JP5676579B2 - 電子用途用の重水素化合物 - Google Patents

電子用途用の重水素化合物 Download PDF

Info

Publication number
JP5676579B2
JP5676579B2 JP2012511981A JP2012511981A JP5676579B2 JP 5676579 B2 JP5676579 B2 JP 5676579B2 JP 2012511981 A JP2012511981 A JP 2012511981A JP 2012511981 A JP2012511981 A JP 2012511981A JP 5676579 B2 JP5676579 B2 JP 5676579B2
Authority
JP
Japan
Prior art keywords
deuterated
layer
compound
group
added
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
JP2012511981A
Other languages
English (en)
Japanese (ja)
Other versions
JP2012527468A5 (https=
JP2012527468A (ja
Inventor
デイビッド ルクロー ダニエル
デイビッド ルクロー ダニエル
フェニモア アダム
フェニモア アダム
ウェイイン ガオ
ウェイイン ガオ
サビーナ ラドゥ ノーラ
サビーナ ラドゥ ノーラ
ウー ウェイシー
ウー ウェイシー
ロストフツェフ フセヴォロド
ロストフツェフ フセヴォロド
ヘンリー ハワード ジュニア マイケル
ヘンリー ハワード ジュニア マイケル
ホン メン
ホン メン
ユーロン シェン
ユーロン シェン
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
EIDP Inc
Original Assignee
EI Du Pont de Nemours and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by EI Du Pont de Nemours and Co filed Critical EI Du Pont de Nemours and Co
Publication of JP2012527468A publication Critical patent/JP2012527468A/ja
Publication of JP2012527468A5 publication Critical patent/JP2012527468A5/ja
Application granted granted Critical
Publication of JP5676579B2 publication Critical patent/JP5676579B2/ja
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • HELECTRICITY
    • H10SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10KORGANIC ELECTRIC SOLID-STATE DEVICES
    • H10K85/00Organic materials used in the body or electrodes of devices covered by this subclass
    • H10K85/60Organic compounds having low molecular weight
    • H10K85/615Polycyclic condensed aromatic hydrocarbons, e.g. anthracene
    • H10K85/626Polycyclic condensed aromatic hydrocarbons, e.g. anthracene containing more than one polycyclic condensed aromatic rings, e.g. bis-anthracene
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C15/00Cyclic hydrocarbons containing only six-membered aromatic rings as cyclic parts
    • C07C15/20Polycyclic condensed hydrocarbons
    • C07C15/27Polycyclic condensed hydrocarbons containing three rings
    • C07C15/28Anthracenes
    • HELECTRICITY
    • H05ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05BELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
    • H05B33/00Electroluminescent light sources
    • H05B33/12Light sources with substantially two-dimensional [2D] radiating surfaces
    • H05B33/14Light sources with substantially two-dimensional [2D] radiating surfaces characterised by the chemical or physical composition or the arrangement of the electroluminescent material, or by the simultaneous addition of the electroluminescent material in or onto the light source
    • HELECTRICITY
    • H05ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05BELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
    • H05B33/00Electroluminescent light sources
    • H05B33/12Light sources with substantially two-dimensional [2D] radiating surfaces
    • H05B33/20Light sources with substantially two-dimensional [2D] radiating surfaces characterised by the chemical or physical composition or the arrangement of the material in which the electroluminescent material is embedded
    • HELECTRICITY
    • H10SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10KORGANIC ELECTRIC SOLID-STATE DEVICES
    • H10K50/00Organic light-emitting devices
    • H10K50/10OLEDs or polymer light-emitting diodes [PLED]
    • H10K50/11OLEDs or polymer light-emitting diodes [PLED] characterised by the electroluminescent [EL] layers
    • HELECTRICITY
    • H10SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10KORGANIC ELECTRIC SOLID-STATE DEVICES
    • H10K85/00Organic materials used in the body or electrodes of devices covered by this subclass
    • H10K85/60Organic compounds having low molecular weight
    • H10K85/615Polycyclic condensed aromatic hydrocarbons, e.g. anthracene
    • HELECTRICITY
    • H10SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10KORGANIC ELECTRIC SOLID-STATE DEVICES
    • H10K85/00Organic materials used in the body or electrodes of devices covered by this subclass
    • H10K85/60Organic compounds having low molecular weight
    • H10K85/631Amine compounds having at least two aryl rest on at least one amine-nitrogen atom, e.g. triphenylamine
    • H10K85/633Amine compounds having at least two aryl rest on at least one amine-nitrogen atom, e.g. triphenylamine comprising polycyclic condensed aromatic hydrocarbons as substituents on the nitrogen atom
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07BGENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00Indexing scheme relating to specific properties of organic compounds
    • C07B2200/05Isotopically modified compounds, e.g. labelled
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2603/00Systems containing at least three condensed rings
    • C07C2603/02Ortho- or ortho- and peri-condensed systems
    • C07C2603/04Ortho- or ortho- and peri-condensed systems containing three rings
    • C07C2603/22Ortho- or ortho- and peri-condensed systems containing three rings containing only six-membered rings
    • C07C2603/24Anthracenes; Hydrogenated anthracenes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Optics & Photonics (AREA)
  • Electroluminescent Light Sources (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
JP2012511981A 2009-05-19 2010-05-19 電子用途用の重水素化合物 Active JP5676579B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US17940709P 2009-05-19 2009-05-19
US61/179,407 2009-05-19
PCT/US2010/035356 WO2010135395A2 (en) 2009-05-19 2010-05-19 Deuterated compounds for electronic applications

Publications (3)

Publication Number Publication Date
JP2012527468A JP2012527468A (ja) 2012-11-08
JP2012527468A5 JP2012527468A5 (https=) 2013-07-04
JP5676579B2 true JP5676579B2 (ja) 2015-02-25

Family

ID=43126737

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2012511981A Active JP5676579B2 (ja) 2009-05-19 2010-05-19 電子用途用の重水素化合物

Country Status (7)

Country Link
US (1) US20110121269A1 (https=)
EP (1) EP2432848A4 (https=)
JP (1) JP5676579B2 (https=)
KR (1) KR20120026095A (https=)
CN (1) CN102428158B (https=)
TW (1) TW201105612A (https=)
WO (1) WO2010135395A2 (https=)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2016178326A (ja) * 2009-02-27 2016-10-06 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニーE.I.Du Pont De Nemours And Company 電子用途用の重水素化合物

Families Citing this family (38)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8759818B2 (en) * 2009-02-27 2014-06-24 E I Du Pont De Nemours And Company Deuterated compounds for electronic applications
WO2010114583A1 (en) * 2009-04-03 2010-10-07 E. I. Du Pont De Nemours And Company Electroactive materials
WO2011040939A1 (en) * 2009-09-29 2011-04-07 E. I. Du Pont De Nemours And Company Deuterated compounds for luminescent applications
TW201114771A (en) 2009-10-29 2011-05-01 Du Pont Deuterated compounds for electronic applications
TW201229010A (en) * 2010-12-13 2012-07-16 Du Pont Electroactive materials
JP5727038B2 (ja) 2010-12-20 2015-06-03 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニーE.I.Du Pont De Nemours And Company 電子技術応用のための組成物
KR102064949B1 (ko) * 2018-07-24 2020-01-10 머티어리얼사이언스 주식회사 유기 화합물 및 이를 포함하는 유기 전계 발광 소자
EP3754734A4 (en) 2018-09-20 2021-06-30 Lg Chem, Ltd. ORGANIC LIGHT DIODE
US20200111962A1 (en) 2018-10-03 2020-04-09 Idemitsu Kosan Co., Ltd. Organic electroluminescence device and electronic apparatus provided with the same
WO2020075769A1 (ja) 2018-10-09 2020-04-16 出光興産株式会社 有機エレクトロルミネッセンス素子及びそれを用いた電子機器
US12284915B2 (en) 2018-10-09 2025-04-22 Idemitsu Kosan Co., Ltd. Organic electroluminescence device and electronic apparatus provided with the same
US12171141B2 (en) 2018-10-09 2024-12-17 Idemitsu Kosan Co., Ltd. Organic electroluminescence device and electronic apparatus provided with the same
US20220169656A1 (en) 2018-10-09 2022-06-02 Idemitsu Kosan Co., Ltd. Novel compound, organic electroluminescence device and electronic apparatus
US12433162B2 (en) 2018-10-09 2025-09-30 Idemitsu Kosan Co., Ltd. Compound, organic electroluminescence device, and electronic apparatus
WO2020075784A1 (ja) 2018-10-09 2020-04-16 出光興産株式会社 有機エレクトロルミネッセンス素子及びそれを用いた電子機器
CN112823434B (zh) 2018-10-16 2025-06-03 出光兴产株式会社 有机电致发光元件和电子设备
KR102777993B1 (ko) 2018-10-16 2025-03-06 이데미쓰 고산 가부시키가이샤 유기 일렉트로루미네센스 소자 및 전자 기기
WO2020085829A1 (en) * 2018-10-26 2020-04-30 Rohm And Haas Electronic Materials Korea Ltd. A plurality of light-emitting materials and organic electroluminescent device comprising the same
EP4180501B1 (en) * 2018-10-26 2025-12-10 Canon Kabushiki Kaisha Methods for producing a composition and a organic light-emitting device
KR102895676B1 (ko) 2018-11-08 2025-12-04 이데미쓰 고산 가부시키가이샤 신규 화합물, 그것을 이용한 유기 일렉트로루미네센스 소자 및 전자 기기
KR101978650B1 (ko) * 2018-11-14 2019-05-15 머티어리얼사이언스 주식회사 중수소화 방향족 화합물의 중간체 및 이를 이용한 중수소화 방향족 화합물의 제조 방법
US12453284B2 (en) * 2019-10-30 2025-10-21 Lg Chem, Ltd. Anthracene compound and organic light-emitting device comprising same
KR102805898B1 (ko) * 2019-10-30 2025-05-09 주식회사 엘지화학 중수소화 화합물의 제조 방법
KR20210116996A (ko) * 2020-03-18 2021-09-28 에스에프씨 주식회사 고효율 및 장수명의 유기발광소자
KR20210125937A (ko) * 2020-04-09 2021-10-19 에스에프씨 주식회사 신규한 안트라센 화합물 및 이를 포함하는 유기발광소자
WO2021210800A1 (ko) 2020-04-17 2021-10-21 주식회사 엘지화학 중수소화 화합물의 제조 방법
US20210384444A1 (en) * 2020-05-29 2021-12-09 Lg Display Co., Ltd. Organic light emitting device
KR102886633B1 (ko) * 2020-07-24 2025-11-13 주식회사 엘지화학 신규한 화합물 및 이를 이용한 유기 발광 소자
CN115349182A (zh) * 2020-08-05 2022-11-15 株式会社Lg化学 组合物以及包含其的电子器件和有机发光器件
WO2022030946A1 (ko) * 2020-08-05 2022-02-10 주식회사 엘지화학 조성물, 및 이를 포함하는 전자 소자 및 유기 발광 소자
CN112010762B (zh) * 2020-08-18 2022-02-22 南京高光半导体材料有限公司 一种有机电致发光化合物及有机电致发光器件
KR102913358B1 (ko) * 2020-10-29 2026-01-14 주식회사 엘지화학 중수소화 화합물의 분석방법, 소자 제조용 중수소화 화합물의 선별방법 및 전자 소자의 제조방법
EP4011872A1 (en) * 2020-12-08 2022-06-15 SFC Co., Ltd. Organic electroluminescent compound and organic electroluminescent device including the same
TW202309242A (zh) 2021-04-09 2023-03-01 德商麥克專利有限公司 用於有機電致發光裝置之材料
US20250194413A1 (en) * 2022-03-01 2025-06-12 Fuyang Sineva New Material Technology Co., Ltd. Deuterated composition, organic light-emitting device and display device
CN116693358A (zh) * 2022-03-01 2023-09-05 阜阳欣奕华材料科技有限公司 一种氘代组合物、有机电致发光器件和显示装置
CN116143740B (zh) * 2023-02-27 2025-01-28 阜阳欣奕华新材料科技股份有限公司 氘代的苯并呋喃类化合物及有机电致发光器件及显示装置
CN119039259B (zh) * 2024-10-30 2025-02-07 石家庄诚志永华显示材料有限公司 一种蓝色发光化合物、蓝色发光组合物及包含其的有机电致发光器件、显示装置和照明装置

Family Cites Families (36)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB8909011D0 (en) * 1989-04-20 1989-06-07 Friend Richard H Electroluminescent devices
US5408109A (en) * 1991-02-27 1995-04-18 The Regents Of The University Of California Visible light emitting diodes fabricated from soluble semiconducting polymers
US6670645B2 (en) * 2000-06-30 2003-12-30 E. I. Du Pont De Nemours And Company Electroluminescent iridium compounds with fluorinated phenylpyridines, phenylpyrimidines, and phenylquinolines and devices made with such compounds
US6579630B2 (en) * 2000-12-07 2003-06-17 Canon Kabushiki Kaisha Deuterated semiconducting organic compounds used for opto-electronic devices
US20060159838A1 (en) * 2005-01-14 2006-07-20 Cabot Corporation Controlling ink migration during the formation of printable electronic features
TW200404054A (en) * 2002-07-26 2004-03-16 Wako Pure Chem Ind Ltd Method for deuteration of aromatic ring
CA2499364A1 (en) * 2002-09-24 2004-04-08 E. I. Du Pont De Nemours And Company Water dispersible polyanilines made with polymeric acid colloids for electronics applications
AU2003275203A1 (en) * 2002-09-24 2004-04-19 E.I. Du Pont De Nemours And Company Water dispersible polythiophenes made with polymeric acid colloids
WO2004044088A1 (ja) * 2002-11-12 2004-05-27 Idemitsu Kosan Co., Ltd. 有機エレクトロルミネッセンス素子用材料及びそれを用いた有機エレクトロルミネッセンス素子
US6872475B2 (en) * 2002-12-03 2005-03-29 Canon Kabushiki Kaisha Binaphthalene derivatives for organic electro-luminescent devices
US7651788B2 (en) * 2003-03-05 2010-01-26 Lg Display Co., Ltd. Organic electroluminescent device
JP3848306B2 (ja) * 2003-06-27 2006-11-22 キヤノン株式会社 アントリル誘導基置換化合物およびそれを使用した有機発光素子
JP3848307B2 (ja) * 2003-06-27 2006-11-22 キヤノン株式会社 アミノアントリル誘導基置換化合物およびそれを使用した有機発光素子
JP4035482B2 (ja) * 2003-06-27 2008-01-23 キヤノン株式会社 置換アントリル誘導体およびそれを使用した有機発光素子
JP3840235B2 (ja) * 2003-06-27 2006-11-01 キヤノン株式会社 有機発光素子
US6852429B1 (en) * 2003-08-06 2005-02-08 Canon Kabushiki Kaisha Organic electroluminescent device based on pyrene derivatives
US7365230B2 (en) * 2004-02-20 2008-04-29 E.I. Du Pont De Nemours And Company Cross-linkable polymers and electronic devices made with such polymers
US7351358B2 (en) * 2004-03-17 2008-04-01 E.I. Du Pont De Nemours And Company Water dispersible polypyrroles made with polymeric acid colloids for electronics applications
US7402681B2 (en) * 2004-12-14 2008-07-22 Xerox Corporation Compound with indolocarbazole moieties and devices containing such compound
JP4677221B2 (ja) * 2004-11-26 2011-04-27 キヤノン株式会社 有機発光素子
JP4599142B2 (ja) * 2004-11-26 2010-12-15 キヤノン株式会社 有機発光素子
JP4429149B2 (ja) * 2004-11-26 2010-03-10 キヤノン株式会社 フルオレン化合物及び有機発光素子
JP4955971B2 (ja) * 2004-11-26 2012-06-20 キヤノン株式会社 アミノアントリル誘導基置換ピレン化合物および有機発光素子
CN101115708B (zh) * 2005-02-07 2010-10-13 出光兴产株式会社 芳香族胺衍生物以及使用其的有机电致发光元件
KR100739498B1 (ko) * 2005-05-07 2007-07-19 주식회사 두산 중수소화된 신규 아릴아민 유도체, 그 제조 방법 및 이를이용한 유기 전계 발광 소자
JP2007137837A (ja) * 2005-11-21 2007-06-07 Idemitsu Kosan Co Ltd 芳香族アミン誘導体及びそれを用いた有機エレクトロルミネッセンス素子
KR100852328B1 (ko) * 2006-03-15 2008-08-14 주식회사 엘지화학 신규한 안트라센 유도체, 이의 제조방법 및 이를 이용한유기 전기 발광 소자
KR100877876B1 (ko) * 2006-03-23 2009-01-13 주식회사 엘지화학 신규한 디아민 유도체, 이의 제조방법 및 이를 이용한유기전자소자
DE602007010616D1 (de) * 2006-06-05 2010-12-30 Du Pont Verfahren zur herstellung einer organischen elektrovorrichtung
JP5264723B2 (ja) * 2006-06-30 2013-08-14 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー 導電性ポリマーと部分フッ素化酸ポリマーとの安定化組成物
JP2008270737A (ja) * 2007-03-23 2008-11-06 Fujifilm Corp 有機電界発光素子
JP5484690B2 (ja) * 2007-05-18 2014-05-07 ユー・ディー・シー アイルランド リミテッド 有機電界発光素子
JP2009016693A (ja) * 2007-07-07 2009-01-22 Idemitsu Kosan Co Ltd ホスト材料および有機el素子
JP2009076865A (ja) * 2007-08-29 2009-04-09 Fujifilm Corp 有機電界発光素子
KR101092003B1 (ko) * 2007-11-05 2011-12-09 에스에프씨 주식회사 안트라센 유도체 및 이를 채용한 유기전계발광소자
CN102482570B (zh) * 2009-09-03 2014-11-12 E.I.内穆尔杜邦公司 用于电子应用的氘代化合物

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2016178326A (ja) * 2009-02-27 2016-10-06 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニーE.I.Du Pont De Nemours And Company 電子用途用の重水素化合物

Also Published As

Publication number Publication date
WO2010135395A2 (en) 2010-11-25
KR20120026095A (ko) 2012-03-16
CN102428158B (zh) 2014-06-25
US20110121269A1 (en) 2011-05-26
WO2010135395A3 (en) 2011-03-03
JP2012527468A (ja) 2012-11-08
EP2432848A4 (en) 2012-12-05
CN102428158A (zh) 2012-04-25
TW201105612A (en) 2011-02-16
EP2432848A2 (en) 2012-03-28

Similar Documents

Publication Publication Date Title
JP5676579B2 (ja) 電子用途用の重水素化合物
JP5714014B2 (ja) 電子用途用の重水素化合物
JP5671054B2 (ja) 電子用途用の化合物の組合せの一部としての重水素化合物
US9577199B2 (en) Deuterated compounds for electronic applications
KR101427457B1 (ko) 전자적 응용을 위한 중수소화된 화합물
JP6148271B2 (ja) 有機電子デバイス用の重水素化合物および、それらの重水素化合物を有する有機電子デバイス。
US8465849B2 (en) Deuterated zirconium compound for electronic applications
JP6110307B2 (ja) 電気活性材料

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20130510

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20130510

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20140417

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20140422

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20140722

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20140812

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20141028

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20141125

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20141225

R150 Certificate of patent or registration of utility model

Ref document number: 5676579

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

S111 Request for change of ownership or part of ownership

Free format text: JAPANESE INTERMEDIATE CODE: R313113

S531 Written request for registration of change of domicile

Free format text: JAPANESE INTERMEDIATE CODE: R313531

R350 Written notification of registration of transfer

Free format text: JAPANESE INTERMEDIATE CODE: R350

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250