JP5896968B2 - 炭化ジルコニウムのインゴット及び粉末の製造方法 - Google Patents

炭化ジルコニウムのインゴット及び粉末の製造方法 Download PDF

Info

Publication number
JP5896968B2
JP5896968B2 JP2013196717A JP2013196717A JP5896968B2 JP 5896968 B2 JP5896968 B2 JP 5896968B2 JP 2013196717 A JP2013196717 A JP 2013196717A JP 2013196717 A JP2013196717 A JP 2013196717A JP 5896968 B2 JP5896968 B2 JP 5896968B2
Authority
JP
Japan
Prior art keywords
zirconium carbide
ingot
zirconium
carbon
powder
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
JP2013196717A
Other languages
English (en)
Japanese (ja)
Other versions
JP2015063414A5 (https=
JP2015063414A (ja
Inventor
卓二 鍋田
卓二 鍋田
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Daiichi Kigenso Kagaku Kogyo Co Ltd
Original Assignee
Daiichi Kigenso Kagaku Kogyo Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to JP2013196717A priority Critical patent/JP5896968B2/ja
Application filed by Daiichi Kigenso Kagaku Kogyo Co Ltd filed Critical Daiichi Kigenso Kagaku Kogyo Co Ltd
Priority to EP14847888.6A priority patent/EP3029009A4/en
Priority to PCT/JP2014/067879 priority patent/WO2015045547A1/ja
Priority to KR1020167006295A priority patent/KR20160060039A/ko
Priority to US15/022,612 priority patent/US20160229698A1/en
Priority to CN201480050498.0A priority patent/CN105555737A/zh
Publication of JP2015063414A publication Critical patent/JP2015063414A/ja
Publication of JP2015063414A5 publication Critical patent/JP2015063414A5/ja
Application granted granted Critical
Publication of JP5896968B2 publication Critical patent/JP5896968B2/ja
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/653Processes involving a melting step
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B28WORKING CEMENT, CLAY, OR STONE
    • B28BSHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
    • B28B1/00Producing shaped prefabricated articles from the material
    • B28B1/54Producing shaped prefabricated articles from the material specially adapted for producing articles from molten material, e.g. slag refractory ceramic materials
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B28WORKING CEMENT, CLAY, OR STONE
    • B28BSHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
    • B28B17/00Details of, or accessories for, apparatus for shaping the material; Auxiliary measures taken in connection with such shaping
    • B28B17/02Conditioning the material prior to shaping
    • B28B17/026Conditioning ceramic materials
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • C01B32/90Carbides
    • C01B32/914Carbides of single elements
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G25/00Compounds of zirconium
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/515Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
    • C04B35/56Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbides or oxycarbides
    • C04B35/5607Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbides or oxycarbides based on refractory metal carbides
    • C04B35/5622Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbides or oxycarbides based on refractory metal carbides based on zirconium or hafnium carbides
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/62605Treating the starting powders individually or as mixtures
    • C04B35/62695Granulation or pelletising
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/61Micrometer sized, i.e. from 1-100 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/10Solid density
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/90Other properties not specified above
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3231Refractory metal oxides, their mixed metal oxides, or oxide-forming salts thereof
    • C04B2235/3244Zirconium oxides, zirconates, hafnium oxides, hafnates, or oxide-forming salts thereof
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/42Non metallic elements added as constituents or additives, e.g. sulfur, phosphor, selenium or tellurium
    • C04B2235/422Carbon
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/50Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
    • C04B2235/54Particle size related information
    • C04B2235/5418Particle size related information expressed by the size of the particles or aggregates thereof
    • C04B2235/5436Particle size related information expressed by the size of the particles or aggregates thereof micrometer sized, i.e. from 1 to 100 micron
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/66Specific sintering techniques, e.g. centrifugal sintering
    • C04B2235/661Multi-step sintering
    • C04B2235/662Annealing after sintering
    • C04B2235/664Reductive annealing
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/72Products characterised by the absence or the low content of specific components, e.g. alkali metal free alumina ceramics
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/74Physical characteristics
    • C04B2235/77Density
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/95Products characterised by their size, e.g. microceramics
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/96Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Organic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Carbon And Carbon Compounds (AREA)
JP2013196717A 2013-09-24 2013-09-24 炭化ジルコニウムのインゴット及び粉末の製造方法 Active JP5896968B2 (ja)

Priority Applications (6)

Application Number Priority Date Filing Date Title
JP2013196717A JP5896968B2 (ja) 2013-09-24 2013-09-24 炭化ジルコニウムのインゴット及び粉末の製造方法
PCT/JP2014/067879 WO2015045547A1 (ja) 2013-09-24 2014-07-04 炭化ジルコニウムのインゴット及び粉末の製造方法
KR1020167006295A KR20160060039A (ko) 2013-09-24 2014-07-04 탄화 지르코늄 잉곳 및 분말의 제조방법
US15/022,612 US20160229698A1 (en) 2013-09-24 2014-07-04 Method for producing ingot and powder of zirconium carbide
EP14847888.6A EP3029009A4 (en) 2013-09-24 2014-07-04 Method for producing ingot and powder of zirconium carbide
CN201480050498.0A CN105555737A (zh) 2013-09-24 2014-07-04 碳化锆的锭及粉末的制造方法

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2013196717A JP5896968B2 (ja) 2013-09-24 2013-09-24 炭化ジルコニウムのインゴット及び粉末の製造方法

Publications (3)

Publication Number Publication Date
JP2015063414A JP2015063414A (ja) 2015-04-09
JP2015063414A5 JP2015063414A5 (https=) 2015-05-28
JP5896968B2 true JP5896968B2 (ja) 2016-03-30

Family

ID=52742705

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2013196717A Active JP5896968B2 (ja) 2013-09-24 2013-09-24 炭化ジルコニウムのインゴット及び粉末の製造方法

Country Status (6)

Country Link
US (1) US20160229698A1 (https=)
EP (1) EP3029009A4 (https=)
JP (1) JP5896968B2 (https=)
KR (1) KR20160060039A (https=)
CN (1) CN105555737A (https=)
WO (1) WO2015045547A1 (https=)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10488114B1 (en) * 2015-06-09 2019-11-26 Materion Corporation Fluid-cooled copper lid for arc furnace
CN107382321B (zh) * 2017-09-25 2019-12-20 常熟理工学院 一种超细碳化锆粉体及其制备方法
KR102631871B1 (ko) 2019-08-05 2024-02-01 카와사키 주코교 카부시키 카이샤 로봇 핸드, 로봇, 로봇 시스템 및 반송 방법
KR102445158B1 (ko) * 2020-07-09 2022-09-22 한국재료연구원 제어된 크기, 모양, 및 다공도를 갖는 탄화 지르코늄의 제조 방법
CN115041699A (zh) * 2022-07-22 2022-09-13 华材(山东)新材料有限公司 一种3d打印用球形锆粉的生产方法

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5812239B2 (ja) * 1980-03-25 1983-03-07 科学技術庁無機材質研究所長 炭化ジルコニウムの結晶体の製造法
JPH0218310A (ja) * 1988-07-05 1990-01-22 Kawasaki Steel Corp ジルコニウム系セラミック粉末の製造方法
JPH0768563B2 (ja) * 1991-05-27 1995-07-26 大同特殊鋼株式会社 硬質粒子分散合金粉末の製造方法
JPH0753272A (ja) * 1993-08-12 1995-02-28 Agency Of Ind Science & Technol 被覆セラミックス準微粒子、セラミックス基焼結体及びその製造法
US5609695A (en) * 1993-12-21 1997-03-11 Matsushita Electric Industrial Co., Ltd. Method for producing alloy powder of the R2 T17 system, a method for producing magnetic powder of the R2 T17 Nx system, and a high pressure heat-treatment apparatus
CA2154216A1 (en) * 1994-08-01 1996-02-02 Gregg Alan Zank Preparation of high density zirconium carbide ceramics with preceramic polymer binders
JP3977164B2 (ja) * 2002-06-25 2007-09-19 中部電力株式会社 プラズマ溶融装置及びプラズマ溶融方法
JP3955901B2 (ja) * 2005-02-17 2007-08-08 国立大学法人大阪大学 導電性ジルコニア焼結体及びその製造方法
JP2007045670A (ja) * 2005-08-10 2007-02-22 Hyogo Prefecture 金属炭化物の製造方法
CN104321838B (zh) * 2012-02-23 2018-04-06 吉坤日矿日石金属株式会社 钕基稀土类永久磁铁及其制造方法

Also Published As

Publication number Publication date
EP3029009A4 (en) 2017-03-15
CN105555737A (zh) 2016-05-04
EP3029009A1 (en) 2016-06-08
WO2015045547A1 (ja) 2015-04-02
JP2015063414A (ja) 2015-04-09
US20160229698A1 (en) 2016-08-11
KR20160060039A (ko) 2016-05-27

Similar Documents

Publication Publication Date Title
KR101659700B1 (ko) 질화알루미늄 및 질화알루미늄기 복합상 물질의 합성 방법
Balog et al. Industrially fabricated in-situ Al-AlN metal matrix composites (part A): Processing, thermal stability, and microstructure
JP5896968B2 (ja) 炭化ジルコニウムのインゴット及び粉末の製造方法
JP4649586B2 (ja) 窒素プラズマによるSiCナノ粒子の製造法
US5382405A (en) Method of manufacturing a shaped article from a powdered precursor
TW201829299A (zh) 高純度氮化矽粉末之製造方法
CN102242303A (zh) 一种原位纳米TiC陶瓷颗粒增强铜基复合材料及其制备方法
Bokhonov et al. Formation of self-supporting porous graphite structures by Spark Plasma Sintering of nickel–amorphous carbon mixtures
CN103834824B (zh) 一种无粘结相碳化钨硬质合金及其制备方法
Lv et al. Review on the development of titanium diboride ceramics
JP5101277B2 (ja) 炭素熱還元炉用の耐破壊性電極
JPWO2020166380A1 (ja) スパッタリングターゲット材
CN106478109A (zh) ZrC/ZrB2复相陶瓷粉末、制备方法及其应用
Cho et al. Synthesis and consolidation behavior of Al/AlN composite powders by reactive RF thermal plasma spraying
Sakkaki et al. In-situ synthesized phases during the spark plasma sintering of g-C3N4 added TiB2 ceramics: A thermodynamic approach
JP6648161B2 (ja) 硼化ジルコニウム及びその製造方法
CN104529456B (zh) 一种B4C‑HfB2高温共晶自生复合陶瓷的制备方法
Rosinski et al. Properties of WCCO/diamond composites produced by PPS method intended for drill bits for machining of building stones
JP2013014487A (ja) 導電性セラミックスの製造方法
JP2008031016A (ja) 炭化タンタル粉末および炭化タンタル−ニオブ複合粉末とそれらの製造方法
Zhang et al. Synthesis of tungsten monocarbide by self-propagating high-temperature synthesis in the presence of an activative additive
Nikkhah et al. Investigation on mechanochemical synthesis of Al2O3/BN nanocomposite by aluminothermic reaction
JP5252460B2 (ja) 窒素プラズマによるSiCナノ粒子の製造法
RU2653393C1 (ru) Композит с металлической матрицей и упрочняющими наночастицами карбида титана и способ его изготовления
Roghani et al. Effect of milling parameters on the phase transformations and morphology changes of B4C-SiC nanocomposite powder in situ synthesized by MAVCS method

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20150409

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20150409

A871 Explanation of circumstances concerning accelerated examination

Free format text: JAPANESE INTERMEDIATE CODE: A871

Effective date: 20150409

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20150821

A975 Report on accelerated examination

Free format text: JAPANESE INTERMEDIATE CODE: A971005

Effective date: 20150821

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20150901

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20160209

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20160301

R150 Certificate of patent or registration of utility model

Ref document number: 5896968

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250