JP5606070B2 - 高い比表面積を有する透明な硫化亜鉛 - Google Patents
高い比表面積を有する透明な硫化亜鉛 Download PDFInfo
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- JP5606070B2 JP5606070B2 JP2009538729A JP2009538729A JP5606070B2 JP 5606070 B2 JP5606070 B2 JP 5606070B2 JP 2009538729 A JP2009538729 A JP 2009538729A JP 2009538729 A JP2009538729 A JP 2009538729A JP 5606070 B2 JP5606070 B2 JP 5606070B2
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- zinc sulfide
- zinc
- sulfide
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2/00—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor
- A61L2/16—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor using chemical substances
- A61L2/23—Solid substances, e.g. granules, powders, blocks, tablets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G9/00—Compounds of zinc
- C01G9/08—Sulfides
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/30—Sulfur-, selenium- or tellurium-containing compounds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/04—Compounds of zinc
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/66—Additives characterised by particle size
- C09D7/67—Particle size smaller than 100 nm
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/66—Additives characterised by particle size
- C09D7/68—Particle size between 100-1000 nm
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09G—POLISHING COMPOSITIONS; SKI WAXES
- C09G1/00—Polishing compositions
- C09G1/02—Polishing compositions containing abrasives or grinding agents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y40/00—Manufacture or treatment of nanostructures
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/12—Surface area
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Materials Engineering (AREA)
- Nanotechnology (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Epidemiology (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Chemical & Material Sciences (AREA)
- Polymers & Plastics (AREA)
- Physics & Mathematics (AREA)
- Composite Materials (AREA)
- Veterinary Medicine (AREA)
- General Physics & Mathematics (AREA)
- Crystallography & Structural Chemistry (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
- Glass Compositions (AREA)
- Paper (AREA)
- Chemically Coating (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Paints Or Removers (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Description
例1:
貯蔵容器中に、温度65℃の蒸留水50mlおよびZnSO4水溶液(120g/l)500mlならびにNa2S水溶液(60g/l)500mlを同時に撹拌下で添加した。該溶液は同様に65℃の温度を有していた。懸濁液中のpH値が3〜4になるように制御しつつ、両方の溶液を貯蔵容器へ添加した。
Claims (22)
- 硫化亜鉛において、300未満の散乱能および白色力(DIN55982による)、15〜300m2/gの比表面積(BET、DIN−ISO9277により測定)、および40nm未満の平均微結晶サイズを有することを特徴とする、硫化亜鉛、ただし、比表面積径85nm、比表面積17.3m2/gを有するZnS微粒子、比表面積径10nm、比表面積147.7m2/gを有するZnS微粒子、および数平均粒子径4.7nmのZnSナノ粒子を除く。
- 100未満の散乱能および白色力および30〜250m2/gの比表面積を有することを特徴とする、請求項1記載の硫化亜鉛。
- 70未満の散乱能および白色力および50〜200m2/gの比表面積を有することを特徴とする、請求項1または2記載の硫化亜鉛。
- 硫化亜鉛が無機的かつ/または有機的に後処理されていることを特徴とする、請求項1から3までのいずれか1項記載の硫化亜鉛。
- 請求項1から4までのいずれか1項記載の硫化亜鉛の製造方法において、硫化物イオンを含有する化合物の水溶液を、亜鉛化合物を含有する水溶液と混合し、その際、5のpH値を越えないようにこの混合を制御し、かつ硫化亜鉛の沈殿後に、撹拌下で硫化物イオンを含有する化合物の水溶液をさらに添加することにより懸濁液のpH値を7の値になるまで調整し、得られた硫化亜鉛を濾過し、洗浄し、乾燥させることを特徴とする、請求項1から4までのいずれか1項記載の硫化亜鉛の製造方法。
- 硫化亜鉛を乾燥後、さらに、粉砕することを特徴とする、請求項5項記載の硫化亜鉛の製造方法。
- 硫化亜鉛を乾燥後、または乾燥および粉砕後、さらに、無機的かつ/または有機的に後処理することを特徴とする、請求項5又は6記載の硫化亜鉛の製造方法。
- 硫化亜鉛の一次粒径を、原料溶液の選択によって制御することを特徴とする、請求項5から7までのいずれか1項記載の方法。
- 硫化物イオンを含有する化合物として、金属硫化物、金属多硫化物、有機硫化物イオン含有物質、またはこれらの化合物の混合物を使用することを特徴とする、請求項5から8までのいずれか1項記載の方法。
- 金属多硫化物がアルカリ金属の群の化合物であり、かつ/または有機硫化物イオン含有物質がチオアセトアミドであることを特徴とする、請求項9記載の方法。
- 亜鉛化合物として、硫酸亜鉛、塩化亜鉛、または有機亜鉛化合物、またはこれらの化合物の混合物を使用することを特徴とする、請求項5から10までのいずれか1項記載の方法。
- 有機亜鉛化合物が酢酸亜鉛であることを特徴とする、請求項11記載の方法。
- 亜鉛化合物の水溶液に、気体状の硫化水素(H2S)を導通し、その際、5のpH値を越えないように、気体状の硫化水素(H2S)の添加を制御し、かつ硫化亜鉛の沈殿後に、気体状の硫化水素(H2S)をさらに添加することによって、懸濁液のpH値を7の値になるまで調整し、得られた硫化亜鉛を濾過し、洗浄し、乾燥させることを特徴とする、請求項1から4までのいずれか1項記載の硫化亜鉛の製造方法。
- 硫化亜鉛を乾燥後、さらに粉砕することを特徴とする、請求項13に記載の方法。
- 超微粒子状の硫化亜鉛の沈殿を、沈降セル、T/Y強制ミキサー、マイクロ反応器またはマイクロジェット反応器中で、連続的もしくは不連続的な運転法で行うことを特徴とする、請求項5から14までのいずれか1項記載の方法。
- 沈殿を、一段階で、もしくは多段階で行うことができることを特徴とする、請求項5から15までのいずれか1項記載の方法。
- 沈殿を二段階で行うことを特徴とする、請求項16記載の方法。
- 乾燥を、回転管炉、噴霧乾燥器、炉床炉中で、または凍結乾燥により行うことを特徴とする、請求項5から17までのいずれか1項記載の方法。
- 水の除去を、フラッシュ技術により行うことを特徴とする、請求項5から17までのいずれか1項記載の方法。
- 硫化亜鉛を、ピンミル、コロプレックスミル、ジルコプレックスミル、蒸気ジェットミルまたは空気ジェットミル中で超微粉砕することを特徴とする、請求項6から19までのいずれか1項記載の方法。
- 透明性および/または着色性を有する合成有機ポリマー、該ポリマーから製造される成形部材、被覆、目地材、またはシーラント中での請求項1から4までのいずれか1項記載の硫化亜鉛の使用。
- プラスチック中での、ポリマー製造の際の、ラッカー、塗料、繊維、紙、接着剤、セラミック、エナメル、吸着剤、イオン交換体、研磨剤もしくはポリッシング剤、耐寒性潤滑剤もしくは耐寒性潤滑剤コンセントレート、耐火製品、硬質コンクリート材料、医療用品、または化粧品における請求項1から4までのいずれか1項記載の硫化亜鉛の使用。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE102006057224.6 | 2006-12-01 | ||
DE102006057224 | 2006-12-01 | ||
PCT/EP2007/063199 WO2008065208A1 (de) | 2006-12-01 | 2007-12-03 | Transparentes zinksulfid grosser spezifischer oberfläche |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2010510953A JP2010510953A (ja) | 2010-04-08 |
JP5606070B2 true JP5606070B2 (ja) | 2014-10-15 |
Family
ID=39047547
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2009538729A Active JP5606070B2 (ja) | 2006-12-01 | 2007-12-03 | 高い比表面積を有する透明な硫化亜鉛 |
Country Status (12)
Country | Link |
---|---|
US (1) | US20100063164A1 (ja) |
EP (1) | EP2099868A1 (ja) |
JP (1) | JP5606070B2 (ja) |
KR (1) | KR101424029B1 (ja) |
CN (1) | CN101679770B (ja) |
AR (1) | AR064117A1 (ja) |
BR (1) | BRPI0719734A2 (ja) |
CA (1) | CA2671046A1 (ja) |
DE (1) | DE102007055693A1 (ja) |
MX (1) | MX2009005631A (ja) |
TW (1) | TW200837017A (ja) |
WO (1) | WO2008065208A1 (ja) |
Families Citing this family (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20120132277A1 (en) * | 2010-11-30 | 2012-05-31 | General Electric Company | Photovoltaic device and method for making |
EP2511236B1 (en) | 2011-04-14 | 2015-07-01 | Rohm and Haas Company | Improved quality multi-spectral zinc sulfide |
EP2634157B1 (en) | 2011-05-24 | 2016-08-10 | Rohm and Haas Company | Improved quality multi-spectral zinc sulfide |
US9163130B2 (en) | 2012-06-12 | 2015-10-20 | Sachtleben Chemie Gmbh | Method for the production of ZnS particles having a metal oxide coating and a cobalt content, products obtained thereby, and use of said products |
CN103288123B (zh) * | 2013-05-08 | 2015-03-11 | 洛阳市宏源化工研究所 | 一种闭路循环制备精细硫化锌的方法 |
CN103965657B (zh) * | 2014-05-05 | 2016-01-13 | 潍坊大耀新材料有限公司 | 一种ZnS粉的表面改性方法 |
EP2966051B1 (en) * | 2014-07-10 | 2023-11-01 | Centre National De La Recherche Scientifique | Method of manufacturing a sulfide-based ceramic element for IR-optics applications |
DE102014018586A1 (de) | 2014-12-17 | 2016-06-23 | Merck Patent Gmbh | Lasermarkierbare und laserschweißbare polymere Materialien |
JP7238472B2 (ja) * | 2019-02-28 | 2023-03-14 | 東洋インキScホールディングス株式会社 | グラビアもしくはフレキソ白色インキとその利用 |
CN115895295B (zh) * | 2022-10-25 | 2024-03-29 | 中信钛业股份有限公司 | 一种玻纤增强尼龙专用型二氧化钛颜料的制备方法 |
CN117023628B (zh) * | 2023-10-07 | 2024-02-23 | 艾肯希红外科技(广东)有限公司 | 一种金属硫化物及其应用、含有金属硫化物的树脂组合物 |
Family Cites Families (19)
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US3941603A (en) * | 1974-02-01 | 1976-03-02 | E. I. Du Pont De Nemours & Company | TiO2 Pigment for industrial paints based on water reducible systems |
GB1479989A (en) * | 1975-07-17 | 1977-07-13 | Tioxide Group Ltd | Treatment of pigment |
US4075031A (en) * | 1976-09-30 | 1978-02-21 | E. I. Du Pont De Nemours And Company | TiO2 Pigment coated with dense silica and porous alumina/silica |
JPH0781936A (ja) * | 1993-09-10 | 1995-03-28 | Nippon Mektron Ltd | 表面修飾金属硫化物超微粒子の製造法 |
DE19638475A1 (de) * | 1996-09-20 | 1998-03-26 | Metallgesellschaft Ag | Zinksulfid-Pigment für den Einsatz in Formteilen aus synthetischen organischen Polymeren und in Beschichtungen |
EP1179566B1 (en) * | 1998-12-03 | 2007-03-07 | Kaneka Corporation | Elastomer composition and thermoplastic resin composition containing the same |
US6228815B1 (en) * | 1999-06-29 | 2001-05-08 | Alliedsignal Inc. | Solid lubricants containing bismuth sulfide for use in friction lining |
US6071612A (en) * | 1999-10-22 | 2000-06-06 | Arteva North America S.A.R.L. | Fiber and filament with zinc sulfide delusterant |
US6724141B2 (en) * | 2001-10-30 | 2004-04-20 | Agfa-Gevaert | Particular type of a thin layer inorganic light emitting device |
US20050084543A1 (en) * | 2002-01-11 | 2005-04-21 | Sandrine Rochat | Use of zinc sulfide as an anti-mite agent |
DE10217005A1 (de) * | 2002-02-28 | 2003-09-04 | Roehm Gmbh | Polymethacrylimid-Schaumstoffe mit verminderter Entflammbarkeit sowie Verfahren zur Herstellung |
JP4238011B2 (ja) * | 2002-10-31 | 2009-03-11 | 株式会社日本触媒 | 金属硫化物の製造方法 |
DE10260718A1 (de) * | 2002-12-23 | 2004-07-08 | Degussa Ag | Mit Siliziumdioxid umhülltes Titandioxid |
JP2004296733A (ja) * | 2003-03-26 | 2004-10-21 | Masakazu Kobayashi | 固体の分離方法 |
JP2005239505A (ja) * | 2004-02-27 | 2005-09-08 | Bando Chem Ind Ltd | 硫化金属粒子およびその製造方法ならびに複合粒子 |
US20070131136A1 (en) * | 2004-04-27 | 2007-06-14 | Osmose, Inc. | Composition And Process For Coloring Wood |
WO2006038420A1 (ja) * | 2004-09-30 | 2006-04-13 | Kaneka Corporation | ポリマー修飾金属カルコゲン化物ナノ粒子の製造方法 |
US20060216508A1 (en) * | 2005-03-24 | 2006-09-28 | 3M Innovative Properties Company | Polymer nanocomposite having surface modified nanoparticles and methods of preparing same |
JP2009526822A (ja) * | 2006-02-16 | 2009-07-23 | ザッハトレーベン ヒェミー ゲゼルシヤフト ミット ベシュレンクテル ハフツング | 殺生物組成物 |
-
2007
- 2007-12-03 JP JP2009538729A patent/JP5606070B2/ja active Active
- 2007-12-03 CN CN200780044404.9A patent/CN101679770B/zh active Active
- 2007-12-03 US US12/515,973 patent/US20100063164A1/en not_active Abandoned
- 2007-12-03 TW TW096145864A patent/TW200837017A/zh unknown
- 2007-12-03 KR KR1020097013697A patent/KR101424029B1/ko active IP Right Grant
- 2007-12-03 CA CA002671046A patent/CA2671046A1/en not_active Abandoned
- 2007-12-03 MX MX2009005631A patent/MX2009005631A/es unknown
- 2007-12-03 WO PCT/EP2007/063199 patent/WO2008065208A1/de active Application Filing
- 2007-12-03 DE DE102007055693A patent/DE102007055693A1/de not_active Withdrawn
- 2007-12-03 EP EP07847710A patent/EP2099868A1/de not_active Withdrawn
- 2007-12-03 BR BRPI0719734-9A patent/BRPI0719734A2/pt not_active IP Right Cessation
- 2007-12-04 AR ARP070105406A patent/AR064117A1/es not_active Application Discontinuation
Also Published As
Publication number | Publication date |
---|---|
AR064117A1 (es) | 2009-03-11 |
CN101679770B (zh) | 2014-12-17 |
JP2010510953A (ja) | 2010-04-08 |
EP2099868A1 (de) | 2009-09-16 |
DE102007055693A1 (de) | 2008-06-05 |
CA2671046A1 (en) | 2008-06-05 |
CN101679770A (zh) | 2010-03-24 |
TW200837017A (en) | 2008-09-16 |
US20100063164A1 (en) | 2010-03-11 |
KR20090086271A (ko) | 2009-08-11 |
MX2009005631A (es) | 2009-06-30 |
BRPI0719734A2 (pt) | 2013-12-10 |
WO2008065208A1 (de) | 2008-06-05 |
KR101424029B1 (ko) | 2014-07-28 |
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