JP6064901B2 - 縦型遠心薄膜蒸発器及び単量体の精製方法 - Google Patents
縦型遠心薄膜蒸発器及び単量体の精製方法 Download PDFInfo
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- JP6064901B2 JP6064901B2 JP2013508703A JP2013508703A JP6064901B2 JP 6064901 B2 JP6064901 B2 JP 6064901B2 JP 2013508703 A JP2013508703 A JP 2013508703A JP 2013508703 A JP2013508703 A JP 2013508703A JP 6064901 B2 JP6064901 B2 JP 6064901B2
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- wiper
- fixing support
- thin film
- cylindrical body
- film evaporator
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- 239000010409 thin film Substances 0.000 title claims description 40
- 239000000178 monomer Substances 0.000 title claims description 28
- 238000000746 purification Methods 0.000 title claims description 13
- 238000000034 method Methods 0.000 title claims description 11
- 239000007788 liquid Substances 0.000 claims description 66
- 230000002093 peripheral effect Effects 0.000 claims description 34
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims description 13
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 description 29
- 239000000126 substance Substances 0.000 description 20
- 238000001704 evaporation Methods 0.000 description 17
- 230000008020 evaporation Effects 0.000 description 15
- 238000009835 boiling Methods 0.000 description 13
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 10
- 239000000463 material Substances 0.000 description 10
- 229920002554 vinyl polymer Polymers 0.000 description 10
- 229940044192 2-hydroxyethyl methacrylate Drugs 0.000 description 9
- WOBHKFSMXKNTIM-UHFFFAOYSA-N Hydroxyethyl methacrylate Chemical compound CC(=C)C(=O)OCCO WOBHKFSMXKNTIM-UHFFFAOYSA-N 0.000 description 9
- -1 polytetrafluoroethylene Polymers 0.000 description 9
- 230000014759 maintenance of location Effects 0.000 description 6
- 239000010408 film Substances 0.000 description 5
- 238000006116 polymerization reaction Methods 0.000 description 5
- 238000007711 solidification Methods 0.000 description 4
- 230000008023 solidification Effects 0.000 description 4
- 150000001252 acrylic acid derivatives Chemical class 0.000 description 3
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 3
- 239000011521 glass Substances 0.000 description 3
- 239000012535 impurity Substances 0.000 description 3
- 239000010935 stainless steel Substances 0.000 description 3
- 229910001220 stainless steel Inorganic materials 0.000 description 3
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 description 2
- 229910000975 Carbon steel Inorganic materials 0.000 description 2
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
- 239000010962 carbon steel Substances 0.000 description 2
- 230000015556 catabolic process Effects 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 238000009833 condensation Methods 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- 239000002826 coolant Substances 0.000 description 2
- 238000006731 degradation reaction Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 2
- 238000012423 maintenance Methods 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- DTGKSKDOIYIVQL-WEDXCCLWSA-N (+)-borneol Chemical group C1C[C@@]2(C)[C@@H](O)C[C@@H]1C2(C)C DTGKSKDOIYIVQL-WEDXCCLWSA-N 0.000 description 1
- MJYFYGVCLHNRKB-UHFFFAOYSA-N 1,1,2-trifluoroethyl 2-methylprop-2-enoate Chemical compound CC(=C)C(=O)OC(F)(F)CF MJYFYGVCLHNRKB-UHFFFAOYSA-N 0.000 description 1
- 229940058015 1,3-butylene glycol Drugs 0.000 description 1
- 125000000954 2-hydroxyethyl group Chemical group [H]C([*])([H])C([H])([H])O[H] 0.000 description 1
- 125000004200 2-methoxyethyl group Chemical group [H]C([H])([H])OC([H])([H])C([H])([H])* 0.000 description 1
- 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 description 1
- YJWZCUHMWDKUES-UHFFFAOYSA-N 3-chloro-n,n-dimethyl-3-phenylpropan-1-amine Chemical class CN(C)CCC(Cl)C1=CC=CC=C1 YJWZCUHMWDKUES-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- 239000004743 Polypropylene Substances 0.000 description 1
- ZJCCRDAZUWHFQH-UHFFFAOYSA-N Trimethylolpropane Chemical compound CCC(CO)(CO)CO ZJCCRDAZUWHFQH-UHFFFAOYSA-N 0.000 description 1
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 description 1
- MZVQCMJNVPIDEA-UHFFFAOYSA-N [CH2]CN(CC)CC Chemical group [CH2]CN(CC)CC MZVQCMJNVPIDEA-UHFFFAOYSA-N 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 125000001797 benzyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])* 0.000 description 1
- 235000019437 butane-1,3-diol Nutrition 0.000 description 1
- 239000003990 capacitor Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 125000000113 cyclohexyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C1([H])[H] 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 150000005690 diesters Chemical class 0.000 description 1
- 125000002147 dimethylamino group Chemical group [H]C([H])([H])N(*)C([H])([H])[H] 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 125000003055 glycidyl group Chemical group C(C1CO1)* 0.000 description 1
- XXMIOPMDWAUFGU-UHFFFAOYSA-N hexane-1,6-diol Chemical compound OCCCCCCO XXMIOPMDWAUFGU-UHFFFAOYSA-N 0.000 description 1
- 239000011346 highly viscous material Substances 0.000 description 1
- 230000001939 inductive effect Effects 0.000 description 1
- 125000000959 isobutyl group Chemical group [H]C([H])([H])C([H])(C([H])([H])[H])C([H])([H])* 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 125000004108 n-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- SNMVRZFUUCLYTO-UHFFFAOYSA-N n-propyl chloride Chemical class CCCCl SNMVRZFUUCLYTO-UHFFFAOYSA-N 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- 229920001748 polybutylene Polymers 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 1
- 239000004810 polytetrafluoroethylene Substances 0.000 description 1
- 125000004079 stearyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 description 1
- ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/22—Evaporating by bringing a thin layer of the liquid into contact with a heated surface
- B01D1/222—In rotating vessels; vessels with movable parts
- B01D1/223—In rotating vessels; vessels with movable parts containing a rotor
- B01D1/225—In rotating vessels; vessels with movable parts containing a rotor with blades or scrapers
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/58—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2012060209 | 2012-03-16 | ||
| JP2012060209 | 2012-03-16 | ||
| PCT/JP2013/052558 WO2013136874A1 (ja) | 2012-03-16 | 2013-02-05 | 縦型遠心薄膜蒸発器及び単量体の精製方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPWO2013136874A1 JPWO2013136874A1 (ja) | 2015-08-03 |
| JP6064901B2 true JP6064901B2 (ja) | 2017-01-25 |
Family
ID=49160793
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2013508703A Active JP6064901B2 (ja) | 2012-03-16 | 2013-02-05 | 縦型遠心薄膜蒸発器及び単量体の精製方法 |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US9981201B2 (zh) |
| JP (1) | JP6064901B2 (zh) |
| KR (1) | KR101604940B1 (zh) |
| CN (1) | CN104168972B (zh) |
| WO (1) | WO2013136874A1 (zh) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2014018708A (ja) * | 2012-07-13 | 2014-02-03 | Osaka Organic Chem Ind Ltd | 縦型薄膜式蒸留器および縦型薄膜式蒸留器用ワイパー |
| CN105884963B (zh) * | 2014-12-31 | 2018-05-01 | 衡水新光化工有限责任公司 | 净味苯丙乳液及以该乳液为成膜物质的净味涂料 |
| KR102413783B1 (ko) * | 2015-03-09 | 2022-06-29 | 간사이가가쿠기카이세이사쿠가부시키가이샤 | 증발 장치 |
| KR102204734B1 (ko) * | 2016-08-04 | 2021-01-20 | 와커 헤미 아게 | 단경로 증발기에서 고 점성 실리콘 유체의 탈휘발 |
| CN107285413B (zh) * | 2017-08-02 | 2020-10-16 | 徐州腾盛新型建材有限公司 | 一种临时板房污水处理装置 |
| KR102239360B1 (ko) * | 2019-08-12 | 2021-04-09 | 고석근 | 박막 증류장치 |
| KR102239359B1 (ko) * | 2019-08-12 | 2021-04-09 | 고석근 | 박막 증류장치 |
| KR102239361B1 (ko) * | 2019-08-12 | 2021-04-09 | 고석근 | 박막 증류장치의 제조방법 |
| CN110947197B (zh) * | 2019-12-26 | 2021-12-03 | 数谱科技(浙江)有限公司 | 一种薄膜蒸发器用布料器 |
| CN114426591A (zh) * | 2020-10-15 | 2022-05-03 | 中国石油化工股份有限公司 | 醋酸乙烯-乙烯共聚乳液异味去除装置 |
| CN113546440A (zh) * | 2021-09-08 | 2021-10-26 | 郑州长城科工贸有限公司 | 适于蒸馏釜的行星笼形液体成膜机构 |
| JP7466028B2 (ja) | 2022-07-25 | 2024-04-11 | 株式会社神鋼環境ソリューション | 液体濃縮方法および薄膜蒸発装置 |
| TW202415434A (zh) * | 2022-07-25 | 2024-04-16 | 日商神鋼環境舒立淨股份有限公司 | 液體濃縮方法及薄膜蒸發裝置 |
| CN115448398B (zh) * | 2022-10-08 | 2023-10-10 | 杭州佰斯维环境科技有限公司 | 一种用于金属加工废水的处理装置 |
| DE102023107156A1 (de) | 2023-03-22 | 2024-09-26 | Röhm Gmbh | Verfahren zur verbesserten Aufarbeitung von Monomer-haltigen Abgasen |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3020211A (en) * | 1958-11-28 | 1962-02-06 | Arthur F Smith | Film-forming and wiping distillation process and apparatus for carrying out the same |
| US3067812A (en) * | 1959-03-23 | 1962-12-11 | Monsanto Chemcial Company | Apparatus for devolatizing viscous fluids |
| US3130108A (en) * | 1960-11-07 | 1964-04-21 | Blaw Knox Co | Rotating blade type evaporators |
| CS229404B1 (en) * | 1981-06-22 | 1984-06-18 | Alexander Prof Drsc Tkac | Bloc short travel evaporator with a wiped film |
| JP2003170001A (ja) * | 2001-12-07 | 2003-06-17 | Mitsubishi Chemicals Corp | 薄膜蒸発器 |
| CN1572781A (zh) | 2001-10-30 | 2005-02-02 | 三菱化学株式会社 | （甲基）丙烯酸的精制方法 |
| JP2011033241A (ja) | 2009-07-30 | 2011-02-17 | Toshiba Corp | 遠心式薄膜乾燥機 |
| CN102139165A (zh) | 2010-02-01 | 2011-08-03 | 张亚宇 | 空心轴内循环刮板式薄膜蒸发器 |
-
2013
- 2013-02-05 KR KR1020147022423A patent/KR101604940B1/ko active IP Right Grant
- 2013-02-05 JP JP2013508703A patent/JP6064901B2/ja active Active
- 2013-02-05 US US14/381,020 patent/US9981201B2/en active Active
- 2013-02-05 WO PCT/JP2013/052558 patent/WO2013136874A1/ja active Application Filing
- 2013-02-05 CN CN201380014339.0A patent/CN104168972B/zh active Active
Also Published As
| Publication number | Publication date |
|---|---|
| US20150038736A1 (en) | 2015-02-05 |
| CN104168972B (zh) | 2016-01-06 |
| US9981201B2 (en) | 2018-05-29 |
| CN104168972A (zh) | 2014-11-26 |
| KR20140119113A (ko) | 2014-10-08 |
| WO2013136874A1 (ja) | 2013-09-19 |
| JPWO2013136874A1 (ja) | 2015-08-03 |
| KR101604940B1 (ko) | 2016-03-18 |
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