CN102099332B - 提纯二烷基硫醚的方法 - Google Patents

提纯二烷基硫醚的方法 Download PDF

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Publication number
CN102099332B
CN102099332B CN200980127616.2A CN200980127616A CN102099332B CN 102099332 B CN102099332 B CN 102099332B CN 200980127616 A CN200980127616 A CN 200980127616A CN 102099332 B CN102099332 B CN 102099332B
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CN
China
Prior art keywords
metal
sulfide
alkaline earth
dialkyl
alkali
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Expired - Fee Related
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CN200980127616.2A
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English (en)
Chinese (zh)
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CN102099332A (zh
Inventor
E·伯克哈特
K·奈
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BASF SE
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BASF SE
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Publication of CN102099332A publication Critical patent/CN102099332A/zh
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/26—Separation; Purification; Stabilisation; Use of additives
    • C07C319/28—Separation; Purification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B57/00—Separation of optically-active compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C321/00—Thiols, sulfides, hydropolysulfides or polysulfides
    • C07C321/12—Sulfides, hydropolysulfides, or polysulfides having thio groups bound to acyclic carbon atoms
    • C07C321/14—Sulfides, hydropolysulfides, or polysulfides having thio groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F5/00—Compounds containing elements of Groups 3 or 13 of the Periodic Table
    • C07F5/02—Boron compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F5/00—Compounds containing elements of Groups 3 or 13 of the Periodic Table
    • C07F5/02—Boron compounds
    • C07F5/027—Organoboranes and organoborohydrides

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
CN200980127616.2A 2008-07-15 2009-07-10 提纯二烷基硫醚的方法 Expired - Fee Related CN102099332B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US8086808P 2008-07-15 2008-07-15
US61/080868 2008-07-15
PCT/EP2009/058848 WO2010007006A1 (en) 2008-07-15 2009-07-10 Process to purify dialkyl sulfides

Publications (2)

Publication Number Publication Date
CN102099332A CN102099332A (zh) 2011-06-15
CN102099332B true CN102099332B (zh) 2014-02-12

Family

ID=41110509

Family Applications (1)

Application Number Title Priority Date Filing Date
CN200980127616.2A Expired - Fee Related CN102099332B (zh) 2008-07-15 2009-07-10 提纯二烷基硫醚的方法

Country Status (11)

Country Link
US (2) US8586796B2 (enExample)
EP (1) EP2315743B1 (enExample)
JP (1) JP5587310B2 (enExample)
KR (1) KR101617055B1 (enExample)
CN (1) CN102099332B (enExample)
CA (1) CA2730707C (enExample)
DK (1) DK2315743T3 (enExample)
ES (1) ES2727702T3 (enExample)
RU (1) RU2515986C2 (enExample)
SI (1) SI2315743T1 (enExample)
WO (1) WO2010007006A1 (enExample)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2965562B1 (fr) * 2010-09-30 2013-03-01 Arkema France Procede de preparation de disulfures de dialkyle
FR2994974B1 (fr) * 2012-08-30 2015-05-01 Arkema France Distillation reactive des dso
CN107674026B (zh) * 2017-11-03 2019-12-06 海化生命(厦门)科技有限公司 鲁索替尼中间体(3r)-3-(4-溴-1h-吡唑-1-基)-环戊烷基丙腈的制备方法
CN107857728A (zh) * 2017-11-20 2018-03-30 成都惟邦药业有限公司 一种利非司特中间体的合成方法
US10774040B1 (en) 2019-04-29 2020-09-15 Chevron Phillips Chemical Company Lp Processes for removing carbon disulfide from symmetrical and asymmetrical sulfide product streams
CN116283687A (zh) * 2022-09-07 2023-06-23 金川集团股份有限公司 一种二异戊基硫醚的合成工艺
US11945770B1 (en) * 2023-03-06 2024-04-02 Chevron Phillips Chemical Company Lp Catalytic processes and systems for alkyl sulfide purification

Family Cites Families (31)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1681600A (en) * 1925-07-21 1928-08-21 Christiaan Van Loon Process of preparing alkali-metal alcoholates of compounds containing alcoholic hydroxyl groups
JPS496287B1 (enExample) 1968-01-26 1974-02-13
US3835559A (en) 1972-03-27 1974-09-17 G Kotter Machine for ironing trousers
US4173619A (en) 1978-03-14 1979-11-06 Erickson Donald C Combustion gas desulfurization
US4358297A (en) 1980-01-02 1982-11-09 Exxon Research And Engineering Company Removal of sulfur from process streams
AR230264A1 (es) * 1980-11-26 1984-03-01 Merz & Co Gmbh & Co Procedimiento para la obtencion de compuestos de xantato
CA1244480A (en) * 1981-10-05 1988-11-08 Daniel A. Dimmig Deodorization of dialkyl polysulfides
DE3572129D1 (en) 1985-02-01 1989-09-14 Euratom Process for selective adsorption of sulfur compounds from gaseous mixtures containing mercaptans
US4964957A (en) * 1988-12-06 1990-10-23 Phillips Petroleum Company Purification of high boiling alkyl sulfides
US5480860A (en) 1988-12-23 1996-01-02 Petrolite Corporation Methods for reducing sulfides in sewage gas
US5382417A (en) 1990-01-03 1995-01-17 Herr Haase, Inc. Process for removal of selected component gases from multi-component gas streams
US5089246A (en) * 1990-01-29 1992-02-18 Atochem North America, Inc. Process for converting carbon disulfide to hydrogen sulfide in hydrogen sulfide/carbon disulfide mixtures
US5157201A (en) 1990-06-22 1992-10-20 Exxon Chemical Patents Inc. Process for adsorbing sulfur species from propylene/propane using regenerable adsorbent
US5302771A (en) 1991-04-08 1994-04-12 Exxon Chemical Patents, Inc. Process for upgrading the quality of light ends
LU87923A1 (de) 1991-04-24 1992-11-16 Euratom Verfahren zum entfernen von schwefelwasserstoff und/oder schwefelkohlenstoff aus abgasen
FR2694197B1 (fr) 1992-07-30 1994-09-02 Atochem Elf Sa Désodorisant des effluents de papeterie à base d'ester d'acide undécylénique.
RU2152421C1 (ru) 1994-05-19 2000-07-10 Мицуи Петрокемикал Индастриз Лтд. СПОСОБ ОЧИСТКИ α-ОЛЕФИНОВ ДЛЯ ПОЛИМЕРИЗАЦИИ И СПОСОБ ПОЛУЧЕНИЯ ПОЛИ-α-ОЛЕФИНОВ
US5559271A (en) 1995-07-26 1996-09-24 Phillips Petroleum Company Organic polysulfide compositions having reduced odor
JP3567034B2 (ja) * 1995-11-30 2004-09-15 ジーイー東芝シリコーン株式会社 アルコキシシランの精製方法
US6136144A (en) 1996-06-06 2000-10-24 Thermatrix, Inc. Method of removing sulfur from a process gas stream using a packed bed calcinator
JPH11137964A (ja) * 1997-11-06 1999-05-25 Nec Corp 悪臭物質の除去方法及び脱臭装置
AR014299A1 (es) 1998-01-14 2001-02-07 Ecolab Inc Un procedimiento para remover un olor de un efluente atmosférico, un tratamiento previo o un tratamiento posterior para remover un olor de un efluente atmosférico y efluente atmosférico obtenido con dicho procedimiento.
US6015536A (en) 1998-01-14 2000-01-18 Ecolab Inc. Peroxyacid compound use in odor reduction
DE19828977A1 (de) 1998-06-29 1999-12-30 Basf Ag Verfahren zur Entfernung saurer Gasbestandteile aus Gasen
FR2781795B1 (fr) 1998-07-31 2000-09-08 Atochem Elf Sa Compositions a base de dimethyldisulfure a odeur masquee
US6051739A (en) * 1999-01-26 2000-04-18 Phillips Petroleum Company Process for producing organic polysulfides
JP2002020765A (ja) * 2000-07-04 2002-01-23 Idemitsu Petrochem Co Ltd 炭化水素中の二硫化炭素の除去方法
US6736879B2 (en) 2002-05-01 2004-05-18 Chevron Phillips Chemical Company Lp Process to prepare low carbon disulfide containing dimethyl sulfide
US7446077B2 (en) 2004-03-17 2008-11-04 Intevep, S.A. Selective sulfur removal from hydrocarbon streams by absorption
US20070123729A1 (en) * 2005-11-29 2007-05-31 Farnham William B Synthesis of trithiocarbonates
ATE478080T1 (de) * 2006-06-26 2010-09-15 Basf Se Boranetherkomplexe

Also Published As

Publication number Publication date
CN102099332A (zh) 2011-06-15
JP5587310B2 (ja) 2014-09-10
JP2011528011A (ja) 2011-11-10
KR101617055B1 (ko) 2016-04-29
RU2515986C2 (ru) 2014-05-20
US20110124920A1 (en) 2011-05-26
SI2315743T1 (sl) 2019-08-30
DK2315743T3 (da) 2019-06-03
KR20110031974A (ko) 2011-03-29
EP2315743A1 (en) 2011-05-04
US20140051891A1 (en) 2014-02-20
EP2315743B1 (en) 2019-05-08
WO2010007006A1 (en) 2010-01-21
RU2011105242A (ru) 2012-08-20
US8586796B2 (en) 2013-11-19
CA2730707C (en) 2016-09-13
US9073831B2 (en) 2015-07-07
CA2730707A1 (en) 2010-01-21
ES2727702T3 (es) 2019-10-18

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Granted publication date: 20140212