JP5831036B2 - ピペラジン−ｎ，ｎ’−ビスカルボジチオ酸塩水溶液及びその製造方法 - Google Patents

ピペラジン−ｎ，ｎ’−ビスカルボジチオ酸塩水溶液及びその製造方法 Download PDF

Info

Publication number
JP5831036B2
JP5831036B2 JP2011180509A JP2011180509A JP5831036B2 JP 5831036 B2 JP5831036 B2 JP 5831036B2 JP 2011180509 A JP2011180509 A JP 2011180509A JP 2011180509 A JP2011180509 A JP 2011180509A JP 5831036 B2 JP5831036 B2 JP 5831036B2
Authority
JP
Japan
Prior art keywords
piperazine
carbon disulfide
biscarbodithioate
aqueous solution
carbodithioate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
JP2011180509A
Other languages
English (en)
Japanese (ja)
Other versions
JP2012214429A (ja
Inventor
義則 阿山
義則 阿山
長井　康行
康行 長井
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Tosoh Corp
Original Assignee
Tosoh Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Tosoh Corp filed Critical Tosoh Corp
Priority to JP2011180509A priority Critical patent/JP5831036B2/ja
Priority to CN201180057459.XA priority patent/CN103237796B/zh
Priority to PCT/JP2011/077578 priority patent/WO2012073976A1/ja
Publication of JP2012214429A publication Critical patent/JP2012214429A/ja
Application granted granted Critical
Publication of JP5831036B2 publication Critical patent/JP5831036B2/ja
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
    • C07D295/16—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms acylated on ring nitrogen atoms
    • C07D295/20—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms acylated on ring nitrogen atoms by radicals derived from carbonic acid, or sulfur or nitrogen analogues thereof

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
JP2011180509A 2010-11-30 2011-08-22 ピペラジン−ｎ，ｎ’−ビスカルボジチオ酸塩水溶液及びその製造方法 Active JP5831036B2 (ja)

Priority Applications (3)

Application Number Priority Date Filing Date Title
JP2011180509A JP5831036B2 (ja) 2010-11-30 2011-08-22 ピペラジン−ｎ，ｎ’−ビスカルボジチオ酸塩水溶液及びその製造方法
CN201180057459.XA CN103237796B (zh) 2010-11-30 2011-11-29 哌嗪-n,n’-双二硫代羧酸盐水溶液及其制造方法
PCT/JP2011/077578 WO2012073976A1 (ja) 2010-11-30 2011-11-29 ピペラジン－ｎ，ｎ'－ビスカルボジチオ酸塩水溶液及びその製造方法

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
JP2010266294 2010-11-30
JP2010266294 2010-11-30
JP2011074065 2011-03-30
JP2011074065 2011-03-30
JP2011180509A JP5831036B2 (ja) 2010-11-30 2011-08-22 ピペラジン−ｎ，ｎ’−ビスカルボジチオ酸塩水溶液及びその製造方法

Publications (2)

Publication Number Publication Date
JP2012214429A JP2012214429A (ja) 2012-11-08
JP5831036B2 true JP5831036B2 (ja) 2015-12-09

Family

ID=46171905

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2011180509A Active JP5831036B2 (ja) 2010-11-30 2011-08-22 ピペラジン−ｎ，ｎ’−ビスカルボジチオ酸塩水溶液及びその製造方法

Country Status (3)

Country Link
JP (1) JP5831036B2 (zh)
CN (1) CN103237796B (zh)
WO (1) WO2012073976A1 (zh)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP7293596B2 (ja) * 2017-10-06 2023-06-20 東ソー株式会社 ニッケル含有水溶液用浄化剤及びニッケル含有水溶液の浄化方法
CN112552262B (zh) * 2020-08-13 2022-03-08 成都恒鑫和环保科技有限公司 一种哌嗪-n,n’-双二硫代羧酸钾的合成方法
CN112480039B (zh) * 2020-12-18 2023-04-07 成都恒鑫和环保科技有限公司 一种在反应液中添加不同醇制备哌嗪-n,n’-双二硫代羧酸钾的方法

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6360986A (ja) * 1986-08-29 1988-03-17 Idemitsu Petrochem Co Ltd ジチオカルバミン酸塩およびその製造方法
JP3391173B2 (ja) * 1994-12-02 2003-03-31 東ソー株式会社 飛灰中の重金属の固定化方法及び重金属固定化処理剤
JP4573343B2 (ja) * 2001-11-21 2010-11-04 日本曹達株式会社 ピペラジンビスカルボジチオ酸塩を含有する水溶液の製造方法
US6545172B1 (en) * 2002-04-18 2003-04-08 Bayer Corporation Processes for the production of methyl dithiocarbazinate
JP4696475B2 (ja) * 2004-05-28 2011-06-08 東ソー株式会社 ジチオカルバミン酸塩水溶液及びその製造方法並びに重金属固定化処理剤及び重金属の固定化処理方法
CN100345772C (zh) * 2004-09-08 2007-10-31 中山大学 一种重金属沉淀剂
JP4792810B2 (ja) * 2005-05-13 2011-10-12 東ソー株式会社 重金属処理剤およびそれを用いた重金属処理方法
JP4796824B2 (ja) * 2005-11-30 2011-10-19 栗田工業株式会社 重金属固定化剤用低温貯蔵安定化剤
JP5493244B2 (ja) * 2006-12-07 2014-05-14 東ソー株式会社 ピペラジン系重金属処理剤の製造方法

Also Published As

Publication number Publication date
WO2012073976A1 (ja) 2012-06-07
JP2012214429A (ja) 2012-11-08
CN103237796A (zh) 2013-08-07
CN103237796B (zh) 2015-09-09

Similar Documents

Publication Publication Date Title
JP2014005269A (ja) シュウ酸を配位子とする金属錯体精製物及び該金属錯体の非水溶媒精製溶液の製造方法
JP6333939B2 (ja) ハロアルカン化合物の製造中における副生成物の形成を減少させる方法
US9067907B2 (en) Process for preparing fluorinated 1,3-dioxolan 2-one
JP2016026991A (ja) 錯体中心形成剤、イオン性錯体及びこれらの製造方法
JP5135926B2 (ja) ４−フルオロ−１，３−ジオキソラン−２−オンの製造方法
JP5831036B2 (ja) ピペラジン−ｎ，ｎ’−ビスカルボジチオ酸塩水溶液及びその製造方法
EP2036899A1 (en) Method for producing cyclic disulfonic acid ester
JP2012055825A (ja) 銅エッチング廃液の処理方法
KR100852900B1 (ko) 퍼플르오로 불포화 탄화수소를 제조하는 방법
JP5493244B2 (ja) ピペラジン系重金属処理剤の製造方法
US9440934B1 (en) Synthesis of copper(I) 5-nitrotetrazolate
JP7359141B2 (ja) ヘキサフルオロ－１，３－ブタジエンの製造方法
JP6799040B2 (ja) 改質金属硫化物の製造方法
JP5834750B2 (ja) フルオロリン酸化合物を含む廃水の処理方法
JP5747608B2 (ja) ピペラジン−ｎ，ｎ’−ビスカルボジチオ酸塩水溶液の製造方法
US20070286789A1 (en) Method for Producing Chlorosulfonyl Isocyanate
US8501138B2 (en) Production method of high purity silver tetrafluoroborate
JP2013184901A (ja) アルミニウムアルコキサイドの製造方法
JP6550927B2 (ja) ヨウ化アルキル化合物の製造方法
JP6330064B1 (ja) ヨウ化水素酸の製造方法及びヨウ化金属水溶液の製造方法
JPH07119178B2 (ja) 含フッ素有機基を有するエチレン化合物の精製方法
JP6504059B2 (ja) ヘキサクロロアセトンの製造方法
JP2010260829A (ja) ジアリールヨードニウム化合物の製造方法
JP2012167020A (ja) 臭素化ラクトン類化合物の製造方法
JP2016027029A (ja) 精製イオン性錯体の製造方法及びイオン性錯体

Legal Events

Date Code Title Description
A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20140723

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20150707

A521 Written amendment

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20150904

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20150929

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20151012

R151 Written notification of patent or utility model registration

Ref document number: 5831036

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R151