of the carboxyl radical
- C09J133/062—Copolymers with monomers not covered by C09J133/06
- C09J133/066—Copolymers with monomers not covered by C09J133/06 containing -OH groups
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J7/00—Adhesives in the form of films or foils
- C09J7/20—Adhesives in the form of films or foils characterised by their carriers
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J9/00—Adhesives characterised by their physical nature or the effects produced, e.g. glue sticks
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- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B5/00—Optical elements other than lenses
- G02B5/30—Polarising elements
Landscapes
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- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
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- Adhesives Or Adhesive Processes (AREA)
- Adhesive Tapes (AREA)
- Compositions Of Macromolecular Compounds (AREA)
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| TW103118215A TWI636106B (zh) | 2013-06-28 | 2014-05-26 | Adhesive composition, adhesive and adhesive sheet |
| KR1020140065714A KR102281768B1 (ko) | 2013-06-28 | 2014-05-30 | 점착성 조성물, 점착제 및 점착시트 |
| CN201410301348.4A CN104250524B (zh) | 2013-06-28 | 2014-06-27 | 粘接性组合物、粘接剂以及粘接片 |
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| JP6463192B2 (ja) * | 2015-03-03 | 2019-01-30 | リンテック株式会社 | 粘着剤層付き光学フィルム |
| JP6438817B2 (ja) * | 2015-03-27 | 2018-12-19 | リンテック株式会社 | 粘着性組成物、粘着剤、粘着シートおよび粘着剤層付き光学フィルム |
| JP6554344B2 (ja) * | 2015-06-30 | 2019-07-31 | リンテック株式会社 | 粘着シートおよび表示体 |
| KR101780547B1 (ko) * | 2015-07-31 | 2017-09-22 | 삼성에스디아이 주식회사 | 편광판용 점착 필름, 이를 포함하는 편광판 및 이를 포함하는 광학표시장치 |
| TWI562892B (en) * | 2015-10-28 | 2016-12-21 | Sumika Technology Co Ltd | Touch display device |
| TWI642742B (zh) | 2015-11-24 | 2018-12-01 | 三星Ｓｄｉ股份有限公司 | 偏光板用黏著膜、包括其的偏光板及光學顯示器 |
| KR101908175B1 (ko) * | 2015-11-24 | 2018-10-15 | 삼성에스디아이 주식회사 | 편광판용 점착 필름, 이를 포함하는 편광판 및 디스플레이 장치 |
| CN107163867B (zh) * | 2016-03-07 | 2021-10-26 | 日东电工株式会社 | 光学用粘合片、带粘合剂层的偏振膜和液晶显示装置 |
| TW201825583A (zh) * | 2016-11-16 | 2018-07-16 | 日商東亞合成股份有限公司 | 樹脂片材製造用硬化型組成物 |
| JP7112828B2 (ja) * | 2016-12-16 | 2022-08-04 | 大王製紙株式会社 | 粘着シート |
| KR102158871B1 (ko) * | 2017-07-04 | 2020-09-22 | 삼성에스디아이 주식회사 | 편광판용 점착제 조성물, 이로부터 제조된 편광판용 점착필름, 이를 포함하는 편광판 및 이를 포함하는 광학표시장치 |
| CN109237434A (zh) * | 2018-09-29 | 2019-01-18 | 江苏锐阳照明电器设备有限公司 | 一种矿用照明灯具防尘涂层 |
| CN110387193A (zh) * | 2019-08-09 | 2019-10-29 | 苏州凡赛特材料科技有限公司 | 一种纳米金属导电膜用光学胶黏剂组合物及其胶膜 |
| KR102635555B1 (ko) * | 2021-06-18 | 2024-02-08 | (주)이녹스첨단소재 | 디스플레이용 점착시트 및 이를 포함하는 디스플레이 |
| CN113956423B (zh) * | 2021-08-19 | 2023-05-26 | Oppo广东移动通信有限公司 | 组合物、聚合物分散液晶、薄膜和电子设备 |
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| CN102181244B (zh) * | 2009-12-29 | 2014-02-12 | 第一毛织株式会社 | 粘结剂及其制法、其组合物、粘结剂层制法和光学元件 |
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| KR101839173B1 (ko) * | 2010-10-12 | 2018-03-15 | 스미또모 가가꾸 가부시키가이샤 | 광학 부재용 점착제 조성물, 광학 부재용 점착제, 점착제 부착 광학부재 및 화상 표시장치 |
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| CN104250524B (zh) | 2020-02-21 |
| TW201504376A (zh) | 2015-02-01 |
| JP2015010192A (ja) | 2015-01-19 |
| CN104250524A (zh) | 2014-12-31 |
| KR102281768B1 (ko) | 2021-07-27 |
| KR20150002459A (ko) | 2015-01-07 |
| TWI636106B (zh) | 2018-09-21 |
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