JP5587310B2 - ジアルキルスルフィドの精製方法 - Google Patents

ジアルキルスルフィドの精製方法 Download PDF

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Publication number
JP5587310B2
JP5587310B2 JP2011517882A JP2011517882A JP5587310B2 JP 5587310 B2 JP5587310 B2 JP 5587310B2 JP 2011517882 A JP2011517882 A JP 2011517882A JP 2011517882 A JP2011517882 A JP 2011517882A JP 5587310 B2 JP5587310 B2 JP 5587310B2
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JP
Japan
Prior art keywords
sulfide
dialkyl
dialkyl sulfide
metal
alkali
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JP2011517882A
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English (en)
Japanese (ja)
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JP2011528011A5 (enExample
JP2011528011A (ja
Inventor
バークハート，エリザベス
ネイ，ケビン
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BASF SE
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BASF SE
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/26—Separation; Purification; Stabilisation; Use of additives
    • C07C319/28—Separation; Purification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B57/00—Separation of optically-active compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C321/00—Thiols, sulfides, hydropolysulfides or polysulfides
    • C07C321/12—Sulfides, hydropolysulfides, or polysulfides having thio groups bound to acyclic carbon atoms
    • C07C321/14—Sulfides, hydropolysulfides, or polysulfides having thio groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F5/00—Compounds containing elements of Groups 3 or 13 of the Periodic Table
    • C07F5/02—Boron compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F5/00—Compounds containing elements of Groups 3 or 13 of the Periodic Table
    • C07F5/02—Boron compounds
    • C07F5/027—Organoboranes and organoborohydrides

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
JP2011517882A 2008-07-15 2009-07-10 ジアルキルスルフィドの精製方法 Expired - Fee Related JP5587310B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US8086808P 2008-07-15 2008-07-15
US61/080,868 2008-07-15
PCT/EP2009/058848 WO2010007006A1 (en) 2008-07-15 2009-07-10 Process to purify dialkyl sulfides

Publications (3)

Publication Number Publication Date
JP2011528011A JP2011528011A (ja) 2011-11-10
JP2011528011A5 JP2011528011A5 (enExample) 2012-08-30
JP5587310B2 true JP5587310B2 (ja) 2014-09-10

Family

ID=41110509

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2011517882A Expired - Fee Related JP5587310B2 (ja) 2008-07-15 2009-07-10 ジアルキルスルフィドの精製方法

Country Status (11)

Country Link
US (2) US8586796B2 (enExample)
EP (1) EP2315743B1 (enExample)
JP (1) JP5587310B2 (enExample)
KR (1) KR101617055B1 (enExample)
CN (1) CN102099332B (enExample)
CA (1) CA2730707C (enExample)
DK (1) DK2315743T3 (enExample)
ES (1) ES2727702T3 (enExample)
RU (1) RU2515986C2 (enExample)
SI (1) SI2315743T1 (enExample)
WO (1) WO2010007006A1 (enExample)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2965562B1 (fr) * 2010-09-30 2013-03-01 Arkema France Procede de preparation de disulfures de dialkyle
FR2994974B1 (fr) * 2012-08-30 2015-05-01 Arkema France Distillation reactive des dso
CN107674026B (zh) * 2017-11-03 2019-12-06 海化生命(厦门)科技有限公司 鲁索替尼中间体(3r)-3-(4-溴-1h-吡唑-1-基)-环戊烷基丙腈的制备方法
CN107857728A (zh) * 2017-11-20 2018-03-30 成都惟邦药业有限公司 一种利非司特中间体的合成方法
US10774040B1 (en) 2019-04-29 2020-09-15 Chevron Phillips Chemical Company Lp Processes for removing carbon disulfide from symmetrical and asymmetrical sulfide product streams
CN116283687A (zh) * 2022-09-07 2023-06-23 金川集团股份有限公司 一种二异戊基硫醚的合成工艺
US11945770B1 (en) * 2023-03-06 2024-04-02 Chevron Phillips Chemical Company Lp Catalytic processes and systems for alkyl sulfide purification

Family Cites Families (31)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1681600A (en) * 1925-07-21 1928-08-21 Christiaan Van Loon Process of preparing alkali-metal alcoholates of compounds containing alcoholic hydroxyl groups
JPS496287B1 (enExample) 1968-01-26 1974-02-13
US3835559A (en) 1972-03-27 1974-09-17 G Kotter Machine for ironing trousers
US4173619A (en) * 1978-03-14 1979-11-06 Erickson Donald C Combustion gas desulfurization
US4358297A (en) * 1980-01-02 1982-11-09 Exxon Research And Engineering Company Removal of sulfur from process streams
AR230264A1 (es) * 1980-11-26 1984-03-01 Merz & Co Gmbh & Co Procedimiento para la obtencion de compuestos de xantato
CA1244480A (en) * 1981-10-05 1988-11-08 Daniel A. Dimmig Deodorization of dialkyl polysulfides
EP0189606B1 (en) * 1985-02-01 1989-08-09 European Atomic Energy Community (Euratom) Process for selective adsorption of sulfur compounds from gaseous mixtures containing mercaptans
US4964957A (en) * 1988-12-06 1990-10-23 Phillips Petroleum Company Purification of high boiling alkyl sulfides
US5480860A (en) * 1988-12-23 1996-01-02 Petrolite Corporation Methods for reducing sulfides in sewage gas
US5382417A (en) * 1990-01-03 1995-01-17 Herr Haase, Inc. Process for removal of selected component gases from multi-component gas streams
US5089246A (en) * 1990-01-29 1992-02-18 Atochem North America, Inc. Process for converting carbon disulfide to hydrogen sulfide in hydrogen sulfide/carbon disulfide mixtures
US5157201A (en) * 1990-06-22 1992-10-20 Exxon Chemical Patents Inc. Process for adsorbing sulfur species from propylene/propane using regenerable adsorbent
US5302771A (en) * 1991-04-08 1994-04-12 Exxon Chemical Patents, Inc. Process for upgrading the quality of light ends
LU87923A1 (de) * 1991-04-24 1992-11-16 Euratom Verfahren zum entfernen von schwefelwasserstoff und/oder schwefelkohlenstoff aus abgasen
FR2694197B1 (fr) * 1992-07-30 1994-09-02 Atochem Elf Sa Désodorisant des effluents de papeterie à base d'ester d'acide undécylénique.
RU2152421C1 (ru) * 1994-05-19 2000-07-10 Мицуи Петрокемикал Индастриз Лтд. СПОСОБ ОЧИСТКИ α-ОЛЕФИНОВ ДЛЯ ПОЛИМЕРИЗАЦИИ И СПОСОБ ПОЛУЧЕНИЯ ПОЛИ-α-ОЛЕФИНОВ
US5559271A (en) * 1995-07-26 1996-09-24 Phillips Petroleum Company Organic polysulfide compositions having reduced odor
JP3567034B2 (ja) * 1995-11-30 2004-09-15 ジーイー東芝シリコーン株式会社 アルコキシシランの精製方法
US6136144A (en) * 1996-06-06 2000-10-24 Thermatrix, Inc. Method of removing sulfur from a process gas stream using a packed bed calcinator
JPH11137964A (ja) * 1997-11-06 1999-05-25 Nec Corp 悪臭物質の除去方法及び脱臭装置
US6015536A (en) * 1998-01-14 2000-01-18 Ecolab Inc. Peroxyacid compound use in odor reduction
AR014299A1 (es) * 1998-01-14 2001-02-07 Ecolab Inc Un procedimiento para remover un olor de un efluente atmosférico, un tratamiento previo o un tratamiento posterior para remover un olor de un efluente atmosférico y efluente atmosférico obtenido con dicho procedimiento.
DE19828977A1 (de) 1998-06-29 1999-12-30 Basf Ag Verfahren zur Entfernung saurer Gasbestandteile aus Gasen
FR2781795B1 (fr) * 1998-07-31 2000-09-08 Atochem Elf Sa Compositions a base de dimethyldisulfure a odeur masquee
US6051739A (en) * 1999-01-26 2000-04-18 Phillips Petroleum Company Process for producing organic polysulfides
JP2002020765A (ja) * 2000-07-04 2002-01-23 Idemitsu Petrochem Co Ltd 炭化水素中の二硫化炭素の除去方法
US6736879B2 (en) * 2002-05-01 2004-05-18 Chevron Phillips Chemical Company Lp Process to prepare low carbon disulfide containing dimethyl sulfide
US7446077B2 (en) * 2004-03-17 2008-11-04 Intevep, S.A. Selective sulfur removal from hydrocarbon streams by absorption
US20070123729A1 (en) * 2005-11-29 2007-05-31 Farnham William B Synthesis of trithiocarbonates
KR20090024752A (ko) * 2006-06-26 2009-03-09 바스프 에스이 보란 에테르 착물

Also Published As

Publication number Publication date
CA2730707A1 (en) 2010-01-21
KR20110031974A (ko) 2011-03-29
CA2730707C (en) 2016-09-13
SI2315743T1 (sl) 2019-08-30
WO2010007006A1 (en) 2010-01-21
US9073831B2 (en) 2015-07-07
KR101617055B1 (ko) 2016-04-29
US20140051891A1 (en) 2014-02-20
JP2011528011A (ja) 2011-11-10
RU2011105242A (ru) 2012-08-20
CN102099332B (zh) 2014-02-12
DK2315743T3 (da) 2019-06-03
RU2515986C2 (ru) 2014-05-20
CN102099332A (zh) 2011-06-15
ES2727702T3 (es) 2019-10-18
US20110124920A1 (en) 2011-05-26
EP2315743A1 (en) 2011-05-04
US8586796B2 (en) 2013-11-19
EP2315743B1 (en) 2019-05-08

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