JP5877197B2 - サンプル調製を実行するためのデバイス - Google Patents
サンプル調製を実行するためのデバイス Download PDFInfo
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- JP5877197B2 JP5877197B2 JP2013512783A JP2013512783A JP5877197B2 JP 5877197 B2 JP5877197 B2 JP 5877197B2 JP 2013512783 A JP2013512783 A JP 2013512783A JP 2013512783 A JP2013512783 A JP 2013512783A JP 5877197 B2 JP5877197 B2 JP 5877197B2
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- 238000010438 heat treatment Methods 0.000 claims description 69
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- 229910052751 metal Inorganic materials 0.000 claims description 16
- 239000002184 metal Substances 0.000 claims description 16
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims description 8
- 238000007789 sealing Methods 0.000 claims description 7
- 229910052697 platinum Inorganic materials 0.000 claims description 4
- 239000000523 sample Substances 0.000 description 187
- 238000000197 pyrolysis Methods 0.000 description 31
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- 238000007689 inspection Methods 0.000 description 3
- 239000010453 quartz Substances 0.000 description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 3
- 238000001149 thermolysis Methods 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 238000005251 capillar electrophoresis Methods 0.000 description 2
- 230000015556 catabolic process Effects 0.000 description 2
- 238000006731 degradation reaction Methods 0.000 description 2
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- 238000012360 testing method Methods 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 238000000631 analytical pyrolysis Methods 0.000 description 1
- 239000000538 analytical sample Substances 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
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- 239000012159 carrier gas Substances 0.000 description 1
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- 230000017525 heat dissipation Effects 0.000 description 1
- 239000001307 helium Substances 0.000 description 1
- 229910052734 helium Inorganic materials 0.000 description 1
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 1
- 238000004128 high performance liquid chromatography Methods 0.000 description 1
- 238000011065 in-situ storage Methods 0.000 description 1
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- 238000004808 supercritical fluid chromatography Methods 0.000 description 1
- 229920001059 synthetic polymer Polymers 0.000 description 1
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01L—CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
- B01L3/00—Containers or dishes for laboratory use, e.g. laboratory glassware; Droppers
- B01L3/50—Containers for the purpose of retaining a material to be analysed, e.g. test tubes
- B01L3/508—Containers for the purpose of retaining a material to be analysed, e.g. test tubes rigid containers not provided for above
- B01L3/5082—Test tubes per se
- B01L3/50825—Closing or opening means, corks, bungs
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/16—Injection
- G01N30/18—Injection using a septum or microsyringe
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
- B01D15/12—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to the preparation of the feed
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/10—Devices for withdrawing samples in the liquid or fluent state
- G01N1/12—Dippers; Dredgers
- G01N1/125—Dippers; Dredgers adapted for sampling molten metals
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- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Analytical Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Hematology (AREA)
- Clinical Laboratory Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Sampling And Sample Adjustment (AREA)
Description
Claims (4)
- クロマトグラフを含む分析装置のためのサンプル調製を実行するためのデバイスであって、
自己封止カバーによって閉鎖することができると共に検査対象の物質を受容するためのサンプル区画(31)を含むサンプル容器(1)を含み、
更に加熱ワイヤ・コイル(13)を含むホルダ(12)を含み、前記ホルダ内に、前記検査対象の物質を加熱するためにそのサンプル区画(31)を有する前記サンプル容器(1)を挿入することができ、
前記加熱ワイヤ・コイル(13)は、前記ホルダの底部に配置された内側金属リング電極(22)および外側金属リング電極(21)に接続されるよう構成され、
前記内側金属リング電極(22)および前記外側金属リング電極(21)は、共通の平面に配置され、
前記外側金属リング電極(21)は、前記内側金属リング電極(22)を囲んでおり、
更に、前記加熱ワイヤ・コイル(13)のための電源を含み、前記電源が、定電流制御に基づくと共にパルス幅変調によって比例的に制御される、デバイス。 - 設けられた前記ホルダ(12)が、閉鎖キャップ17によって閉鎖することができるモジュール容器(14)であり、
その内部(40)に前記サンプル容器(1)が挿入可能容器として挿入され、
前記サンプル容器の下部(15)において前記加熱ワイヤ・コイル(13)が前記モジュール容器(14)に一体化されていることを特徴とする、請求項1に記載のデバイス。 - 前記加熱ワイヤ・コイル(13)の前記電源が接続可能加熱基盤(33)を介して外部に設けられていることを特徴とする、請求項2に記載のデバイス。
- 前記加熱ワイヤ・コイル(13)が白金加熱ワイヤ・コイルであることを特徴とする、請求項1〜3のいずれか一項に記載のデバイス。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE102010022016A DE102010022016A1 (de) | 2010-05-29 | 2010-05-29 | Vorrichtung zur Durchführung einer Probenvorbereitung |
DE102010022016.7 | 2010-05-29 | ||
PCT/EP2011/002562 WO2011151026A1 (de) | 2010-05-29 | 2011-05-24 | Vorrichtung zur durchführung einer probenvorbereitung |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2013527461A JP2013527461A (ja) | 2013-06-27 |
JP5877197B2 true JP5877197B2 (ja) | 2016-03-02 |
Family
ID=44245676
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2013512783A Active JP5877197B2 (ja) | 2010-05-29 | 2011-05-24 | サンプル調製を実行するためのデバイス |
Country Status (5)
Country | Link |
---|---|
US (1) | US9061281B2 (ja) |
EP (1) | EP2577284B1 (ja) |
JP (1) | JP5877197B2 (ja) |
DE (1) | DE102010022016A1 (ja) |
WO (1) | WO2011151026A1 (ja) |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE102010022017A1 (de) * | 2010-05-29 | 2011-12-01 | Gerstel Systemtechnik Gmbh & Co.Kg | Verfahren zur Probenvorbereitung bei chromatographischen Trennmethoden und Vorrichtungen zur Durchführung einer Probenvorbereitung |
US11647789B2 (en) * | 2019-12-23 | 2023-05-16 | Tuanfang Liu | Atomizer |
CN113333044B (zh) * | 2021-08-03 | 2021-10-15 | 苏州鼎实医疗科技有限公司 | 一种定量采样加注装置及利用其进行定量采样加注的方法 |
CN113552272B (zh) * | 2021-09-22 | 2021-11-30 | 南通市安特速医疗科技有限公司 | 一种气相色谱仪用样品自动进样装置 |
Family Cites Families (20)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2231322A (en) * | 1941-02-11 | Deodorizing and disinfecting device | ||
DE1846022U (de) * | 1961-07-14 | 1962-02-01 | Joachim Dipl Chem Dr Rer Voigt | Pyrolysegeraet fuer gaschromatographische analysen. |
US3179499A (en) * | 1961-12-12 | 1965-04-20 | American Instr Co Inc | Pyrolyzer for gas chromatog-raphy apparatus |
DE1598436C3 (de) * | 1965-11-25 | 1974-10-31 | Wolfgang Guenther 5300 Bonn-Bad Godesberg Fischer | Verfahren und Vorrichtung zur gaschromatographischen Analyse von durch Wärme zersetzbaren Substanzen |
DE1773141A1 (de) | 1968-04-05 | 1971-07-01 | Bodenseewerk Perkin Elmer Co | Verfahren zur Probengabe bei Gasanalysengeraeten |
JPS5786454A (en) | 1980-11-14 | 1982-05-29 | Iyo Tetsukou Kk | Pallet-container |
JPS5786454U (ja) * | 1980-11-18 | 1982-05-28 | ||
DE3315651C2 (de) * | 1983-04-29 | 1985-08-08 | Bodenseewerk Perkin-Elmer & Co GmbH, 7770 Überlingen | Elektrische Heizung für einen sich drehenden Probengefäßbehälter in einem Probengeber für Gaschromatographen |
DE4206109C2 (de) | 1992-02-27 | 1994-09-01 | Bruker Franzen Analytik Gmbh | Verfahren und Vorrichtung zur Aufbereitung fester Proben mit Hilfe pyrolytischer Verdampfung für eine Analyse mittels eines Massenspektrometers oder eines Gaschromatographen |
US5782964A (en) * | 1997-01-27 | 1998-07-21 | Rvm Scientific, Inc. | Gas chromatography column assembly temperature control system |
DE19720687C1 (de) * | 1997-05-16 | 1998-07-30 | Forschungszentrum Juelich Gmbh | Pyrolyseröhrchen für die Gaschromatographie, Pyrolysatorvorrichtung, gaschromatographisches Verfahren sowie Gaschromatograph |
JP3775008B2 (ja) * | 1997-08-29 | 2006-05-17 | 株式会社島津製作所 | サンプリング装置 |
DE19817016C2 (de) * | 1998-04-17 | 2000-02-03 | Gerstel Gmbh & Co Kg | Probenaufgabeeinrichtung für einen Gaschromatopgraphen |
JP4240764B2 (ja) * | 2000-06-20 | 2009-03-18 | 株式会社島津製作所 | ヘッドスペース試料導入装置 |
US6907796B2 (en) * | 2001-05-30 | 2005-06-21 | Gerstel Systemtechnik Gmbh & Co. Kg | Temperature-controlled injector for a chemical analysis unit |
JP3658553B2 (ja) * | 2001-08-06 | 2005-06-08 | ポリマテック株式会社 | ホルダー及び電子部品の導電接続構造 |
JP2003083978A (ja) | 2001-09-10 | 2003-03-19 | Olympus Optical Co Ltd | 自動分析装置 |
DE102005060291A1 (de) * | 2005-12-15 | 2007-06-28 | Gerstel Systemtechnik Gmbh & Co.Kg | Verfahren zur Vorbereitung von Proben für ein Analysegerät und Probennahmestation hierfür |
DE102005060303A1 (de) * | 2005-12-16 | 2007-06-28 | Gerstel Systemtechnik Gmbh & Co.Kg | Verfahren zur Vorbereitung von Proben für ein Analysegerät und Probenvorbereitungsstation hierfür |
US20080026288A1 (en) * | 2006-07-26 | 2008-01-31 | Eveready Battery Company, Inc. | Electrochemical cell with positive container |
-
2010
- 2010-05-29 DE DE102010022016A patent/DE102010022016A1/de not_active Withdrawn
-
2011
- 2011-05-24 JP JP2013512783A patent/JP5877197B2/ja active Active
- 2011-05-24 US US13/700,711 patent/US9061281B2/en active Active
- 2011-05-24 WO PCT/EP2011/002562 patent/WO2011151026A1/de active Application Filing
- 2011-05-24 EP EP11721243.1A patent/EP2577284B1/de active Active
Also Published As
Publication number | Publication date |
---|---|
JP2013527461A (ja) | 2013-06-27 |
US9061281B2 (en) | 2015-06-23 |
US20130078165A1 (en) | 2013-03-28 |
WO2011151026A1 (de) | 2011-12-08 |
EP2577284A1 (de) | 2013-04-10 |
DE102010022016A1 (de) | 2011-12-01 |
EP2577284B1 (de) | 2019-10-02 |
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